柱塞泵油膜压力分析的高效有限单元法

The paper concerns numerical analysis of pressure distribution of an oil film on the valve plate in the variable height gap of an axial piston pump. The analysis employs the finite element method. For determination of oil pressure variations in the gap, the Reynolds equation, commonly applied in the theory of lubrication, is applied. The equation is solved numerically with the use of self-developed program based on the finite element method. In order to obtain high accuracy of the results, an adaptive mesh refinement based on residual estimations of solution errors is applied. The calculation results are represented as dependent on the geometric and working parameters of the pump.     

A STUDY ON COSMOGENIC NUCLIDES IN JILIN METEORITE AND ITS TWO-STAGE IRRADIATION HISTORY

Forty-four burk samples of the H chondrite Jilin have been analysed for their contents ofspallogenic, trapped and radiogenic noble gases, and thirty-five samples have been determinedfor their radiocosmogenic nuclides. The Jilin meteorite has an extreme complicated history ofcosmic-ray irradiation. In the 1st-stage, the Jilin meteorite might be located between 0.2--2mbelow the surface of the parent body travelling about 8 m. y. in space and under a geometryof 2π subjected to the radiation of cosmic-ray. According to the data of ~(60)Co dating the burialdepth of all samples in the 2nd-stage can be determined and the preatmospheric form andsize of the parent body can be restored (under a geometry of 4π). The result of this recon-struction is that, the 2nd-stage has a nearly spheric form, with a radius of 85±5 cm, weighing9.7±1.7 Ts. The position of the center of the preatmospheric body is: X=55, Y=55 andZ=39. Jilin meteorite No.1 is located at the center of the parent body and is surroundedwith the fragments. The ablation rate is estimated at about 30%. We have proposed a new modelof the two-stage irradiation, and based on the contents of ~(21)Ne-~(60)Co in the samples, a classificationscheme can be worked out for the restoration of relative position of the samples within theparent body.     

235,238U核数据的快中子基准实验积分检验

用四个快中子基准实验检验了ＥＮＤＦ／Ｂ－ＶＩ、ＪＥＮＤＬ－３和ＣＥＮＤＬ－２三个评价核数据库中的２３５Ｕ和２３８Ｕ等数据．计算结果指出，ＥＮＤＦ／Ｂ－ＶＩ库的数据对快中子积分实验的预言更准确． Four fast benchmark experiments have been used to the data of 235,238U in testEndf/B-VI,JENDL-3 and CENDL-2 nuclear date libraries...     

流动相组成对有机硒手性化合物拆分的影响

 在自制的涂敷型纤维素 三 (3,5 二甲基苯基氨基甲酸酯 ) (CDMPC)手性固定相上拆分了一些结构相似的有机硒手性化合物 ,详细考察了三元流动相对手性拆分的影响 ,并探讨了溶质分子与手性固定相相互作用的模式。实验结果表明 :在二元流动相中加入极少量的质子性改性剂 (醇 )或非质子性改性剂 (乙腈 ) ,可使溶质的保留和手性拆分发生较大的变化。     

氧化镍在倒置平面钙钛矿太阳能电池中的应用进展

近年来有机-无机杂化钙钛矿太阳能电池(perovskite solar cells,PSCs)因具有光电转换效率高、制备工艺简单等优点而受到广泛关注.空穴传输层(hole transport layer,HTL)的选择及其优化对器件的性能至关重要.氧化镍(NiOx)HTL具有化学稳定性好、空穴迁移率高、制备方法简单等特...     

营养不良婴幼儿红细胞内外锌、铜、钙、镁变化及其意义

对１８例营养不良婴幼儿血浆及红细胞内的锌,铜,钙,镁元素含量进行了测定,并与１５例健康婴幼儿进行对照。结果表明,营养不良患儿血浆中锌,钙降低,与健康组相比有显著性差异（Ｐ〈０．０１）;营养不良患儿红细胞内锌,镁降低,钙升高,与健康组相比均有显著性差异（Ｐ〈０．０１）。因此,营养不良婴幼儿红细胞内外锌,钙,镁的变化应引起重视。     

1 kHz single-frequency,injection-seeded Er:YAG laser with an optical feedback

A novel 1 kHz single-frequency, Q-switched Er-doped yttrium aluminum garnet(Er:YAG) laser pumped by a 1470 nm laser diode is demonstrated. The 500 ns, 5.52 mJ single-frequency, diffraction-limited pulses are obtained by using a ‘ramp-fire' injection-seeding technique and an optical feedback architecture. The full width at half-maximum of the pulse spectrum is measured to be 1.47 MHz by using the heterodyne technique. The beam quality M2 factors are measured to be 1.18 and 1.24 in the x and y directions, respectively.     

