Ag2S纳米粒子原位合成以增强PAI涂层机械和摩擦学性能

借助单源前驱体热分解在聚酰胺酰亚胺(PAI)涂层中原位合成了硫化银(Ag₂S)纳米粒子,并通过调节单源前驱体的含量进一步调控纳米粒子尺寸. 采用X射线衍射仪和高分辨场发射扫描电镜对原位合成Ag₂S纳米粒子的物相结构、形貌、尺寸和尺寸分布进行了表征和分析;详细研究了Ag₂S纳米粒子对PAI涂层机械性能和摩擦学性能的影响;对其增强机制进行了探讨. 结果表明:PAI涂层中原位合成的Ag₂S纳米粒子粒径较小而且分散均匀,且调节单源前驱体能有效调控Ag₂S纳米粒子的尺寸和尺寸分布. Ag₂S纳米粒子的原位引入(优化质量分数为5.0%)有效改善了PAI涂层的机械性能和摩擦学性能,其摩擦学性能的增强归因于机械强度的提高和诱导转移膜的形成.      

有机共沉淀-火焰原子吸收光谱法测定水样及奶茶粉中的微量铅

研究了用4-(2-吡啶偶氮)-间苯二酚(PAR)为沉淀剂,以Fe(Ⅲ)为载体离子的共沉淀体系快速共沉淀分离富集水样和奶茶粉中的铅,并用火焰原子吸收光谱(FAAS)方法测定。共沉淀过程受体系酸度、载体铁、沉淀剂PAR的用量及陈化时间的影响。结果显示,在pH为6.0的条件下,能够定量共沉淀试样中的铅。方法检出限为18.7μg.L-1,用于水样及奶茶粉的加标回收率为94.2%～98.3%,相对标准偏差为1.03%～2.24%,排除了基体干扰,结果较为满意。本法与传统的共沉淀方法比较,具有快速、简便、重现性好的优点。     

胶片判读数据的滤波平滑处理

胶片判读后的原始测量数据包含着一定的高频无序随机误差,仅仅用加权平滑及差商法对数据加工计算,势必严重影响运动分析可靠性。本文将讨论数据滤波平滑的必要性,介绍在胶片判读处理中几种行之有效的数据滤波平滑方法。它们是:最小二乘曲线拟     

Orientation distribution of fibres in a channel flow of fibre suspension

The orientation and concentration distributions of fibres in laminar and turbulent channel flows are investigated numerically. The obtained results are in good agreement with the experimental data. In the laminar flow regime, more fibres orient to the flow direction as the Reynolds number increases. The shear rate of fluid around a fibre plays an important role in determining the orientation distribution of fibres, while the fibre density and the fibre aspect-ratio have marginal influence on the orientation distribution. In the turbulent regime, the orientation distribution of fibres becomes more homogeneous with the increase of Reynolds number, and the concentration profile is flatter than that in the laminar regime. The fluctuating intensity of fibre velocity in the downstream direction is larger than that in the lateral directions.     

高压直流远距离输电

 现代远距离输电工程中并存着高压交流输电和高压直流输电两种方式。现行高中物理第二册第111页指出:“实际(交流)输电线路中,导线的电感和电容的影响也会引起很大的电压损失。要彻底解决这个问题就要用直流高压输电”。     

一类基于变量分离的稳定化混合有限元方法

Based on a seperated model for saddle-point problems, we develop a new sta-bilized mixed finite element method. Such a model consists of two subproblems with respect to the primal and the dual variables, respectively. We show that the new method is coercive and that optimal error bounds hold. As an application,the nearly incompressible elastic problem is analyzed with our method.     

Large Enhancement of Optical Nonlinearities of New Organophosphorus Fullerene Derivative

Optical nonlinearities of new organophosphorus fullerene derivative were determined by the Z-scan method with a pulsed Q-switch Nd:YAG laser at 532nm. The experimental results demonstrated that the derivative has much larger excited-states nonlinear absorption and nonlinear refraction than C60. A five-level model was utilized to fit the experimental data, and a good agreement is reached. Some parameters such as excited-state absorption cross and refraction cross were obtained. To our knowledge, the excited-state cross section of new organophosphorus fullerene derivative and its effective ratio to the ground-state cross section are the largest values among the fullerene derivatives reported to date.     

激光增强极化^129Xe和^3He的磁共振成像

当激光增强极化的＾１２９Ｘｅ或者＾３Ｈｅ被输送到一些感兴趣的生物体内组织中（例如：人或者动物的肺部），由于它们具有高的自旋密度对比度，可以给出大的核磁共振信号强度、高的成像空间分辨和数据率，有希望应用于质子成像不能达到的一些有意义的生物组织的成像。该文简述了激光增强极化＾１２９Ｘｅ和＾３Ｈｅ样品的制备、储存、输送方法和成像应用，以及相应过程中的物理量。     

Batrachion序列的数值求解

Batrachion序列是一类奇特的序列，有着非常的分形图形行为和轨迹，已引起计算机图形领域许多学者的兴趣和重视．本文给出Batrachion序列的完整求解，并且予以严格的证明．在证明过程中，同时显示了它与杨晖三角形密切的关系．