排序方式: 共有21条查询结果,搜索用时 15 毫秒
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核酸水解产物嘌呤、嘧啶碱基在BDS柱上的分离及测定 总被引:7,自引:0,他引:7
用高效液相色谱法测定了核酸水解的中间产物及最终产物 6种嘌呤、嘧啶碱基 ,探讨了色谱柱、流动相等对其分离的影响 ,确定了最佳色谱条件为 :HypersilBDS C18柱 ,乙腈 0 1mol/LKH2 PO4 (H3 PO4 调节 pH至4 0 5 ) (体积比为 2∶98)作流动相 ,紫外检测器在 2 6 0nm波长下检测。方法的精密度在 3%以内 ,回收率在 82 %~ 114%。方法应用于酵母核酸样品的测定中 ,取得了很好的结果。 相似文献
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The China Dark Matter Experiment (CDEX) is located at the China Jinping Underground Laboratory (CJPL) and aims to directly detect the weakly interacting massive particles (WIMP) flux with high sensitivity in the low mass region. Here we present a study of the predicted photon and electron backgrounds including the background contribution of the structure materials of the germanium detector, the passive shielding materials, and the intrinsic radioactivity of the liquid argon that serves as an anti-Compton active shielding detector. A detailed geometry is modeled and the background contribution has been simulated based on the measured radioactivities of all possible components within the GEANT4 program. Then the photon and electron background level in the energy region of interest (<10-2 events·kg-1·day-1·keV-1 (cpkkd)) is predicted based on Monte Carlo simulations. The simulated result is consistent with the design goal of the CDEX-10 experiment, 0.1cpkkd, which shows that the active and passive shield design of CDEX-10 is effective and feasible. 相似文献
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吴昱城 郝喜庆 岳骞 李元景 程建平 康克军 陈云华 李金 李荐民 李玉兰 刘书魁 马豪 任金宝 申满斌 王继敏 吴世勇 薛涛 易难 曾雄辉 曾至 朱忠华 《中国物理 C》2013,(8):51-55
The China JinPing underground Laboratory (CJPL) is the deepest underground laboratory running in the world at present. In such a deep underground laboratory, the cosmic ray flux is a very important and necessary parameter for rare-event experiments. A plastic scintillator telescope system has been set up to measure the cosmic ray flux. The performance of the telescope system has been studied using the cosmic rays on the ground laboratory near the CJPL. Based on the underground experimental data taken from November 2010 to December 2011 in the CJPL, which has an effective live time of 171 days, the cosmic ray muon flux in the CJPL is measured to be (2.0±0.4)×10-10/(cm2 ·s). The ultra-low cosmic ray background guarantees an ideal environment for dark matter experiments at the CJPL. 相似文献
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液相色谱法测定生物发酵液中水溶性维生素的研究 总被引:6,自引:0,他引:6
本文采用反相离子对色谱测定了生物发酵液中的七种水溶性维生素。提出了用自行装填的酸性氧化铝(0.19~0.15mm)前置柱,和5%乙酸洗脱样品的前处理方法;并就有关的色谱条件进行了选择。色谱柱为NovaPakC18;流动相A液为0.05mol/L庚烷磺酸盐(PICB7),冰乙酸调pH=2.5;B液为甲醇+三乙胺(100+0.5);梯度洗脱;UV254nm、290nm、360nm同时测定。线性范围为0.1~10μg,各种维生素的RSD在1.2%~3.0%之间(VitaminB12除外),回收率大于90%。 相似文献
