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Arena DA Bartynski RA Nayak RA Weiss AH Hulbert SL Weinert M 《Physical review letters》2003,91(17):176403
The Pd M4VV and M5VV Auger spectra of the 0.1 ML Pd/Ag(100) dilute surface alloy have been measured using Auger-photoelectron coincidence spectroscopy. The M4VV spectrum indicates that Pd 3d(3/2) core holes have a Coster-Kronig decay rate that is approximately 10 times that of Pd metal. Our calculations show that this giant enhancement arises from the local electronic structure of excited Pd atoms at the surface. Anomalous features in the Auger line shape are similar to those seen in dilute bulk PdAg alloys, and these features in the M5VV and M4VV lines are in good agreement with theoretical predictions. 相似文献
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R. L. Barbour J. R. Mooney M. Mehicic R. J. Weinert K. C. Benton J. G. Grasselli 《Macromolecular Symposia》1986,5(1):49-59
Polymer coatings on steel substrates were analyzed by reflectance/absorbance infrared spectroscopy. Initial studies were performed ex-situ on samples which had been cured at a variety of temperatures on two different substrates. Further studies were done in-situ under both air and nitrogen atmospheres. The two substrates studied were untreated cold-rolled steel and cold-rolled steel with a conversion coating of zinc phosphate. Changes in the spectra of the phosphate conversion layer correlated well with anti-corrosion properties. Mechanisms of degradation and cure could be determined from the in-situ studies (1). 相似文献
5.
Thilo Weinert 《Mathematical Logic Quarterly》2010,56(6):659-665
We introduce the Bounded Axiom A Forcing Axiom (BAAFA). It turns out that it is equiconsistent with the existence of a regular ∑2‐correct cardinal and hence also equiconsistent with BPFA. Furthermore we show that, if consistent, it does not imply the Bounded Proper Forcing Axiom (BPFA) (© 2010 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) 相似文献
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H. L. Weinert R. H. Byrd G. S. Sidhu 《Journal of Optimization Theory and Applications》1980,30(2):255-268
Many of the optimal curve-fitting problems arising in approximation theory have the same structure as certain estimation problems involving random processes. We develop this structural correspondence for the problem of smoothing inaccurate data with splines and show that the smoothing spline is a sample function of a certain linear least-squares estimate. Estimation techniques are then used to derive a recursive algorithm for spline smoothing. 相似文献
7.
A review will be given of recent calculations on metal films which give information about metal-metal interfaces. The systems discussed will include palladium on niobium, cesium on tungsten, and nickel on copper. In general it is found that the electronic structure closely resembles the bulk within one or two atomic layers of the interface. Using these methods it is possible to calculate directly the interface energy. 相似文献
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U(VI) can be separated from Ga, Fe(III), Bi, Pb, Cd, Zn, Cu(II) and Au(III) by quantitative elution with 0.50M HBr in 86% acetone or with 0.35M HBr in 90% acetone from a column of AG50W-X4 cation-exchange resin of 200-400 mesh particle size. U(VI) and many other ions are retained. U(VI) then can be eluted selectively with 0.50M HCl in 83% acetone or with 0.35M HCl in 85% acetone. Co(II), Mn(II), Mg, Ca, Ti(IV), Al, Zr, Th and La are quantitatively retained by the column. These elements then can be eluted with 5M HNO(3). At the higher acid concentration (0.50M) the separation between U(VI) and Li is not satisfactory but is excellent at the lower acid concentration; the U(VI) peak is sharper at the higher acid concentration. Separations are sharp and quantitative, as is demonstrated by results for some synthetic mixtures. Distribution coefficients and elution curves are presented. 相似文献
10.
The new cluster [Bu4N]2[W6Cl8(OSO2CF3)6] (1) has been prepared and structurally characterized. This material is an effective precursor for the generation of cluster ions with the general formula [W6C18L6]n (L = Cl-, Br-, I-, NCS-, NCO-, NCSe-, and O=PPh3; n = 2- or 4+). The last three clusters are new. The products have been characterized by IR spectroscopy, NMR spectroscopy, and FAB mass spectrometry. In addition to 1, the products [Bu4N]2[W6C18(NCS)6] (5) and [Bu4N]2[W6C18(NCO)6] (7) were structurally characterized. Crystal data for 1: space group, P2(1/c) (No. 14); a = 11.116(5) A; b = 27.952(1) A; c = 24.516(1) A; beta = 95.182(9) degrees; V = 7586.3(5) A3; Z = 4. Crystal data for 5: space group, P2(1/n) (No. 14); a = 11.3323(9) A; b = 12.3404(9) A; c = 44.583(3) A; beta = 97.089(1) degrees ; V = 6187.1(7) A3; Z = 4. Crystal data for 7: space group, P1 (No. 2); a = 11.8009(8) A; b = 11.9332(8) A; c = 11.9522(8) A; alpha = 77.904(1) degrees; beta = 95.182(9) degrees; gamma = 62.574(1) degrees V = 1450.5(2) A3; Z = 1. 相似文献