四种Keggin型多酸纳米材料的制备及其吸附有机染料的性能

以4种Keggin型多酸作为原料(分别为H₃PW₁₂O₄₀·36H₂O(简写为PW₁₂^a)、H₃PMo₁₂O₄₀·34H₂O(简写为PMo₁₂^a)、H₄SiW₁₂O₄₀·35H₂O(简写为SiW₁₂^a)和H₄GeW₁₂O₄₀·40H₂O(简写为GeW₁₂^a)),采用表面活性剂智能化控制的软化学法制备了相应的4种Keggin型多酸纳米材料,分别为Ag₃PW₁₂O₄₀·36H₂O(简写为PW₁₂^b)、Ag₃PMo₁₂O₄₀·34H₂O(简写为PMo₁₂^b)、Ag₄SiW₁₂O₄₀·35H₂O(简写为SiW₁₂^b)和Ag₄GeW₁₂O₄₀·40H₂O(简写为GeW₁₂^b)。采用IR、UV-Vis、XRD和SEM表征多酸的结构和纳米粒子的形貌。在室内黑暗条件下,100mg样品可在5min内把20mg·L^-1的100mL亚甲基蓝(MB)染料溶液脱色,使其变为接近无色,吸附效率最高可达96.3%,吸附效率大小为PMo₁₂^b >PW₁₂^b >GeW₁₂^b >SiW₁₂^b。相同条件下,100mg样品使20mg·L^-1的100mL罗丹明B(RhB)染料溶液30min内脱色完全,脱色效率最高可达96.1%,吸附效率大小为PW₁₂^b >PMo₁₂^b >SiW₁₂^b >GeW₁₂^b。说明该4种多酸纳米材料具有较高的吸附有机染料性能。     

金属-有机纳米管

金属-有机纳米管(metal-organic nanotubes,MONTs)是由无机金属离子和有机配体通过自组装方法构筑的具有纳米级隧道的框架结构,由于其管状结构独特的内部孔径、多样的拓扑结构及其在诸多领域的多重应用,越来越受到关注,是无机化学和配位化学等领域研究中的一个热点。本文评述了金属-有机纳米管的存在形式和构建策略,包括杯芳烃及环糊精类配体构筑MONTs、常规吡啶氮类配体或芳香羧酸配体构筑MONTs和混合配体策略构筑MONTs,着重介绍了近年来国内外金属-有机纳米管研究领域的最新成果和进展,并指出了金属-有机纳米管领域今后的研究方向。     

矩形截面超导线圈的径高比对最大磁场点位置和幅值的影响分析

为了充分利用超导线材的载流能力,需要精确计算超导线圈产生的最大磁场值,还需要明确最大磁场值所处的具体位置.其中,最大磁场点的位置主要由线圈的形状(径高比)决定.本文基于单积分法并通过MATLAB编程,将矩形截面线圈的径高比α和β参数化,计算分析线圈内壁边上和端面边上各点磁场的变化趋势.同时,利用电磁场有限元软件ANSYS,对矩形截面线圈的空间磁场进行仿真分析,得到线圈的内壁磁场系数、端面磁场系数和最大磁场系数随α和β的变化规律;进而,计算并寻找到了线圈截面上最大磁场点的位置和幅值.综合分析表明,线圈内壁边上的最大磁场点并不是始终位于内壁中点B_c处,而是可能偏离端点B_e一小段距离的某点(a₁,b-δ)处;线圈端面边上的最大磁场点一定不位于端点B_e处,而是偏离端点B_e一小段距离的某点(a₁+δ,b)处.本文给出了线圈截面上最大磁场系数K_mc对应于线圈径高比(α,β)变化的等高曲线,矩形截面超导线圈最大磁场值可以通过计算内壁中点的磁场值与最...