Study on hydrogen sulfide 790-nm laser diode plasma passivation of cavity surface

In order to improve the optical properties of the Ⅲ-Ⅴ laser diodes （LDs） by means of H2S plasma passivation technology, H2S plasma passivation treatment is performed on the GaAs（110） surface. The optimum passivation conditions obtained are 60-W radio frequency （RF） power and 20-min duration. So the laser cavity surfaces are treated under the optimum passivation conditions. Consequently, compared with unpassivated lasers with only AR/HR-eoatings, the catastrophic optical damage （COD） threshold value of the passivated lasers by H2S plasma treatment is increased by 33%, which is almost the same as that of （NH4）2Sx treatment. And the life-test experiment has demonstrated that this passivation method is more stable than （NH4）2Sx solution wet-passivated treatment.     

低成本硫化物固态电解质Li6-xPS5-xClx的制备与性能研究

硫化物固体电解质以其室温电导率高,热稳定性好,电化学窗口宽等特点,在高功率及室温固态电池方面优势突出,是极具潜力的固态电解质材料. 但制备其所需的高纯度Li₂S原料高昂的价格使其实际应用受到掣肘,故本文使用单质锂金属（99.9%）、升华硫、氯化锂和五硫化二磷等低成本原料,采用球磨法和高温热处理制备得到了Li_6-xPS_5-xCl_x（x = 0.5）固态电解质粉末,通过X射线衍射（XRD）、拉曼（Raman）、扫描电子显微镜（SEM）及能谱仪（EDS）对Li_6-xPS_5-xCl_x（x = 0.5）固态电解质进行了表征,并使用交流阻抗法测试了其电导率,电导率可达8.29×10 ^-4 S·cm ^-1,将Li_6-xPS_5-xCl_x（x = 0.5）固态电解质粉末进行冷压制片,制成Li对Li半电池后显示了良好的循环性能.     

基于BP网络和专家系统的铝电解槽分层故障诊断

针对铝电解槽故障种类繁多和不易诊断的问题,设计了基于BP网络和专家系统的分层故障诊断系统,包括前层分类和后层预报;通过对槽电阻信号的频谱分析,提取了故障特征信息,并对故障进行分类;建立了基于BP网络的前层分类器,用于诊断特征显著的故障;制定了故障诊断和控制规则,完善了专家系统的知识库,根据前层分类结果对余下故障进行诊断;通过制定规则,将前层分类和后层预报相结合,实现了故障诊断系统的整体设计;仿真结果及理论分析表明,该系统可有效预报单一及复合故障,提高故障诊断的准确率,保证铝电解槽工作状况的稳定。     

大型望远镜交流伺服控制系统综述

本文主要介绍了当前国际上地基大口径望远镜交流伺服控制系统的发展现状,详细论述了望远镜驱动方式的选择、交流永磁同步力矩电机的应用情况、控制系统的硬件组成以及伺服系统的控制策略。讨论了大型望远镜交流伺服控制系统设计的难点及未来发展趋势,为大型望远镜交流伺服控制系统的设计提供一定的参考。     

成都市学龄前儿童末梢血微量元素检测结果的分析

为探讨成都市学龄前儿童末梢血微量元素的缺乏现状及其含量与年龄和性别的关系,利用BH 5100型原子吸收光谱仪对23 932例学龄前儿童末梢血中铜、锌、钙、镁和铁元素进行了检测,用SPSS 16.0做了统计分析.结果表明,所测学龄前儿童末梢血铁、锌元素缺乏严重;铜、锌、钙和铁元素含量在年龄上呈现一定变化规律,铜元素在男女...     

Dark Sharma-Tasso-Olver Equations and Their Recursion Operators

A complete scalar classification for dark Sharma-Tasso-Olver's(STO's) equations is derived by requiring the existence of higher order differential polynomial symmetries. There are some free parameters for every class of dark STO systems, thus some special equations including symmetry equation and dual symmetry equation are obtained by selecting a free parameter. Furthermore, the recursion operators of STO equation and dark STO systems are constructed by a direct assumption method.     

应用零价铁基材料还原和催化氧化降解多溴联苯醚

多溴联苯醚（PBDEs）是一类新型的持久性有机污染物（POPs）,由于不合理的使用和处置,在多种环境介质中均存在不同程度的污染。环境中PBDEs的降解技术已成为近年来的研究热点。大量的研究表明,零价铁（ZVI）还原脱溴降解PBDEs是一种高效快速且经济可行的治理技术。本文在总结国内外关于ZVI基材料降解PBDEs研究的基础上,分析了ZVI还原降解PBDEs的机理、动力学、影响因素及降解路径。从总体上看,ZVI作为高活性电子供体虽然能将高溴代PBDEs迅速降解为低溴代产物,但产生的低溴代PBDEs往往具有更大的环境风险,需进一步降解处理。近年来的研究表明,利用ZVI作为间接电子供体,通过催化活化H₂O₂或过硫酸盐产生高活性自由基,能够实现开环降解低溴代PBDEs。基于以上分析,通过构建一套先还原-后氧化的降解体系,有望实现高溴代PBDEs的彻底降解。最后,本文对ZVI降解PBDEs技术的后续研究进行了讨论和展望。     

基于多元统计分析的稚儿灵颗粒质量等级评价

建立稚儿灵颗粒的质量等级评价方法。收集市场上4个厂家共24批次稚儿灵颗粒样品,采用中华人民共和国卫生部标准WS₃-B-0856—1991和探索性研究相结合的方法,对鉴别、检查、指纹图谱、多组分含量测定结果进行研究,综合各项指标,通过方差分析、聚类分析和主成分分析等多种统计分析,筛选分级指标进行稚儿灵颗粒等级划分研究。建立主成分分析模型,并与商品信息中的等级进行对比,确定等级划分模式。初步建立稚儿灵颗粒的质量等级评价模式,制定了稚儿灵颗粒一级、二级质量等级标准。所建立的等级划分标准可用于综合评价稚儿灵颗粒制剂质量。     

Advances in chromatographic analysis of ginsenosidesEI北大核心CSCD

Ginsenosides possess pharmacological activities such as anti-aging，cardiovascular protection，and improving immunity. However，the detection and analysis of ginsenosides commonly suffer from the problem of low sensitivity owing to the complex matrix and low content of ginsenosides. Chromatographic technology was often used to detect ginsenosides owing to the advantages of high accuracy，high sensitivity，good reproducibility and low sample consumption，etc. In this review，the application of chromatographic analysis technologies in ginsenosides detection was summarized. First of all，accuracy of test results for the ginsenosides can be effectively improved by using high performance liquid chromatography（HPLC）combined with various detectors. Secondly，the combination of HPLC with mass spectrometry can be utilized for qualitative and quantitative analysis of ginsenosides， as well as other fields， such as metabonomics， pharmacokinetics， intestinal microorganisms and quality control. Moreover，the application of gas chromatography in analysis of ginsenosides was reviewed. Briefly，with the continuous development of chromatographic technology，the degree of accuracy for ginsenosides detection was effectively improved，which is beneficial to realize the effective analysis of ginsenosides. © 2023, Youke Publishing Co., Ltd. All rights reserved.