Synthesis,Structure and Magnetic Property of One Ni~Ⅱ Based Coordination Polymer

One new coordination polymer, [Ni(m-bix)(m-BDC)](1, m-bix = 1,3-bis(imidazol-1-ylmethyl)benzene, m-BDC = 1,3-benzenedicarboxylic acids), has been hydrothermally synthesized and structurally characterized by elemental analysis, IR, TGA and X-ray single-crystal diffraction. The green block crystal of complex 1(C22H18N4Ni O4) belongs to monoclinic system, space group P21/c with a = 10.0418(3), b = 23.8651(6), c = 8.7872(2) A, β = 112.333(3)o, V = 1947.88(9)A3, Z = 4, Dc = 1.572 g/cm3, Mr = 461.11, F(000) = 952, R = 0.0335 and w R = 0.0683 for 2827 observed reflections(I 2σ(I)). Complex 1 exhibits a novel 6-connected 3D sxd type topological framework. The magnetic characterization of complex 1 shows antiferromagnetic coupling exchange.     

合并高校档案存在的问题及对策

高校档案工作的特点首先是以综合档案室为基础．档案工作法制建设基本配套，业务标准、规范基本具备；第二，工作基本上实现了集中统一管理，并且开发利用率较高，取得的经济效益也不言而喻；再次是档案工作管理健全，高桃档案工作之间注重横向联合。     

基于大量数据反馈的ODS的分析与应用

OD6是整个数据仓库体系架构中一个重要的组件。针对是否在数据仓库体系中选择ODS以及选择什么类型的ODS这一业界的难点问题。从数据更新以及反馈的角度列举了ODS的三种类型，详细的分析了各种类型的ODS的特点，阐述了每种类型的ODS可以满足什么商业需求，并结合零售业的案例具体分析。     

Photoresponse of the In0.3Ga0.7N metal-insulator-semiconductor photodetectors

In0.3Ga0.7N metal-insulator-semiconductor （MIS） and metal-semiconductor （MS） surface barrier photodetectors have been fabricated. The In0.3Ga0.7N epilayers were grown on sapphire by metalorganic chemical vapour deposition （MOCVD）. The photoresponse and reverse current-voltage characteristics of the In0.3Ga0.7N MIS and MS photodetectors were measured. A best zero bias responsivity of 0.18 A/W at 450 nm is obtained for the In0.3Ga0.7N MIS photodetector with 10 nm Si3N4 insulator layer, which is more than ten times higher than the In0.3Ga0.7N MS photodetector. The reason is attributed to the decrease of the interface states and increase of surface barrier height by the inserted insulator. The influence of the thickness of the Si3N4 insulator layer on the photoresponsivity of the MIS photodetector is also discussed.     

从一女性患者尿道分泌物中分离出气球菌样微生物

从在中山医科大学附属三院妇科门诊临床初诊为尿道炎的妇性患者的尿道分泌物中,分别两次,间隔４ｄ,重复分离出相同的ＡＬＯ菌株。     

多模式光学数字全息实验教学系统

研究设计了一种多模式现代光学数字全息成像实验教学系统.该系统可通过多光路模式与CcD技术相结合建立并记录数字全息图频率场,采用不同数学算法和程序实现全息图的全数字化重构再现与图像的三维测量,并通过界面设计详细演示数字全息成像的原理与过程.     

High Solubility of Hetero-Valence Ion （Cu^2＋） for Reducing Phase Transition and Thermal Expansion of ZrV1.6P0.4O7

Large thermal expansion at room temperature and high phase transition temperature of ZrV2O7 limit its practical applications and are reduced by the high solubility of hetero-valence ion （Cu^2＋） on the basis of an equal-valence substitution of P^5＋ for V^5＋. The temperature-dependent Raman spectra show that Zr0.9CU0.1V1.6P0.4O6.9 maintains a normal parent cubic structure till 173 K and transforms to a 3 × 3 × 3 cubic superstructure below 173K. Temperature dependent x-ray diffraction patterns of Zr0.9CU0.1V1.6P0.4O6.9 show near zero and negative thermal expansion. High solubility of lower valence Cu^2＋ relates to an equal-valence substitution of smaller pH for P^5＋, which extends the bond angle of V（P）-O-V in ZrV1.6P0.4O7 close to 180°. The change of microstructure is considered to be responsible for reduced phase transition temperature and thermal expansion.     

KLL dielectronic recombination process of He-like to O-like xenon ions

In this work,the KLL dielectronic recombination (DR) processes of highly charged He-like to O-like xenon ions are studied systematically by using a DR program,which is based on the multi-configuration Dirac-Fock (MCDF) method.The KLL DR resonant energies and the corresponding resonant strengths are calculated,emphasizing especially the effect of the Breit interaction on the DR strengths.The theoretical KLL DR spectra are obtained and compared with the latest experimental results obtained in the Shanghai Electron Beam Ion Trap.     

基于数据特征提取和SSA-BiLSTM的短期风电功率预测

为提高风电功率预测的准确性，提出了一种基于数据特征提取和麻雀算法优化双向长短期记忆网络（sparrow search algorithm optimised bi-directional long and short-term memory network,SSA-BiLSTM）短期风电功率预测模型。首先根据皮尔逊相关系数（Pearson correlation coefficient,PCC）分析风电数据中各影响因素与风电功率之间的相关性，根据计算结果将功率无关的因素去除。然后，采用自适应噪声完全集成经验模态分解（complete ensemble empirical mode decomposition with adaptive noise,CEEMDAN）将原始风电功率序列进行分解，得到一系列子序列分量。再将所有子序列输入麻雀算法（sparrow search algorithm,SSA）优化的双向长短期记忆（bi-directional long short-term memory,BiLSTM）模型中进行预测，根据所得预测值对风速序列进行修正。将修正所得的风速序列与风电功率...     

浅谈基建项目档案管理

随着高等教育事业的飞速发展,高校基建档案数量大幅度增长,但是高校基建档案管理水平滞后的状况仍然比较突出。基建档案意识存在淡薄、归档渠道不畅、进馆档案数量不足等问题,这些必将对高校今后的基本建设的维修和改建工作带来无法弥补的损失。本文针对高校基本建设档案管理目前还有意识存在淡薄、归档渠道不畅、进馆档案数量不足等问题,提出了相应的对策。