镀膜长周期光纤光栅的折射率传感特性

基于严格的光栅三包层模型及其色散方程,对镀膜长周期光纤光栅的折射率传感特性进行了详细的研究.研究发现,镀膜长周期光纤光栅的谐振波长随环境折射率的变化而变化,而且这种变化有一个跳跃,跳跃后的变化与跳跃前相同:如跳跃前向短波方向漂移,则跳跃后也向短波方向漂移.镀膜后,长周期光纤光栅的折射率探测范围得到拓宽,而且探测的灵敏度...     

电共轭流体微型泵的实验研究（英文）

为了解决MEMS技术制备具有超厚、高深宽比电极结构的射流发生器中三角柱电极尖端部分出现的弧形缺陷以及脱模时缝隙电极易脱落等问题,提高射流发生器的制作质量以及电共轭流体微型泵的输出性能。结合理论分析与反复试验提出了一系列改进措施:优化涂胶、热处理、显影等工艺的参数以及缝隙电极的形状,采用新型KMPR光刻胶去除方法等。通过应用上述方法获得的射流发生器中,三角柱电极-缝隙电极对厚度约500μm,深宽比高,三角柱电极尖端结构完整,缝隙电极附着率有很大提高。同时,利用制备的射流发生器,设计、装配了电共轭流体微型泵的样机。     

负载型介孔Au/NiO催化剂的制备、表征与光谱特性研究

采用还原法和沉积-沉淀法制备了介孔Au/NiO催化剂,并运用XRD、N2吸附-脱附、UV-Vis、FTIR、和XPS等方法对其进行了表征,考察了制备方法对Au/NiO催化剂物理化学性质和丙烷氧化脱氢制丙烯反应催化性能的影响.实验结果表明Au/NiO催化剂具有一定的低温催化活性,而还原法制备的催化剂催化性能好于沉积-沉淀法制备的催化剂,反应温度350℃时,还原法制备的Au/NiO催化剂的丙烷转化率和丙烯选择性分别达到25.1%和39.8%.制备方法对表面Au的价态分布、颗粒大小及分散度均有影响.催化剂表面Auδ+物种是催化剂的主要活性组分.     

大功率铁磁性微波部件微放电演变机理与抑制

铁氧体环行器是承载航天器微波系统大功率的关键器件,其大功率微放电效应是影响航天器在轨安全、可靠运行的瓶颈问题。从影响微放电效应的关键因素——二次电子发射特性出发,提出铁磁性微波部件微放电效应物理演变模型,揭示了铁磁性微波部件内部初始自由电子与二次电子运动的空间规律;通过改变铁磁性微波部件表面二次电子发射特性,揭示了铁磁性微波部件抗微放电优化设计的物理原理。在S频段铁氧体环行器中验证了基于表面二次电子发射特性的微放电效应抑制,将器件的微放电阈值从380 W提高至3400 W以上,提升效率大于900%。     

Effect of Cu doping on the secondary electron yield of carbon films on Ag-plated aluminum alloy

Reducing the secondary electron yield (SEY) of Ag-plated aluminum alloy is important for high-power microwave components. In this work, Cu doped carbon films are prepared and the secondary electron emission characteristics are studied systematically. The secondary electron coefficient δ_max of carbon films increases with the Cu contents increasing at first, and then decreases to 1.53 at a high doping ratio of 0.645. From the viewpoint of surface structure, the higher the content of Cu is, the rougher the surface is, since more cluster particles appear on the surface due to the small solid solubility of Cu in the amorphous carbon network. However, from viewpoint of the electronic structure, the reduction of the sp² hybrid bonds will increase the SEY effect as the content of Cu increases, due to the decreasing probability of collision with free electrons. Thus, the two mechanisms would compete and coexist to affect the SEY characteristics in Cu doped carbon films.     

管内污垢监测模型研究

提出了一种基于质量传递理论的监测模型。它不但适应热质同时交换现象,还增加了对单纯质交换的适应性,并且避免了因温差描述产生污垢热阻为负值的特异现象。最后进行了相关正交实验,表明了该监测模型的合理性。     

高压密封微波消解-ICP-AES法测定五种蒙药中无机元素

采用HNO3-HClO4消解体系分别对额日敦-乌日勒、德都红花七味丸、通拉嘎-5、乌珠目-7、给旺-9等五种蒙药样品进行高压微波消解制样,利用电感耦合等离子体原子发射光谱法(ICP-AES)同时测定了镁、铝、钙、铬、锰、铁、钴、镍、铜、锌、砷、硒、锶、钼、银、镉和铅等17种无机元素的含量。通过添加标准回收实验,回收率均在97.25%~106.35%之间,验证了分析数据的可靠性。所有元素测定结果的相对标准偏差均小于3.3%,具有良好的准确度和精密度。实验结果表明,其中常量元素Ca,Mg和Fe,Mn,Zn,Cu的含量较高,测定结果可为开发研制蒙药新制剂、研制蒙药的质量控制标准和提高蒙药药效提供理论依据。     

Fabrication of Mn-Doped GaN Nanobars

We report a new method for large-scale production of GaMnN nanobars, by ammoniating Ga2O3 films doped with Mn under flowing ammonia atmosphere at 1000oC. The Mn-doped GaN sword-like nanobars are a single-crystal hexagonal structure, containing Mn up to 5.43 atom%. Thickness is about 100 nm and with a width of 200-400 nm. The nanobars are characterized by x-ray diffraction, scanning electron microscopy, x-ray photoelectron spectroscopy, high-resolution transmission electron microscopy and photoluminescence. The GaN nanobars show two emission bands with a well-defined PL peak at 388 nm and 409 nm respectively. The large distinct redshift （409 nm） are comparable to pure GaN（370 nm） at room temperature. The red-shift photoluminescence is due to Mn doping. The growth mechanism of crystalline GaN nanobars is discussed briefly.     

一类模糊数系数矩阵的模糊线性方程组的迭代算法

讨论模糊线性方程组X=A~X U解的存在条件及其迭代算法(其中,A~是以模糊数为元素的n×n矩阵,未知量X和常量U都是以模糊数为元素的n维向量,并且其加法和乘法均由Zadeh的扩张原理定义)。首先研究解的存在条件,尔后探讨求解的迭代算法及误差估计。