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二氯二茂锆同异丁基格氏试剂以1:2摩尔比反应,于室温下生成有机锆中间体,后者同烯烃、炔烃或二烯反应,最后生成还原的二聚物或分子内环化产物。 相似文献
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Fe(OH)2悬浮液在EDTA作用下氧气氧化生成δ-FeOOH的机理研究 总被引:2,自引:0,他引:2
At room temperature and in the presence of trace EDTA, the formation of δ-FeOOH was studied by the rapid oxidation of Fe(OH)2 suspension with O2. The structural and morphological changes were characterized by various techniques such as XRD, FTIR and TEM. γ-FeOOH and δ-FeOOH formed simutaneously in the early period of oxidation. But as the rate of mass transfer was in equilibrium, trace γ-FeOOH vanished gradually. Accordingly, pure phase δ-FeOOH was obtained. At the same time, critical amount ratio K of EDTA to Fe^2 was verified. The experiments show that the reactivity, rate of the oxidizing agent and pH of the initial medium were important factors for the formation of pure phase δ-FeOOH. Under the auxiliary effect of EDTA, the reactivity of O2 was nearly improved to that of H2O2. And the process of the oxidation that Fe(OH)2 suspension was oxidized by O2 under that condition was discussed. 相似文献
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运用电光采样技术揭示了反应离子刻蚀(RIE)ZnTe晶体表面THz辐射的光学整流产生机制, 观察到0.25 ps的THz场分布.通过比较刻蚀前后以及不同刻蚀条件下ZnTe样品在不同激发功 率下的THz辐射强度,发现由于反应离子刻蚀破坏了ZnTe样品表面的有序性,晶体的电光系 数随射频功率的增加而减小.借助于计算不同刻蚀条件下ZnTe晶体的频率响应函数,分析了 随射频功率增加ZnTe晶体响应频谱展宽的现象.
关键词:
THz辐射
反应离子刻蚀
ZnTe 相似文献
17.
Monodisperse Au-Fe 3 O 4 heterodimeric nanoparticles (NPs) were prepared by injecting precursors into a hot reaction solution.The size of Au and Fe 3 O 4 particles can be controlled by changing the injection temperature.UV-Vis spectra show that the surface plasma resonance band of Au-Fe 3 O 4 heterodimeric NPs was evidently red-shifted compared with the resonance band of Au NPs of similar size.The as-prepared heterodimeric Au-Fe 3 O 4 NPs exhibited superparamagnetic properties at room temperature.The Ag-Fe 3 O 4 heterodimeric NPs were also prepared by this synthetic method simply using AgNO 3 as precursor instead of HAuCl 4.It is indicated that the reported method can be readily extended to the synthesis of other noble metal conjugated heterodimeric NPs. 相似文献
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A new one-dimensional phenomenological model based on the dynamic strain aging mechanism is developed. In order to account for the elastic shrinkage induced by the Portevin-Le Chatelier effect, elastic deformation is considered under the boundary conditions of the present model. The simulated results are found to be in good agreement with the experimental observations. 相似文献
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boldmath Broadband water window supercontinuum generation with a ω+3ω/2 multicycle two-colour pulse
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We propose a method to generate a high-efficiency broadband water window supercontinuum with a ω+3ω/2 multicycle two-colour pulse. Our results reveal that the 3ω/2 laser pulse can simultaneously modulate the acceleration step and the ionization step, which not only broadens the bandwidth but also enhances the yield of the generated supercontinuum. An ultra-broadband supercontinuum from 290 eV to 555 eV covering the whole water window is generated. Using this method, we expect that an isolated 62-as pulse with a minor pre-pulse can be directly obtained. 相似文献