循环流化床膜式壁传热试验与模型

本文研究循环流化中膜式壁的传热规律．采用电加热膜式壁传热测量元件试验研究了固体颗粒悬浮密度，膜式壁传热测板长度和空截面流化气速对传热系数的影响．对颗粒团壁面更新传热模型中的重要参数颗粒团壁面覆盖率进行探讨，提出适宜于循环流化床密相区和稀相区中的K、Y值．     

Phase Space Prediction Model Based on the Chaotic Attractor

A new prediction technique is proposed for chaotic time series.The usefulness of the technique is that it removes some false neighbouring points which are not suitable for the local estimation of the dynamics systems.We use a feedforward neural network to approximate the local dominant Lyapunov exponent,and choose the neighbouring points by the exponent.The model is tested for the convection amplitude of the Lorenz model,and the results indicate that this prediction technique can improve the prediction of chaotic time series.     

~(55)Mn(α,n)~(58m,g)Co,~(55)Mn(α,2n)~(57)Co和~(55)Mn(α,α′n)~(54)Mn反应的激发函数

用活化法和迭靶技术,在入射α粒子能量从10.4到26.5MeV范围内,测量了~(55)Mn(α,n)~(58m,g)Co、~(55)Mn(α,2n)~(57)Co和~(55)Mn(α,α′n)~(54)Mn反应的截面,并同激子模型理论计算作了比较,结果表明在上述反应中存在平衡前发射反应机制。     

新型可聚合蒽醌染料单体及其共聚物乳液的制备及性能

通过多步有机反应合成了新型蒽醌染料单体1-(间(2-(2-(丙烯酰氧基)乙氧基)乙基砜基)苯胺基)蒽醌(AVSAQ),对其化学结构进行了表征;然后将其与苯乙烯(St)、丙烯酸丁酯(BA)和甲基丙烯酸(MAA)进行半连续乳液共聚合,制备出了共价键合型P(St-BA-MAA-AVSAQ)橙红色聚合物乳液,并对乳液以及乳胶膜的性能进行了表征,系统考察了AVSAQ和过硫酸铵(APS)用量对单体总转化率以及乳液胶体性质的影响.结果表明,当AVSAQ用量不高于单体总量的4.0 wt%、APS用量不低于单体总量的0.5 wt%时,聚合反应可以平稳进行,所得乳胶粒水合粒径均在60 nm左右.总单体转化率和AVSAQ转化率随着AVSAQ用量的增加而降低,当AVSAQ用量达到4.0 wt%时,二者分别为95.0%和93.6%.P(St-BA-MAA-AVSAQ)的UV-Vis吸收光谱特性与AVSAQ完全一致,最大吸收波长均为486.8 nm.与相应非共价键合型橙红色聚合物乳液相比,P(StBA-MAA-AVSAQ)聚合物乳液具有良好的储存稳定性和保色性,乳胶膜的光色牢度和耐溶剂牢度也显著提高.     

Relativity Between Extrication Wave of Mental Load (EML) and Emot''''on

This experiment which was divided into three items studied the relativity between normal human emotion and extrication wave of mental load (EML) in a paradigm of combining CNV feedback with EML. Fourteen young persons were taken as subjects. After Fz, Cz, Pz, P_3—T_5 and P_4—T_6 were recorded, shorter EML latency and higher EML amplitude were caused by positive emotion in comparison with those caused by negative emotion. EML changes of the five recorded points were consistent under the effects of positive and negative emotions. This experiment also discussed the question of EML brain sources. Under the emotional conditions provided in the present experiment, EML possibly can be regarded as ERP index reflecting its positive and negative attributes.     

基于双吡啶脲类Cd(Ⅱ)、Zn(Ⅱ)、Hg(Ⅱ)配合物的合成及晶体结构

间苯二胺和3-吡啶异氰酸酯在甲苯中加热回流得到双吡啶脲类配体L,然后将配体分别与CdSO_4·8H_2O,ZnI_2,HgI_2,HgCl_2进行配位反应,得到4个配合物{[Cd(L)(SO_4)(H_2O)_3]·H_2O}n(1),{[Zn(L)I_2]·2C_2H_5OH}n(2),{[Hg(L)I_2]·C_2H_5OH}n(3),[Hg(L)Cl_2]·H_2O(4),并用元素分析、FT-IR、X射线单晶衍射、粉末衍射对其进行了表征。配合物1形成一维螺旋链结构,配合物2和3形成一维"之"字链结构,配合物4形成32元环状结构。