溶胶-凝胶法制备金属铂高分散的二氧化钛薄膜

Uniform and crack free TiO 2 thin films with highly dispersed platinum were prepared from i PrOH TTIP DEA H 2O system containing H 2PtCl 6·6H 2O as metal source by sol gel method. The microstructure and morphology of the films were characterized by TEM and XRD respectively. It was found that the Pt particles dispersed in the films and had a homogeneous distribution in the shape of sphere with an average size of about 5 nm. This study also showed that the doping with few percent of Pt resulted in the formation of pure rutile phase at a temperature as low as 550 ℃, whereas the same pure phase was formed at the temperature higher than 650 ℃ in TiO 2 or Au/TiO 2 thin films.     

A CLASS OF QUADRATIC HAMILTONIAN SYSTEMS UNDER QUADRATIC PERTURBATION

1 IntroductionConsider a Hamiltonian system with small perturbationwhere E is a small parameter. H(x, y), P(x, y) and Q(x, y) are all real polynimials of x and ywith degH = n 1, degP degQ 5 n. We suppose there is a fandly of ovals r(h) C {H(x, y) = h}for h E (ho, h1).The nunther of limit cycles of (1.1). l which tend to some r(h) as e -- 0, is closely relatedto the number of isolated zeroes of Abelian integraJThe next problem is to determille the lowest bound of the isolated zeroes of M…     

TiCl4水解法制备TiO2薄膜的表征及光催化性能

TiCl4水解法制备TiO2薄膜的表征及光催化性能;TiCl4水解;TiO2薄膜;光催化;乙酸     

单个、自生的RP-Au-PR结构增强金属纳米团簇的光致发光量子产率19倍

膦保护金纳米团簇的研究可追溯到1969年,"RP-Au-PR"(R为烷基)结构在膦保护的金纳米团簇上目前还未见报道,而相似的"RS-Au-SR"结构在硫醇保护金纳米团簇中经常被发现,其具有多种功能(例如增强团簇发光).本工作以双膦作为配体成功合成出原予层次单分布的金银纳米团簇[Au10Ag4(Dppp)5Cl4]Cl2...     

新型液体火箭发动机燃烧不稳定性研究

应用CFD方法对新型液体火箭发动机燃烧过程进行全尺寸数值模拟。首次有针对性地系统得出了混合比、液氧喷雾初始尺寸分布、缩进区液氧蒸发质量对氢氧火箭发动机燃烧振荡的影响规律,评估了1轮毂3径向喷嘴隔板抑制燃烧振荡的效果,并对氢氧、液氧/甲烷两种火箭发动机的燃烧不稳定性特征进行了对比分析。结果表明:存在某一特定的混合比、喷雾液滴直径、缩进区液氧蒸发质量敏感区间,易导致不稳定燃烧;喷嘴轮毂隔板可很好地抑制燃烧振荡;氢氧、液氧/甲烷燃烧分别以高频和低频压力振荡为主。     

可补半环上的同余

研究可补丰环上的同余关系,得出一些重要性质.并证明了一个半环R是可补半环当且仅当它是某个布尔环和布尔代数的直积,因而可补半环必是来法可交换的.     

Reducing Thermal Effect in End-Diode-Pumped Laser Crystal by Using a Novel Resonator

We report a new way, i.e. double-end-pumping, to extend the stability range of a laser resonator, in advantage of making the thermal loading be effectively divided between the ends of the laser crystal to reduce the thermal effect, thus to extend the stability range. Using this new way, we experimentally obtained a 2.7-W cw laser source at 671 nm by intracavity frequency doubling of 1342nm ofa Nd:YVO4 laser based on the nonlinear crystal LIB3O5. The maximum pump power is 28 W, which is higher than 13 W of the single-end-pumping.     

线性混合模型方差分量的检验

对于含有两个方差分量的随机效应设计阵为任意阵的线性混合模型的方差分量单边检验问题给出了精确的F检验和基于广义p值的检验.对于给出的精确的F检验给出检验存在条件以及是一致最优无偏检验的条件.通过数值模拟,基于广义p值检验的功效和犯第一类错误的概率被讨论,由模拟结果可以看出基于广义p值的检验很好地控制了犯第一类错误的概率.     

基于组合模型的武隆景区长期游客流量预测

由于某景区经营权回购需进行景区游客量长期预测。为克服长期预测的不确定性,我们采用基于旅游地环境容量的LOGISTIC模型和考虑客源地旅游需求的回归迭代模型进行组合预测。前者包含旅游地的环境容量限制参数,主要基于供给制约因素结合时间序列数据进行预测。后者主要从客源地的人均收入、价格水平、价格弹性和收入弹性进行预测。然后整合两模型进行组合预测,对两种预测结果进行加权得到组合预测游客流量,很好地解决了集成旅游地环境容量、"申遗"前后与高速公路通车前后游客量变化、游客时间序列规律、客源地人均可支配收入、旅游地吸引力和旅游地生命周期等众多因素进行长期预测的问题。预测结果作为政府部门经营权回购中补偿额确定的主要依据,已被采用。