石墨炉原子吸收光谱法测定奶牛血清中硒

本文采用石墨炉原子吸收技术加入基体改进剂直接测定奶牛血清中的痕量元素硒。实验发现使用0.1%Ni(NO3)2作为基体改进剂，可使样品灰化温度提高到1000℃，实际使用灰化温度为600℃经氕灯校正背景，直接测定奶牛血清中的硒含量方法简便省时，回收率在104%-93.3%之间，相对标准偏差为4.9%。     

ORIGIN OF MONOAMINERGIC INNERVATION OF THE NUCLEUS RAPHE MAGNUS——A COMBINED MONOAMINE HISTOCHEMISTRY AND FLUORESCENT RETROGRADE TRACING STUDY IN THE RAT

By the use of the fluorescent retrograde tracer, Fast Blue (FB), in combination with monoamine fluorescence histochemistry, the origin of monoaminergic input to the region of the nucleus raphe magnus (NRM) was investigated in the rat. After mieroinjection of FB into the NRM, a great number of FB-laboled NA-containing cells were found in the region of the nucleus reticularis lateralis (corresponding to A1 NA areas), the reticular formation just dorsolateral to the nucleus olivaris inferior (corresponding to the A3 NA area), the ventral part of the locus coeruleus (A6 NA area), and the lateral parts of the nucleus raphe dorsalis (B7 area). In the other NA cell groups of the brain stem, FB-labeled cells could not be observed. Serotoninergic input originating from nucleus raphe obscurus (B2), nucleus raphe pallidus (B1) and nucleus raphe pontis (BS-B6) to the NRM was also observed. A large number of cells containing serotonin (5-HT) in the B2 and B6 areas were labeled by FB, while only a few FB-labeled 5-HT     

手征σ模型中σ介子的质量与核物质结合能曲线关系的研究

文中研究了手征σ模型下σ介子的质量m_σ与核物质结合能曲线的关系,主要的目的是研究在单圈图近似下所谓的“快子极点”问题,即σ或π介子质量的平方变为负数,这将导致能量密度为虚数.把m_σ看成自由参数并通过拟合核物质的饱和性质而确定,结果表明,在单圈图真空起伏近似下,并选重整化点在质量壳上,当m_σ=307.5MeV而且核密度小于4.43倍正常饱和密度时,“快子极点”没有出现,因此首先得到了核物质结合能曲线以及计算了不可压缩系数K(≌175.7MeV).     

DNTF的合成与表征

3，4-二（硝基呋咱基）氧化呋咱（DNTF）是一新型高能量密度化合物，其感度较HMX的低，能量较HMX的高，与CL-20的相当。文中对DNTF及其中间体3-氨基-4-酰胺肟基呋咱（AAOF），3-氨基-4-酰氯肟基呋咱（ACOF），3，4-二（氨基呋咱基）氧化呋咱（DATF）及其异构体3，6-二（3＇-氨基呋咱基-4-基）-1，4-二氧杂-2，5-二氮杂环己-2，5-二烯（BADDD）的合成，表征和主要的物化和炸药性能进行了报道。     

Two-electron and one-photon transitions in highly charged nickel-like ions

This paper calculates the transition wavelengths and probabilities of the two-electron and one-photon (TEOP) transition from the $(3{\rm s}^{-1}_{1/2}4{\rm d}_{j})_{J=1,2}$ to $(3{\rm p}^{-1}_{3/2}4{\rm s}_{1/2})_{J=1}$ and the $(3{\rm p}^{-1}_{1/2}4{\rm s}_{1/2})_{J=1}$ to $(3{\rm d}^{-1}_{j}4{\rm d}_{j'})_{J=1,2}$ for highly charged Ni-like ions with atomic number $Z$ in the range $47\leq Z\leq92$. In the calculations, the multi-configuration Dirac--Fock method and corresponding program packages GRASP92 and REOS99 were used, and the relativistic effects, correlation effects and relaxation effects were considered systematically. It is found that the TEOP transitions are very sensitive to the correlation of electrons, and the probabilities will be enhanced sharply in some special $Z$ regions along the isoelectronic sequence. The present TEOP transition wavelengths are compared with the available data from some previous publications, good agreement is obtained.     

级联双折射光纤环镜滤波特性的分析

从理论上研究了级联双折射光纤环镜滤波器的滤波特性，给出加隔离器与不加隔离器两种不同结构的串联双环镜滤波器透射光强的表达式，并对于两个环镜取不同的周期比时的滤波特性进行了数值模拟和分析.得出串联环镜滤波效果与级联顺序无关，光隔离器对滤波效果不会产生影响，只是增加了插入损耗.通过级联和改变两个环镜的双折射光纤长度比，可以获得不同的滤波效果.最后给出了多个环镜直接级联后透射光强的通项表达式，通过对通项式的理论分析可以设计不同的滤波器.     

Yb:Y2O3透明陶瓷的光学性能研究

介绍了一种基于纳米粉末真空烧结技术的新型固体激光材料--Yb:Y2O3多晶陶瓷的制备工艺、物理化学特性、能级结构和光谱特性,并与Yb:YAG单晶进行了对比.采用紧凑型有源镜激光器(CAMIL)的抽运方式,验证了Yb:Y2O3透明陶瓷的激光输出性能.在35W的最大抽运功率下,得到波长1078 nm,功率10.5 W的连续激光输出.斜率效率达到37.5%.实验中还观察到激光输出波长随抽运功率增加而红移以及随输出耦合镜变化而漂移的现象.Yb:Y2O3多晶陶瓷是一种理想的激光材料,不仅具有与Yb:YAG单晶同样优秀的物理化学性能和光谱特性,而且其热导率和发射带宽约为Yb:YAG单晶的两倍,非常适合于高亮度激光器和超短脉冲激光器领域的发展应用.     

Fabrication of Two-Dimensional Photonic Crystals with Controlled Defects by Combination of Holographic Lithography and Two-Photon Polymerization

A new ternary photopolymer system is used in fabricating photonic crystals （PhCs） with controlled defects by combination of single-photon and two-photon photopolymerization. The former process can produce PhCs in one-step recording with a low-power （tens mW） continuous-wave laser at 532nm, while the latter can create desired defects. The preparation of the material, the optical setup and the preliminary experimental results are given. Compared with other methods, this approach is much more accessible and convenient for use of visible light and has advantages of making PhCs in a large scale quickly and economicaJly and introducing any defects exactly, especially for three-dimensional structures.     

Mn掺杂ZnSe前驱体纳米带的制备及其磁光性质

采用了改进的水热途径制备稀磁半导体Mn掺杂ZnSe前驱体纳米带MnxZn1-xSe?en3 (en=ethylenediamine). 与先前方法相比， 具有省时高效的优势. 并通过电子能谱仪、热重分析仪、场发射扫描电子显微镜表征这种前聚体的形态与组成. 在有关电子顺磁共振波谱(ESR)和发光光谱(PL)的实验中，ESR和PL用来研究和表征Mn2+掺杂效率及ZnSe前驱体纳米带中Mn2+-Mn2+的相互作用.Mn掺杂ZnSe前驱体纳米带的ESR谱出现Mn2+特征超精细分裂六重峰，表明了Mn2+-Mn2+的