排序方式: 共有42条查询结果,搜索用时 0 毫秒
1.
The effect of incorporating sorbic acid (SA), an echo-friendly curing agent, and silica or carbon black (CB) filler, as well as gamma irradiation on the physico-chemical, mechanical and thermal properties of ethylene propylene diene monomer rubber (EPDM) was investigated. The results indicated that the developed composites revealed improvement in the studied parameters over the untreated samples. Filler incorporation into rubber matrix has been proven a key factor in enhancing the swelling resistance, tensile strength and thermal properties of the fabricated composites. The improvement in tensile strength and modulus was attributed to better interfacial bonding via SA. Alternatively, a comparison was established between the performance of the white and black fillers. The utmost mechanical performance was reported for the incorporated ratios 10 phr SA and 40 phr white filler into a 50 kGy irradiated composite. Meanwhile, the incorporation of CB yielded better thermally stable composites than those filled with silica at similar conditions. 相似文献
2.
The new compounds podophyllotoxone oxime (3) and epipodophyllotoxin azide (5) were prepared. The known dehydroanhydropicropodophyllin (6) was unexpectedly obtained from podophyllotoxin (1) by treatment with TMSCl/NaI/MeCN. 相似文献
3.
Physics of Atomic Nuclei - We present an analytic calculation of Branching Ratio (BR) and Charge–Parity (CP) violating asymmetries of the $$B_{s}^{0}$$ -meson decay into the two light vectors... 相似文献
4.
The synthesis of several new polyfunctionally substituted fused pyrazoles via reaction of 5‐amino‐3‐methylthio‐1H‐pyrazole‐4‐carboxylate ( 2 ) with different reagents is described. 相似文献
5.
The time-delayed Burgers equation is introduced and the improved tanh-function method is used to construct exact multiple-soliton and triangular periodic solutions. For an understanding of the nature of the exact solutions that contained the time-delay parameter, we calculated the numerical solutions of this equation by using the Adomian decomposition method and the variational iteration method (IVM) to the boundary value problem. 相似文献
6.
A multi-mode opto-thermo-mechanical stretching system was modified to study the changes in the 3D of optical and structural properties of stretched fibre along its axis. The structural deformation of isotactic Polypropylene, (iPP), fibres was studied at different draw ratios. The modified system coupled with Pluta polarising interference microscope was used to determine the variation of the birefringence in three dimensions during stretching process. Using this modified system, the multi-necking was detected. Subfringe analysis technique was used to determine the phase distribution of the obtained microinterferograms, which were given for illustration. 相似文献
7.
Treatment of 2‐cyano‐3‐phenyl‐2‐pentenedinitrile with some heterocyclic diazonium salts afforded the corresponding heterocyclic hydrazones. Some of the latter hydrazones were converted into fused polyaza‐heterocycles upon boiling in pyridine. Reaction of 2‐cyano‐3‐phenyl‐2‐pentenedinitrile with phenylisothiocyanate gave a tricyano‐thiole derivative which on treatment with hydrazonoyl chlorides and 1‐(benzothiazol‐2‐yl)‐2‐bromoethanone furnished 1,3,4‐thiadiazole and thiazole derivatives, respectively. 相似文献
8.
Four C-2 unsubstituted naphtho[2,3-b]furan-4,9-quinones were prepared via the corresponding phthalides obtained by directed ortho-metalation-based route. 相似文献
9.
Saúde-Guimarães DA Perry KS Raslan DS Chiari E Barrero AF Oltra JE 《Magnetic resonance in chemistry : MRC》2007,45(12):1084-1087
The chemical transformations of eremantholide C (1), a trypanocidal sesquiterpene lactone isolated from Lychnophora trichocarpha Spreng., gave five new oxide derivatives: 3'-hydroxyeremantholide C (2), 1'-formyleremantholide C (3), 1'-carboxyeremantholide C (4), 1'-carbomethoxyeremantholide C (5) and sodium 1'-carboxylate of eremantholide C (6). The (1)H and (13)C NMR data of all these derivatives were assigned based on 1D and 2D techniques. The derivatives were evaluated against Y and CL strains of Trypanosoma cruzi. All of them were inactive against the Y strain. Compounds 2 and 5 displayed 100% activity on the CL strain while compounds 4 and 6 were partially active on the CL strain. 相似文献
10.
Reaction of 3,5‐diaminothiophene‐2‐carbonitrile derivatives 3a‐c with ethoxycarbonylmethyl isothiocyanate and/or N‐[bis(methylthio)methylene]glycine ethyl ester led to formation of 7‐substituted‐8‐amino‐5‐thioxo‐6H‐imidazo[1,2:1′,6′]pyrimido[5,4‐b]thiophene‐2(3H)‐one derivatives 6a‐c and 7‐substituted‐8‐amino‐5‐(methylthio)imidazo[1,2:1′,6′]pyrimido[5,4‐b]thiophene‐2(3H)‐one 7a‐c , respectively. Also, the synthetic potential of the β‐enaminonitrile moiety in 3a‐c has been explored; it proved to be a promising candiate for the synthesis of 1,6‐disubstituted‐2,4‐diamino‐7,8‐dihydro‐8‐oxopyrrolo[1,2‐a]thieno[2,3‐e]pyrimidine derivatives 10a‐f and pyrido[2′,3′:6,5]pyrimido[3,4‐a]benzimidazole derivatives 12a,b . 相似文献