N-5-(1H-1,2,4-三唑基)-N′-芳甲酰基脲的合成与生物活性

以5-氨基-1H-1,2,4-三唑-3-羧酸与酰基异氰酸酯反应,合成了15个新的N-5-(1H-1,2,4-三唑基)-N′-芳甲酰基脲,用核磁共振氢谱、红外光谱和元素分析确证了其结构,并进行了室内生物活性测试.生测试验证明部分酰基脲类化合物具有良好的植物生长调节活性,其中N-5-(3-羧基-1,2,4-三唑基)-N′-o-氯苯甲酰基脲、N-5-(3-羧基-1,2,4-三唑基)-N′-o-溴苯甲酰基脲和N-5-(3-羧基-1,2,4-三唑基)-N′-P(或m)-甲基苯甲酰基脲具有优良的生长素活性.     

掺铁TiO2气相光催化降解正己烷的研究

利用钛酸丁酯水解浸渍、共沉淀、水热等方法制备了掺铁TiO2纳米复合粉体材料并通过XRD、BET、TEM等手段作了表征，研究了掺铁TiO2对气相光催化降解正己烷反应的活性并和商品TiO2 Degussa P-25作了比较，考察了制法、掺铁量、焙烧温度等的影响。结果表明，和大多数液相反应不同，铁的掺入抑制了TiO2对正己烷的气相光催化降解。水热处理能较大程度地改善掺铁和未掺铁TiO2的光催化性能。P-25对正己烷的气相光催化活性则明显小于未掺铁TiO2样品，也小于某些掺铁样品。     

某类解析函数的Fekete-szeg(o)问题

引入某族定义在单位圆内的解析函数K(λ,β),它是β型近于凸函数族的推广类.讨论了该族函数的Fekete-Szeg(o)问题,得到其Fekete-Szeg(o)不等式并证明了在一定条件下结果是准确的.     

倍频激光直接驱动透镜列阵均匀照明系统的优化设计与实验考核

在目前“神光”-Ⅱ器件尚不具备其它更为先进的束匀滑手段的前提下，2004年对透镜列阵束匀滑系统作了进一步的优化设计，以改善和提高靶面光强均匀性。在进行大量计算和比对的基础上，设计了如表1所列的3套新的列阵透镜参数。3套均匀化系统的焦斑尺寸大小基本一样，这是因为实验对此有一定的要求，但对冲击波平面性有很大影响的衍射调制周期有较大的差别，这可能成为决定冲击波平面性好坏的关键所在。     

α粒子激励下氩激发态光谱

用自制的单光子计数系统,测定了氩在α粒子激励下的发射光谱.在 300～600 nm范围,认证得到4条 Arl,24条 ArⅡ1条ArⅢ谱线.实验研究了谱线强度随气体压强的变化规律.经初步统计分析,提出在472.8 nm,487.9nm等谱线上实现核泵浦激光振荡的可能性.     

Visibility in magnetostrictive fiber-optic interferometric sensors and its dependence on the input SOP

The visibility in magnetostrictive fiber-optic interferometric sensors using a Gaussian laser beam is analyzed. It is shown that the conventional Gaussian laser beam has little influence on the visibility. The visibility depends strongly on the input state of polarization (SOP). We implement a cylindrical transducer and build a measurement setup with a polarization controller. The visibility dependent on the SOP of input light is measured. The estimated values are similar to the experiment results, which verifies the analysis.     

A 2 by 2 wavelength tunable Fabry-Perot filter by using an electro-optic polymer film

A tunable Fabry-Perot (F-P) filter by using electro-optic polymer film is proposed. The electro-optic polymer is alkoxysilane dye (ASD)/SiO2-TiO2 hybrid material, whose electro-optic coefficient γ33 is about 5 pm/V. The wavelength tuning range of 3.8 nm under 400-V DC voltage and the nonlinear characteristic with the electric field have been obtained via electro-optical properties of polymer. Both of polymer film fabrication and F-P filter design have been introduced. The tunable F-P filter is designed for the application of two-input/two-output port wavelength-selective optical switch. Also, some problems have been discussed in this letter.     

长周期光纤光栅模式与耦合的研究

长周期光纤光栅是在光纤纤芯中沿轴向形成折射率周期性调制的带阻型光纤器件。与光纤布拉格光栅不同，它表现为前向传播的纤芯基模与同向传播的各阶次包层模式在特定波长的耦合。研究了纤芯基模、包层模式（HE1t/EH1t）及其有效折射率随波长的变化，研究了纤芯基模与包层模式（HE1t/EH1t）的耦合系数。研究表明，纤芯基模与一阶低次包层模式的有效折射率随波长增大而减小，纤芯基模与HE1t产生的耦合系数远大于与EH1t的耦合系数，并且包层模式次数较低时，耦合系数随次数的升高而增加。这与以前的研究结果有所不同。     

Experimental investigation on divertor tungsten sputtering with neon seeding in ELMy H-mode plasma in EAST tokamak

Neon (Ne) seeding is used to cool the edge plasma by radiation to protect the divertor tungsten (W) target in the Experimental Advanced Superconducting Tokamak (EAST). The W sputtering in the outer divertor target with Ne seeding is assessed by the divertor visible spectroscopy system. It is observed that the W sputtering flux initially increases with Ne concentration in the divertor despite the decreasing plasma temperature. After reaching a maximum around 25 eV, the W sputtering rate starts to decrease, presenting a suppression effect. The effect on the divertor W sputtering flux and yield due to the competition between the increase of the Ne concentration and the decrease of the plasma temperature is discussed. The results show that enough Ne seeding is essential to effectively reduce the electron temperature and thus to suppress W sputtering. Moreover, ELM suppression is observed when Ne and W impurities enter the core plasma, which could be correlated to the enhanced turbulence transport in the pedestal.     

重视思维参与 提高复习课的有效性——高三复习课问题透视与应对策略

复习课,作为高三教学的一种常态课型,广大高三教师最为关注的是其有效性.然而,仔细审视高三课堂,不难发现,由于忽视学生的思维参与而导致的低效及无效的现象仍不时出现,下面就调研中发现的复习课中存在的一些普遍问题,谈一谈笔者的思考与建议,以期对提高高三复习课的有效性有所启示.