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符长波 陈勋 陈云华 崔祥仪 方德清 Karl Giboni Franco Giuliani 韩柯 季向东 巨永林 刘江来 马余刚 冒亚军 任祥祥 谈安迪 王宏伟 王萌 王秋宏 王思广 吴士勇 肖梦蛟 谢鹏伟 杨勇 张宏光 张涛 赵力 周宁 周小鹏 《原子核物理评论》2017,34(3):290-295
PandaX是位于四川的中国锦屏地下实验室(CJPL)内的,利用氙作为工作物质,探测暗物质等其它极稀有事件的大型地下粒子探测实验计划。PandaX探测器中的氙工作在气液两相的模式。通过检测液相和气相中闪烁光强的比例,实现对目标粒子包括WIMP和Axion等疑似信号的鉴别。PandaX已顺利完成了有效区体积约为120 kg氙的一期计划,目前正在运行实施有效区体积约为500 kg氙的二期计划。在WIMP质量为45 GeV/c2附近,探测灵敏度达2.97×10-45 cm2(90%置信度),没有发现WIMP疑似信号。本工作介绍了PandaX一期和二期的进展,以及后续升级计划,其中包括升级PandaX的时间投影室至4吨,建造用于屏蔽岩石放射性本底的水屏蔽,以及136Xe双贝塔衰变的研究计划等。PandaX is a xenon-based dark matter and other rare events searching project located at China JinPing underground Laboratory (CJPL), Sichuan province, China. Dual phases, liquid and gas phase of xenon are used in the detector. Particles, including Weak Interaction Massive Particles (WIMPs) or axions etc., may induce scintillating signals in both liquid (S1 signal) and gas (S2 signal) phases, and then are identified by analyzing the ratio of S1 and S2. The PandaX had completed its first stage, the 120 kg in fiducial volume, and now is running in its stage Ⅱ with fiducial volume of 500 kg. The running results show that the WIMP-matter cross section detecting sensitivity of about 2.97×10-45 cm2(90% C.L.) has been achieved at a WIMP mass of 44.7 GeV/c2, and no WIMP candidates are identified. The upgrading plan of the PandaX is discussed, which include to build a larger Time project chamber (TPC) of about 4 tons, a water tank for radiation shielding, and the plan of 136Xe double beta decay studies. 相似文献
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Pickering乳液模板法制备Janus粒子 总被引:4,自引:0,他引:4
本文以SiO2粒子稳定的水包油(O/W)型Pickering乳液作为模板, 在乳液连续相进行SI-ATRP, 将聚合物刷接枝到SiO2粒子外半表面, 破乳得到半修饰的Janus粒子. 相似文献
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A Search for Solar Axions and Anomalous Neutrino Magnetic Moment with the Complete Panda X-Ⅱ Data 下载免费PDF全文
周小朋 曾鑫宁 宁旭阳 阿布都沙拉木·阿布都克力木 陈葳 谌勋 陈云华 程晨 崔祥仪 樊英杰 方德清 符长波 付孟婷 耿立升 Karl Giboni 顾琳慧 郭绪元 韩柯 何昶达 黄迪 黄焱 黄彦霖 黄周 季向东 巨永林 李帅杰 刘华萱 刘江来 芦晓盈 马文博 马余刚 冒亚军 孟月 倪恺翔 宁金华 任祥祥 商长松 申国防 司琳 谈安迪 王安庆 王宏伟 王萌 王秋红 王思广 王为 王秀丽 王舟 武蒙蒙 吴世勇 邬维浩 夏经铠 肖梦姣 谢鹏伟 燕斌斌 杨继军 杨勇 喻纯旭 袁鞠敏 袁影 张丹 张涛 赵力 郑其斌 周济芳 周宁 《中国物理快报》2021,(1):30-34
We report a search for new physics signals using the low energy electron recoil events in the complete data set from PandaX-Ⅱ,in light of the recent event excess reported by XENON1 T.The data correspond to a total exposure of 100.7 ton·day with liquid xenon.With robust estimates of the dominant background spectra,we perform sensitive searches on solar axions and neutrinos with enhanced magnetic moment.It is found that the axionelectron coupling gAe<4.6×10-12 for an axion mass less than 0.1 keV/c2 and the neutrino magnetic moment μv<4.9×10-11μB at 90%confidence level.The observed excess from XENON1 T is within our experimental constraints. 相似文献