聚酰胺酸合成工艺研究

 采用超声波在线测量溶液粘度的方法，研究了合成聚酰胺酸过程中实验条件的影响，并对实验结果进行分析，由此确定了合成高分子量聚酰胺酸的最佳实验条件。研究表明：在加料次序为先加二胺后加二酐（二酐与二胺的摩尔比为1.01～1.02：1）、试剂中含水量尽可能少，反应温度0～5℃、反应时间以溶液粘度到达最大值为止的条件下，所合成的聚酰胺酸溶液粘度最大，可满足惯性约束聚变（ICF）充气腔靶端口膜的需要。     

NOVEL FORMATION AND DECAY MECHANISMS OF NANOSTRUCTURES ON THE SURFACE

For decades the research on thin-film growth has attracted considerable attention as these kinds of materials have the potential for a new generation of device application. It is known that the nuclei at the initial stage of the islands are more stable than others and certain atoms are inert while others are active. In this paper, by using kinetic Monte Carlo simulations, we will show that, when a surfactant layer is used to mediate the growth, a counter-intuitive fractal-to-compact island shape transition can be induced by increasing deposition flux or decreasing growth temperature. Specifically, we introduce a reaction-limited aggregation (RLA) theory, where the physical process controlling the island shape transition is the shielding effect of adatoms stuck to the stable islands on the incoming adatoms. Moreover, the origin of a transition from triangular to hexagonal and then to inverted triangular as well as the decay characteristics of three-dimensional islands on the surface and relations of our unique predictions with recent experiments will be discussed. Furthermore, we will present a novel idea to make use of the condensation energy of adatoms to control the island evolution along a special direction.     

信息技术与物理研究性学习

 一、研究性学习概述1.研究性学习的界定研究性学习是指学生在教师指导下,根据学生自己选定的课题,以个人或小组合作的形式,通过研究问题主动获取知识、应用知识、培养能力的一种学习方式。研究性学习是以问题为载体,在教学过程中创设一种类似科学研究的情景和途径,让学生通过自己收集、分析和处理信息来实际感受并体验知识的生产过程和应用过程,使学生通过研究对信息的处理能力、探究能力和实践能力得以提高、发展学生的科学态度和合作精神。2.物理教学中研究性学习的开展研究性学习强调以学生为主,教师只是作为咨询者、指导者和帮助者,学生的具体任务由学生自己完成。     

新型电感储能脉冲功率驱动源

提出了将传统单个储能电感利用传输线分隔成两部分的新型电感储能脉冲功率驱动源技术方案。理论分析表明,利用传输线电容的耦合延时作用,可有效对调制器输出脉冲波形进行整形,并且可以进一步提高能量转换效率,从而克服传统电感储能脉冲功率源输出波形质量差(类三角波波形)的缺点。基于该思想开展了实验研究,获得了电压约300 kV,电流约20 kA的电子束,并成功驱动S波段磁绝缘线振荡器获得了百MW量级的微波输出。     

Effect of Reactor Pressure on Qualities of GaN Layers Grown by Hydride Vapour Phase Epitaxy

The influence of reactor pressure on GaN layers grown by hydride vapour phase epitaxy （HVPE） is investigated. By decreasing the reactor pressure from0. 7 to 0.5 mm, the GaN layer growth mode changes from the island-like one to the step flow. The improvements in structural and optical properties and surface morphology of GaN layers are observed in the step flow growth mode. The results clearly indicate that the reactor pressure, similarly to the growth temperature, is One of the important parameters to influence the qualities of GaN epilayers grown by HVPE, due to the change of growth mode.     

Generation of four-photon W state via cavity QED

This paper proposes an alternative scheme for generating four-photon W state via cavity QED. The scheme bases on the resonant interaction of a A-type three level atom with two bimodal cavities. The detection of atom collapses the cavity to the desired state. Comparing with previous schemes, the advantage of this scheme is that the interaction time can be greatly shortened since it uses the resonant interaction between atom and cavities. Moreover, the proposed scheme is more experimentally feasible than the previous ones.     

Absolute small-angle measurement based on optical feedback interferometry

We present a simple but effective method for small-angle measurement based on optical feedback interferometry （or laser self-mixing interferometry）. The absolute zero angle can be defined at the biggest fringe amplitude point, so this method can also achieve absolute angle measurement. In order to verify the method, we construct an angle measurement system. The Fourier-transform method is used to analysis the interference signal. Rotation angles are experimentally measured with a resolution of 10^-6 rad and a measurement range of approximately from -0.0007 to ＋0.0007 rad.     

A NOVEL ACETYLENIC ESTER-VINYL ETHER REARRANGEMENT

A novel acetylenic ester-vinyl ether rearrrangement takes place when perfluoroacetylenicester is subject to hydrolysis with aqueous sodium hydroxide. The rearrangement is highlystereoselective and the Z-isomer predominates to the extent of above 94% in all cases. Thecrossover experiments showed that this rearrangement proceeds predominately intramolecu-larly. By using ~(18)O labeling technique and on the basis of mass spectral study, it wasshown that the rearrangement most likely roceeds through an intramolecular 1, 3 shiftof the methoxy group to the β-carbon atom. A novel mechanism involving a cage reactionin the organic phase of a two-phase system is proposed.     

改进考試方法,发揮学生在学习上的主动性

(一) 怎样引起改进的我们是根据考试的目的来改进考试方法的。对考试目的的认识,我们是有一个过程的。过去,把考试当作推动学生学习的法宝,认为学生学不好,就要考,把它当成强迫学生学习的一种手段,同时,把考试作为检查学生学习质量的唯一手段,认为考试越突然,就越能看出学生的真正水平。基于这些错误认识,伴随而来的就是考试多,采取突然袭击,其结果造成学生过分紧张与畏惧的情绪,造成精神上的沉重负担,学     

光电直读发射光谱的某些新进展

引言自火焰分析法问世一百多年以来,仪器分析,尤其是原子发射光谱分析(AES),虽然几经波折,但得到了突飞猛进的发展,对促进科学技术的开发,做出了积极的贡献。而科学技术的发展,又推进了发射光谱分析技术的不断创新。实用光谱分析仪器中,在看谱镜、摄谱仪和照相测光方法的基础上,Hasler于