FURTHER APPLICATIONS OF POLAR COORDINATES IN C~n

Simplify the proof on the domain of convergence of multiple power series and consider the case where some of z1, ··· , zn are contained only in a finite number of terms of the series. Obtain some results on holomorphic functions in Cn.     

MOLECULES AND NEW INTERACTIONAL STRUCTURES FOR A(2+1)-DIMENSIONAL GENERALIZED KONOPELCHENKO-DUBROVSKY-KAUP-KUPERSHMIDT EQUATION

Soliton molecules(SMs) of the(2+1)-dimensional generalized KonopelchenkoDubrovsky-Kaup-Kupershmidt(gKDKK) equation are found by utilizing a velocity resonance ansatz to N-soliton solutions,which can transform to asymmetric solitons upon assigning appropriate values to some parameters.Furthermore,a double-peaked lump solution can be constructed with breather degeneration approach.By applying a mixed technique of a resonance ansatz and conjugate complexes of partial parameters to multisoliton solu...     

较高场畸变系数的大电流三电极气体开关

气体开关作为脉冲功率装置的关键部件,其自击穿概率以及触发放电延时抖动对整个脉冲功率系统具有至关重要的影响。降低开关工作系数有利于提高开关稳定性,但延时抖动会随之增大。针对用于磁驱动实验的10 MA级大电流装置应用需求,设计了一种具有较高场畸变系数、能在较低工作系数条件下稳定工作的三电极气体开关,并开展了该开关的性能研究。模拟与实验结果表明：在触发电压与充电电压相当的条件下,开关的场畸变系数接近4,开关工作系数高于60%时,开关具有较低的延时抖动,抖动均方根小于3 ns。结合该开关设计了一个两级Marx储能模块,充电电压±50 kV条件下短路放电,模块回路放电电流峰值达到150 kA、周期2μs。上千次放电实验后,开关电极表面未发生明显烧蚀,工作正常。工作系数68.5%时,共计4 000发实验中未出现自放电现象,自击穿概率低于2.5×10-4。上述结果表明该开关可满足300～400只开关同时工作的大电流装置需求。     

基于改进的剪切波变换和引导滤波的红外弱小目标背景抑制方法

由于传统的背景抑制方法没有充分利用信号的方向信息,使其不能有效区分背景边缘和红外弱小目标,从而造成背景抑制结果中有较多的背景泄露.针对上述问题,本文利用改进的剪切波变换和引导滤波,提出了一种新的背景抑制方法.首先,采用改进的剪切波变换对红外弱小目标图像进行多尺度和多方向分解,将图像分解得到不同的高频子带系数和低频子带系数;其次,利用目标信号与边缘在方向上的差异,采用自适应引导滤波对高频子带系数进行处理;再次,对分解后的低频子带系数和处理后的高频子带系数进行改进的剪切波逆变换,得到预测的背景图像;最后,将原图像与背景预测图像相减获得背景抑制且目标增强的红外图像.为了验证本文方法的有效性,采用多组实验对其进行验证,并与经典的Max-Median、TDLMS和Top-hat等方法作比较.多组实验结果均表明本文方法在主观视觉和客观评价指标方面均优于其它三种经典方法,可有效提高红外搜索跟踪系统对红外弱小目标的探测概率.     

Synthesis and characterization of poly[(methylsilylene ethynylenephenyleneethynylene)-co-(dimethylsilylene ethynylenephenyleneethynylene)]s

<正>A series of poly[(methylsilylene ethynylenephenyleneethynylene)-co-(dimethylsilylene ethynylenephenyleneethynylene)]s were synthesized by the incorporation of various ratios of methylsilylene to dimethylsilylene units into the polymer chain backbone.The resultant copolymers were soluble in a variety of common organic solvents at room temperature.The copolymers were characterized by FT-IR,~1H-NMR,GPC,rheological analysis,differential scanning calorimetry(DSC) and thermogravimetric analysis(TGA).The results showed that the copolymers exhibited good processability and cured at low temperatures like 200℃.The curing reactions involved in hydrosilylation of Si—H and alkyne groups and the polymerization of alkynes.Y_(d5)(5%weight loss) of the cured copolymers ranged from 629℃to 686℃,and the decomposition residues of cured copolymers at 1000℃ranged from 88.1%to 90.9%under nitrogen.Thermal stability of the copolymers increased with the introduction of methylsilylene units into polymer chains.The cured copolymers were sintered at 1450℃,and the results of X-ray diffraction analysis showed that β-SiC was formed in the sintered products.     

大肠杆菌为模板制备Au@TiO_2催化剂及其CO氧化反应活性

许多微生物对金属离子有较强的吸附还原能力.本文利用大肠杆菌(DH5α)对金属离子较强的吸附与还原能力制备了Au@DH5α,再利用大肠杆菌的水分来水解钛酸四丁酯,得到Au@DH5α-Ti(OH)4样品,焙烧去除大肠杆菌后得到氧化钛包裹的纳米金粒子催化剂Au@TiO2.以N2吸附,X射线衍射(XRD),紫外-可见漫反射光谱(UV-VisDRS),热重-差热分析(TG-DTA),透射电镜(TEM)对所得材料进行表征.结果表明:该催化剂具有与大肠杆菌类似的杆状结构,以大肠杆菌为生物模板生成的氧化钛孔道结构在一定程度上抑制了金粒子的聚集长大.随菌体用量的增加,金粒子减小,等离子共振吸收发生紫移,催化剂有较大的比表面积,但催化剂中积炭量也会增加.将该催化剂用于CO氧化反应,发现当菌体用量为100或150mL时,制得的金催化剂可在80℃下将CO完全氧化为CO2.     

羰化法合成苯乙酸及其酯类的研究进展

综述了过渡金属催化的羰化法合成苯乙酸和苯乙酸酯近几十年来的研究进展。