不同变质程度煤的高分辨率透射电镜分析

利用高分辨率透射电子显微镜(HRTEM)分析了三种不同变质程度煤样的结构特征。基于傅里叶-反傅里叶变换方法,并结合Matlab、Arcgis和Auto CAD软件,通过图像分析技术,获得了HRTEM照片的晶格条纹参数。结果表明,三种煤样的晶格条纹呈现不同特征,按条纹长度分别归属于1×1-8×8共计八个类型。以3×3为临界点,在1×1和2×2中,ML-8中芳香层片的比例高于DP-4和XM-3;在3×3-8×8中,ML-8中芳香层片的比例低于DP-4和XM-3。对比HRTEM和XRD参数d002发现,随着镜质组反射率的增加d002都呈现递减趋势。     

Photoluminescence Property of Co3O4 Nanowires

Co3O4 nanowire arrays are fabricated by electrodeposition with following heat-treatment in atmosphere ambient. Photoluminescence is investigated at 295K. In the experiment, when increasing the excitation light wavelength from 260 nm to 360 nm, two kinds of emissions corresponding to the increasing excitation light wavelength are observed. One of them alters the excited emission position, another keeps its emission position. The distinct behaviour of excited emissions related to the increasing excitation wavelength indicates that the mechanism of them must be different. According to the experimental comparison and first-principle calculation, the two kinds of emissions are discussed.     

具有粗糙核的Marcinkiewicz积分交换子在齐型Herz-Morrey空间上的有界性

建立了一类具有粗糙核的Marcinkiewicz积分交换子在齐型Herz-Morrey空间上的有界性.     

具有变时滞的离散双向联想记忆神经网络的全局指数稳定性

利用Lyapunov函数和线性矩阵不等式(LMI),给出了判定一类双向联想记忆(BAM)神经网络模型的指数稳定的充分性条件.该条件去掉了以往论文中所要求的激活函数单调,可微分的条件,而且所得结果利用里的工具易于检测.并举例说明本文结果的有效性.     

碳纤维上电沉积Pd-Ag合金纳米粒子链及其氢传感性能

在碳纤维上采用三脉冲电沉积的方法制备出钯银合金纳米粒子链.把表面覆盖有Pd-Ag合金纳米粒子链的碳纤维组装成氢气传感器.采用扫描电子显微镜(SEM)和X射线能谱(EDX)表征了合金纳米粒子链的形貌和成分,应用CHI660B电化学工作站测试其氢传感性能.结果表明,在钯、银离子摩尔比为15∶1的电解液中,在-1.0--1.5 V下,成核5-40 ms;在-0.25--0.35 V,生长200-300 s的条件下,即可获得银的质量分数为16.0%-25.0%的钯银合金纳米粒子链阵列.在室温下,传感器对在0.30%-5.00%(φ,体积分数,下同)范围内的氢气有响应,最快响应时间约为300 s,灵敏度最高可达31.0%;氢在0.30%-1.20%的范围内响应电流与氢气浓度成线性关系,超过4.00%时响应电流不再随浓度的增加而变化;在低于3.50%的浓度下氢传感器的重现性良好.     

傅里叶变换红外光谱法研究核辐照对三七总皂苷粉成分的影响

采用傅里叶变换红外光谱(卷积谱)法对经不同剂量y-射线核辐照的三七总皂苷粉进行了对比研究.辐照剂量不高于9kGy时,三七总皂苷粉样品的化学成分几乎没有发生变化;三七总皂苷粉样品经15kGy及以上的辐照剂量辐照后,可能产生新的化学成分;经21kGy的剂量辐照,三七总皂苷粉产生了人参、三七粉所含的普通成分(非三七总皂苷成分...     

一类推广后的Feigenbaum函数方程的光滑解

考虑一类推广后的Feigenbaum函数方程｛g（0）=1,-1≤g（x）≤1,x∈[-1,1],h（g（x））=g（g（h（x）））其中h（x）是[-1,1]上的递减光滑奇函数且满足h（0）=0,-1〈h’（x）〈0,z∈[-1,1]．利用构造性方法讨论上述方程的光滑解的存在性及唯一性．     

甲烷再燃还原NO过程中SO2的交互作用

综合Leeds机理,采用Chemkin程序的PFR模块,以Glarborg实验中的柱塞流反应器作为模拟对象,研究了甲烷再燃还原NO过程中SO2交互作用的影响.利用该模型计算甲烷再燃还原NO的结果与Glarborg的实验结果吻合;存在最佳空气过量系数0.8时甲烷再燃还原NO效率最高.进一步分析SO2对再燃还原NO影响的结...     

Interaction in the geometro-differential conception of extended particles and the Galilei semigroup of trajectories

Along the lines of a previous work, the geometrical structure of Hibert bundles describing extended quantum free particles is repeated with Galilei external and internal independent symmetries. Then, in order to introduce the interaction, this structure is extended by replacing configuration and momentum spaces by the socelled spaces of trajectories and extended velocity boosts, respectively. These provide representations giving the probability amplitudes for the particle to follow certain trajectories. The interaction can be introduced in the transformation law from functions on the space of trajectories (free dynamics) to functions on spacetime (intracting dynamics). This transformation law, which makes use of a universal distribution, is seen as a functional in our work according to a quantum functional theory which generalizes the ideas of de Broglie. Intertwining of induced representations gives the free propagator in the space of trajectories and, henceforth, the propagator with interaction in space-time for the extended particle.