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排序方式: 共有93条查询结果,搜索用时 31 毫秒
1.
Ş. Erkoç 《Zeitschrift für Physik D Atoms, Molecules and Clusters》1991,19(4):423-425
The structural stability and energetics of carbon, silicon, and germanium microclusters containing 3?7 atoms have been investigated by using a recently developed empirical many-body potential energy function (PEF), which comprises two- and three-body atomic interactions. The PEF satisfies both bulk cohesive energy per atom and bulk stability exactly. It has been found that the most stable C3?4 microclusters are linear withD ∞h symmetry but C5?7 microclusters are planar withD nh symmetry. Silicon and germanium microclusters show similar structural stability. TheX n (X=Si, Ge;n=3?7) microclusters are found to be most stable in the following forms:X 3 is triangular withD 3h symmetry,X 4 is tetragonal withT d symmetry,X 5 is square pyramidal withD 4h symmetry,X 6 is bipyramidal square withO h symmetry, and finallyX 7 is square pyramidal having two atoms underneath withD 2h symmetry. 相似文献
2.
H. Güven N. Güngör A. Alemdar C. Ş. Özben 《Journal of Radioanalytical and Nuclear Chemistry》1996,214(4):269-276
Instrumental neutron activation analysis was applied to the determination of trace elements in a Na-bentonitic clay. The irradiation was done in the Triga Mark II type reactor of ITU Nuclear Energy Institute. The sample was irradiated in two steps for short- and long- lived isotopes. After irradiation, spectra were taken using a germanium detector, multichannel analyzer Canberra System 100 and a fitting program called Sampo 90. The spectra of short-lived isotopes were analyzed to determine Al, Mg, Na, K, Ca, Ti elements and Mn, V trace elements. The spectra of long-lived isotopes were analyzed to determine Sc, Br, Sb, Cs, La, Ce, Sm, Yb, Hf, Pa, Np trace elements. 相似文献
3.
Păcurariu C. Lazău R. I. Lazău I. Stoleriu Ş. 《Journal of Thermal Analysis and Calorimetry》2007,88(3):641-645
A kinetic study of the crystallization processes was performed for some decorative ceramic glazes in the PbO-SiO2-Na2O-K2O-CaO(BaO)-Al2O3-B2O3 system with addition of 10% TiO2 and ZnO. The crystallization kinetics has been studied in non-isothermal conditions using DTA technique. The apparent activation
energies of the crystallization processes were calculated using the Kissinger method. The main crystalline phase, which provides
the decorative effect, is rutile. This has been identified by X-ray diffraction and it is clearly visible in the optical microscopy
images taken in transmitted light, as needle-like or even prismatic crystals arranged in radial-fibrous aggregates. 相似文献
4.
The purpose of this paper is to elaborate a procedure, based on a mathematical model, for the setting of the pulling rate, capillary and thermal conditions, in order to grow a cylindrical rod with prescribed radius and length, by edge-defined film-fed growth (EFG) method. First, in the case of an axisymmetric meniscus, we use simultaneously the catching and the angle fixation conditions in order to find a formula, which describes the fluctuation of the angle between the horizontal axis Or and the tangent line to the free surface of the meniscus at the three phase point. This angle appears in the system of differential equations which describes the evolution of the radius of the rod. During the growth this angle can fluctuate due to the fluctuations of the crystal radius, or crystallization front level, or pressure, respectively. In the second part of the paper it is shown in which kind this formula together with the energy balance equation at the crystallization front level can be used for setting the pulling rate, the thermal and capillary conditions to grow a cylindrical rod with prescribed radius and length. Numerical illustration and simulation are presented for rods having thermo-physical properties similar to NdYAG and InSb. This type of results can be useful for the experiment planning, since personal computer simulation is less expensive than experiment. With this aim the present study was undertaken. 相似文献
5.
ABSTRACT Addition reactions of O-acetylated glycal esters of Kdo mono-, α-(2→8)- and α-(2→4)- linked Kdo disaccharide derivatives 1a - c with NIS in acetic acid afforded good yields of trans-diaxial as well as minor amounts of trans-diequatorial and cis-configured 2-O-acetyl-3-deoxy-3-iodo derivatives, which were efficiently reduced with Bu3SnH/AIBN to give the corresponding per-O-acetylated Kdo methyl ester derivatives. Similar reactions of 1a with NBS or NCS furnished the trans-diaxial 2-O-acetyl-3-bromo-3-deoxy- as well as 3-chloro-3-deoxy derivatives as the main products. Reaction of 1a with NBS in aqueous MeCN provided the 2,3-trans-bromohydrin derivative 11c, which upon treatment with DBU in MeCN gave the elimination product 11 and the α-2,3-anhydro derivative 12 as a suitable donor of glycosides with D-glycero-D-talo- or D-glycero-D-galacto configuration, respectively. 相似文献
6.
7.
This paper comments on a number of inaccuracies in the recently-published article by Balint et al. [S. Balint, A.M. Balint, M. Darau, Linear stability analysis of a non-slipping mean flow in a 2D-straight lined duct with respect to modes type initial (instantaneous) perturbations, Appl. Math. Model. 35 (2011) 1081–1095], concerning initial value acoustic perturbations to a steady mean nonslipping flow in a 2D duct: in particular, the neglect of antisymmetric solutions, and their comments on stability. Here, their dispersion relation is briefly rederived and simplified, two numerical results are presented demonstrating the existence of antisymmetric solutions in a specific case, and the inaccuracy in their comments on instability is highlighted. 相似文献
8.
9.
Balint Farkas Mate Matolcsi Peter Mora 《Journal of Fourier Analysis and Applications》2006,12(5):483-494
Recent methods developed by Tao [18], Kolountzakis and Matolcsi [7] have led to counterexamples to Fugelde’s Spectral Set
Conjecture in both directions. Namely, in
Tao produced a spectral set which is not a tile, while Kolountzakis and Matolcsi showed an example of a nonspectral tile.
In search of lower dimensional nonspectral tiles we were led to investigate the Universal Spectrum Conjecture (USC) of Lagarias
and Wang [14]. In particular, we prove here that the USC and the "tile → spectral" direction of Fuglede’s conjecture are equivalent
in any dimensions. Also, we show by an example that the sufficient condition of Lagarias and Szabó [13] for the existence
of universal spectra is not necessary. This fact causes considerable difficulties in producing lower dimensional examples
of tiles which have no spectra. We overcome these difficulties by invoking some ideas of Révész and Farkas [2], and obtain
nonspectral tiles in
. Fuglede’s conjecture and the Universal Spectrum Conjecture remains open in 1 and 2 dimensions. The one-dimensional case
is closely related to a number theoretical conjecture on tilings by Coven and Meyerowitz [1]. 相似文献
10.
Stefan Balint 《Journal of Mathematical Analysis and Applications》2010,362(1):231-1649
A boundary value problem in the case of the second order axi-symmetric Young-Laplace differential equation (some of whose solutions describe the static meniscus free surface, i.e. the static liquid bridge free surface between the shaper and the crystal, occurring in single crystal rod growth) is analyzed. The analysis concerns the dependence of the solution of an initial value problem of the equation on a parameter p (the controllable part of the pressure difference Δp across the free surface). Inequalities are established for p which are necessary or sufficient conditions for the existence of a solution which represents a stable and convex free surface of a static meniscus. The analysis is numerically illustrated for the static menisci occurring in the NdYAG laser single crystal rod growth from the melt by edge-defined film-fed growth (E.F.G.) technique. This kind of inequalities can be useful in the experiment planning and technology design. 相似文献