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高效液相色谱-荧光检测法测定血清中的犬尿氨酸 总被引:1,自引:0,他引:1
建立了高效液相色谱-荧光检测(HPLC-FLD)测定血清中犬尿氨酸(kynurenine,Kyn)含量的方法。采用Hypersil C8色谱柱(300 mm×6.0 mm,10 μm), 流动相为0.25 mol/L醋酸锌及50 mmol/L醋酸溶液(含3%乙腈),流速为1.5 mL/min, 荧光检测激发波长和发射波长分别为365 nm和480 nm。血清标本经5%(v/v)高氯酸溶液去除蛋白质后取上层清液直接进样, Kyn经流动相等度洗脱分离后,用FLD进行测定。研究结果表明Kyn保留时间约为8.3 min,线性范围为0.098~19.6 μmol/L,最低检出浓度为0.04 μmol/L,回收率为90.8%~96.2%,日内、日间测定的相对标准偏差均小于5%,苯丙氨酸、酪氨酸、色氨酸、5-羟色胺和犬尿喹啉酸等物质对犬尿氨酸的测定均无干扰。建立的方法简便、快速、灵敏、特异,适用于临床和科研应用。 相似文献
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遥感技术可以在宏观上对活动断裂及其构造特征进行全面的解译和识别.在区域遥感影像图制作和地质解译的基础上,采用增强和融合等图像处理方法,提高了遥感影像清晰度和解译精度,同时结合野外调查、测量以及断裂活动年代样品的采集和测定,对孝丰-三门湾断裂进行了详细的研究,查明了它的空间展布,并鉴定了活动时代和运动性质.研究结果表明,孝丰-三门湾断裂在杭州地区以挤压逆冲运动为主,兼有左旋走滑运动,并在各个地段和各个时期表现形式截然不同,影响了杭州南部地区地层沉积和构造演化.该断裂对杭州地区历史地震和现代地震具备一定的控制作用,可能在晚更新世以来有过活动. 相似文献
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The luminescence properties of lanthanum silicon oxynitride(La-Si-O-N) series doped by trivalent Ce ions have been investigated to seek for tunable wavelength-conversion phosphor for white light emitting diode applications.Four compound hosts of LaSiO2N,La4Si2O7N2,La5Si3O12 N,and La2Si6O3N8 were synthesized and examined in this work.Crystallographic examination for the equal amount of Ce 3+ substitution indicated that the covalency degree decreased in a sequence LaSiO2 N > La2Si6O3N8 > La4Si2O7N2 > La5Si3O12 N,not simply in correlation to the ratio of N3/O2.Excitation and emission spectrum measurements showed the main features of Ce3+ luminescence in the series:the centre of gravity of 5d bands depends on crystal-field splitting more strongly than that on covalency of Ce-N bonding;nephelauxetic effect could not be observed clearly for the investigated series;to some extent Stokes shift was dominated by crystal-field splitting rather than Ce-N covalency degree. 相似文献
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Controllable synthesis of high aspect ratio Mg_2B_2O_5 nanowires and their applications in reinforced polyhydroxyalkanoate composites 下载免费PDF全文
Highly pure magnesium borate (Mg2B2O5) nanowires with an average diameter of - 30 nm, an average length of 15 μm, and a high aspect ratio of - 500 have been synthesized on a large scale via a two-step method. MgBO2(OH) nanowires with high aspect ratios were first prepared via a PVP-assisted hydrothermal technique. Using these nanowires as precursors, single crystalline Mg2B205 nanowires were synthesized by post-annealing treatment at a relatively low temperature of 700 ℃. The important effect of the MgBO2(OH)-Mg2B2O5 conversion process on the morphology of the Mg2B2O5 nanowires was investigated and it was indicated that the recrystallization process plays an important role in the protection of the one-dimensional (1D) nanostructure. Moreover, the rigidity and the toughness of the Mg2B2O5 nanowire- reinforced PHA composites were tremendously improved compared to those of the pure PHA. Our results demonstrate the effectiveness of Mg2B2O5 nanowires for reinforcement applications in polymer composites. 相似文献
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通过描述“绳波演示仪”、“气泡的全反射”等若干成功的物理实验设计案例,剖析了其设计思想与方法,指出在实验设计中恰当使用延缓法能有效地提高物理演示实验的可视性,是改进现行教材中物理演示实验的有效途径之一. 相似文献
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一、关于截距一般地 ,已知直线与坐标轴上的截距有关 ,常设截距式 .但截距式不能表示与坐标轴垂直和过原点的直线 ,故用截距式求直线方程时 ,要注意检验过原点及与坐标轴垂直的直线 .例 1 求经过直线 7x + 8y =38及 3x -2 y =0的交点且在两坐标轴上的截距相等的直线 .解 易得两直线交点为 ( 2 ,3) ,设所求直线方程为 xa + ya =1 ,∵ 点 ( 2 ,3)在直线上 ,∴ 2a+ 3a=1 , ∴ a =5 .因此所求方程为 x + y =5 .许多同学往往解题到此结束 .显然题解中漏掉过原点的情况 ,即 3x -2 y =0 .从上题我们知道 ,解此类问题 ,… 相似文献
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采用严格耦合波理论,数值计算了不同参量下周期性极化铌酸锂晶体的电光衍射性质.研究表明:周期性极化铌酸锂晶体的周期性畴反转结构在电场的作用下相当于折射率衍射光栅,衍射性质和晶体的几何结构、周期、施加电场和入射角密切相关.以布喇格角度入射并满足布喇格衍射条件时,0级衍射光能量随施加电场的增大周期性地转化到-1级的衍射光中,最大转化效率达100%,增大周期性极化铌酸锂晶体的长度可以有效地降低转换电压值;以布喇格角度入射但光传输不满足布喇格衍射条件时,0级衍射光和-1级衍射光不能进行100%的能量转换,同时调制的周期性受到破坏.以布喇格角的倍数角入射时,0级光能量可以转化到相应的其他较高衍射级次,其中奇倍数衍射级的最大转换效率可达100%.研究结果为基于PPLN的集成电光器件设计提供有价值的参考. 相似文献
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We investigate the electronic structure, chemical bonding and elastic properties of the hexagonal aluminum carbonitride, Al5C3N, by ab initio calculations. Al5C3N is a semiconductor with a narrow indirect gap of 0.81 eV. The valence bands below the Fermi level (EF) originate from the hybridized Al p-C p and Al p-N p states. The calculated bulk and Young's moduli are 201 GPa and 292 GPa, which are slightly lower than those of Ti3SiC2. The values of the bulk-to-shear-modulus and bulk-modulus-to-c44 are 1.73 and 1.97, respectively, which are higher than those of Ti2AlC and Ti2AlN, indicating that Al5C3N is a ductile ceramic. 相似文献
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阐述了非线性铁氧体传输线的工作机理,并给出了等阻抗的设计方法。针对已有重复频率脉冲功率源输出脉冲特点,设计了工作重复频率可达10 kHz的铁氧体传输线,并可实现将前沿ns级的高压脉冲陡化至几百ps。采用多种NiZn铁氧体磁芯开展陡化实验,研究了磁芯参数、铁氧体传输线长度及外加励磁场等因素对陡化效果的影响,得出采用高饱和磁化强度的磁芯可以获得更快的脉冲前沿;采用小磁芯可以加快输出脉冲前沿,但需要的铁氧体长度更长;外加轴向励磁对陡化前沿也具有促进作用,但励磁场并非越大越好,而是存在一个最佳范围。目前,根据实验结果优化后,经铁氧体传输线可将脉冲前沿从4 ns陡化至450 ps,且输出脉冲电压峰值39 kV,基本实现了高重复频率、高功率及快脉冲输出。 相似文献