马铃薯组织过氧化氢生物传感器的研究

以马铃薯组织作为生物催化材料与氧电极结合研制成过氧化氢传感器，具有灵敏度高、选择性好和寿命长等特点．响应时间５ｍｉｎ，过氧化氢浓度在２×１０－４－４×１０－３ｍｏｌ／Ｌ之间与响应有线性关系，检出限５×１０－５ｍｏｌ／Ｌ．     

氨气敏电极测定有机物中的氮

本文介绍了利用氨气敏电极测定含氯有机物氯含量的实验条件及使用不同催化剂对不同类型的含氯有机物进行消化处理,然后用格氏作图法测定氮含量的方法,本法与一般消化-蒸馏测定法比较更为快速、简便,一般都能得到满意的结果。方法测定范围为10~(-1)—10~(-5)mol/L,回收率为95—105%。     

Effects of Ti and Zr Substituted on the Electrochemical Characteristics of MgNi-Based Alloy Electrodes

Mg-based hydrogen storage alloys MgNi, Mg0.9Ti0.1Ni, and Mg0.9Ti0.06Zr0.04Ni were successfully prepared by means of mechanical alloying （MA）. The structure and the electrochemical characteristics of these Mg-based materials were studied. The X-ray diffraction （XRD） result shows that the main phases of the alloys exhibit amorphous structure. The scanning electron microscopy （SEM） photograph shows that the particle size of Ti and Zr substituted alloys was about 2-4 μm in diameter. The cycle lives of the alloys were prolonged by adding Ti and Zr. After 50 charge-discharge cycles, the discharge capacity of Mg0.9Ti0.06Zr0.04Ni was 91.74% higher than that of MgNi alloy and 37.96% higher than that of Mg0.9Ti0.1Ni alloy. The main reason for the electrode capacity decay is the formation of Mg（OH）2 （product of Mg corrosion） at the surface of alloy. The potentiodynamic polarization result indicates that Ti and Zr doping improves the anticorrosion in an alkaline solution. The electrochemical impedance spectroscopy （EIS） results suggest that proper amount of Ti and Zr doping improves the electrochemical catalytic activity significantly.     

急性再障与中药微量元素及某些免疫指标关系的研究

急性再生障碍性贫血(简称急再)，是由多种病因导致骨髓广泛造血功能障碍的一组综合证，此病发病急，进展快，常伴有严重感染及内脏出血，严重威胁着广大患者的生命，本文从微量元素及免疫角度对急再进行了研究。同时对有关中草药进行了微量元素的测定，并与临床治疗密切结合，开阔了诊治急再的新思路。     

电感耦合等离子体串联质谱法测定半导体级磷酸中15种痕量杂质元素北大核心CSCD

半导体级磷酸是电子行业使用的一种超高纯化学试剂,广泛应用于超大规模集成电路、薄膜液晶显示器等微电子工业,主要用于硅晶片中氮化硅膜、镀金属膜和铝硅合金膜的湿法清洗和蚀刻[1-2]。在硅晶片的蚀刻过程中,磷酸中痕量杂质元素对电子元器件的成品率、电性能及可靠性有很大影响。不同的杂质污染会导致半导体器件的缺陷,如碱金属与碱土金属(钠、钾、钙、镁等)污染可导致器件的击穿电压降低;过渡金属与重金属(铁、铬、镍、铜、金、锰、铅等).     

Hard Photons from a Non-Equilibrated Quark-Gluon Plasma with Finite Baryon Density at a Two-Loop Level

We study hard photon production from a two-loop level （bremsstrahlung and annihilation with scattering） in a chemically equilibrating quark-gluon plasma at finite baryon density based on Jüttner distribution of partons of the system. We find that the photon yield from the two-loop level increases obviously with the increasing initial quark chemical potential.     

基于区域辐射一致性的移动阴影检测

为了同时检测本影与半影区域,提出并证明了阴影区域辐射的一致性属性。获取超像素区域轮廓内的点集合,将像素点集合(PCC)分为目标前景区域(目标PCC)和阴影区域(阴影PCC),利用所提出的基于区域生长的完整阴影检测与目标掩码增长算法,通过融合完整的阴影区域、完整的目标前景区域和ViBe掩码这三个部分,实现了前景目标掩码反向增长。在公开数据集中的实验结果表明,所提方法的阴影检测平均精度达到了82.5%,性能显著优于传统方法。目标掩码的平均增长率达到了8.84%,准确率达到了95%以上。     

Supercontinuum spectra generation in the single-mode optical fibre with concave dispersion profile

In this paper, a new method is proposed to generate broad supercontinuum (SC) spectra in the single-mode optical fibre with concave dispersion profile. We numerically simulate pulse evolutions and discuss physics mechanism in detail for SC spectrum generation in the optical fibre with concave dispersion profile. Furthermore, general criteria are presented for specifying the shape of SC spectrum by introducing normalized parameters, which are related to the fibres and the initial pump pulses. The results show that the flat and broad SC spectra are indeed generated in our proposed optical fibre.     

Geometrical nonlinear waves in finite deformation elastic rods

IntroductionSomenewphenomenaofnonlinearwavesinthesolidmediumsuchasshockwave ,solitarywaveetc.arepaidmoreattentiontoincreasinglybyresearchersbecausetheytakeonalotofimportantproperties.ItistheoreticallyanalyzedinRefs.[1 -6]thattheformationmechanismsofshockwaveandsolitarywaveintheelasticthinrodsaswellastheirpropagationproperties.TheexistenceofsolitarywaveintheelasticmediumsuchasarodandaplatehasbeenverifiedinRef.[7]byexperiments.Shockwaveandsolitarywavearesteadilypropagatingtraveling_wavesgenerat…     

银合欢叶成分槲皮素-3-O-鼠李糖甙的FT-IR和FT-Raman光谱

本文对银合欢叶中的成分槲皮素 - 3- O-鼠李糖甙进行了红外和拉曼光谱的测定 ,并对测定结果进行了详细的分析和讨论