Effects of a carbon convection field on large diamond growth under high-pressure high-temperature conditions

Large diamond crystals were successfully synthesized by a FeNi-C system using the temperature gradient method under high-pressure high-temperature conditions. The assembly of the growth cell was improved and the growth process of diamond was investigated. Effects of the symmetry of the carbon convection field around the growing diamond crystal were investigated systematically by adjusting the position of the seed crystal in the melted catalyst/solvent. The results indicate that the morphologies and metal inclusion distributions of the synthetic diamond crystals vary obviously in both symmetric and non-symmetric carbon convection fields with temperature. Moreover, the finite element method was applied to analyze the carbon convection mode of the melted catalyst/solvent around the diamond crystal. This work is helpful for understanding the growth mechanism of diamond.     

Thermal expansion properties of Lu2-xFexMo3O12

The structures and thermal expansion properties of Lu2-xFexMo3O12 have been investigated by X-ray diffraction(XRD).XRD patterns at room temperature indicate that compounds Lu2-xFexMo3O12 with x≤1.3 exhibit an orthorhombic structure with space group Pnca;compounds with x=1.5 and 1.7 have a monoclinic structure with space group P21/a.Studies on thermal expansion properties show that the linear thermal expansion coefficients of orthorhombic phase vary from negative to positive with increasing Fe content.Attempts to make zero thermal expansion materials indicate that zero thermal expansion can be observed in Lu1.3Fe0.7Mo3O12 in the temperature range of 200-400℃.     

α,α'-二氧代烯酮环二硫代缩醛的NMR研究

报道了7种新的α,α'-二氧代烯酮环二硫代缩醛化合物的NMR谱.应用¹H、¹³C NMR谱等确定了这7种新化合物的分子结构,并对全部谱峰进行了归属,初步探讨了分子结构对化学位移的影响.     

生物小分子与铜锌超氧化物歧化酶相互作用的波谱学研究及其应用

本工作以ESR和NMR为主要手段,并结合其它生化方法,考察了氨基酸、核酸碱基、糖等生命基本物质,和抗坏血酸等生命必需物质与钢锌超氧化物歧化酶的相互作用,实验观测到氨基酸、核酸碱基和抗坏血酸在水溶液中可以与酶中的Cu²⁺作用而使其脱离活性部位,以小分子络合物形式游离在溶液中,同时使酶失活,脱离活性部位的Cu²⁺的比例和酶的失活程度取决于小分子配体的加入量及其与Cu²⁺的络合能力。此外,首次尝试使用ESR方法,并借助氨基酸与酶的作用,考察了铜锌超氧化物歧化酶在盐酸胍变性和热变性过程中的构象变化行为,结果表明这一方法是直观而有效的。     

红外成象分离双透镜系统设计

本文介绍红外成象大孔径、大视场物镜的设计原理及象质评价方法,导出了求解初始结构参数的象差方程,给出了设计实例及象质评价结果。     

大学物理实验教学创新模式的探索与实践

通过认真学习《非物理类理工科大学物理实验教学基本要求》,提出一种大学物理实验课程的创新性补充模式,该模式在本校学生中付诸实践,取得了较好的效果.     

Application of high-precision temperature-controlled FBG filter and light source self-calibration technique in the BOTDR sensor system

A high-precision temperature-controlled narrow band-stop fiber Bragg grating(FBG) filter and light source self-calibration technique are proposed for application in the Brillouin optical time domain reflectometer (BOTDR) sensor system.With the proposed application,the BOTDR sensor system maintains good long-term stability and temperature precision through the reduction of the center wavelength drift in the FBG filters and corresponding decrease in the changes in light intensity.The experiment result shows that temperature precision of 1℃and temperature stability of 0.7℃can be achieved in a temperature sensor over a range of 8 km.     

食品微生物对超高压处理的逆境响应

 超高压（High Hydrostatic Pressure,HHP）作为一种非热杀菌技术,在食品工业中有着很广泛的应用,与传统的热加工处理相比,在保持食品品质、杀菌、钝酶等方面都有其明显的优势。通过对国内外相关文献的分析,对HHP处理后处于亚致死状态食品微生物的细胞膜、遗传与结构物质、机体代谢等方面,以及大部分食品微生物在应对外界的多种刺激时而进行的普遍性调控机制的研究进行了总结,探讨了经过HHP处理后处于亚致死状态的食品微生物在逆境下存活的应激反应。     

水下激光探测系统的水体后向散射光计算与光学参数估计

针对水下激光探测系统的水体后向散射光的计算,给出了系统的光学几何结构,分析了不同距离处的激光光斑与接收视场区域的位置变化关系并进行了定量计算。依据光传输理论建立了水体后向散射光的计算模型,根据模型的算法步骤编写了计算机程序。结合水下激光探测系统的具体参数进行了实例计算,绘制了后向散射光信号波形,并与试验获取的信号波形对比分析,验证了算法的可行性和正确性。研究了使用实测后向散射光信号数据估计水体光学特性参数的方法,通过估算的参数重新绘制曲线并反向叠加在测量数据曲线上以抵消水体后向散射光对目标信号的影响从而能够提取目标信息。     

Quantum correlations between two non-interacting atoms under the influence of a thermal environment

By considering a double Jaynes-Cummings model,we investigate the dynamics of quantum correlations,such as the quantum discord and the entanglement,for two atoms in their respective noisy environments,and study the effect of the purity and the cavity temperature on the quantum correlations.The results show that the entanglement suffers sudden death and revival,however the quantum discord can still reveal the quantum correlations between the two atoms in the region where the entanglement is zero.Moreover,when the temperature of each cavity is high the entanglement dies out in a short time,but the quantum discord still survives for quite a long time.It means that the quantum discord is more resistant to environmental disturbance than the entanglement at higher temperatures.