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1.
W M Niessen M A de Kraa E R Verheij P J Bergers G F La Vos U R Tjaden J van der Greef 《Rapid communications in mass spectrometry : RCM》1989,3(1):1-4
On-line sample pretreatment by means of the phase-system switching approach is an interesting technique for the analysis of aqueous samples, e.g., plasma, by means of supercritical-fluid chromatography. In order to analyse plasma samples the following analytical procedure is used. The plasma sample is injected on to a short precolumn, which is washed with water and subsequently dried with nitrogen. Next, the solutes are desorbed with the supercritical mobile phase, analysed with packed-column supercritical-fluid chromatography and detected with either a UV detector or a mass spectrometer, equipped with a moving-belt interface. The herbicide diuron is selected as a test compound to study the feasibility of this approach. Using a selective detector the procedure is sufficiently sensitive to detect diuron in plasma, but not appropriate to detect the diuron metabolites in a post-mortem plasma sample. These have been identified with liquid chromatography/mass spectrometry. The detection limit of diuron in plasma using the procedure described is about 30 ng/mL. 相似文献
2.
Natale Paolo Vinai 《manuscripta mathematica》2004,115(3):299-311
We prove that the arithmetic degree of a graded or local ring A is bounded above by the arithmetic degree of any of its associated graded rings with respect to ideal I in A. In particular, if Spec(A) is equidimensional and has an embedded component (i.e., A has an embedded associated prime ideal), then the normal cone of Spec(A) along V(I) has an embedded component too. This extends a result of W. M. Ruppert about embedded components of the tangent cone.Mathematics Subject Classification (2000): Primary 13H15, 13A30; Secondary 13D45, 14Q99 相似文献
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5.
For a given two-dimensional surface μ, we studi invariants for oriented links in μ×[0,1] which generalize the two-variable
HOMFLY polynomials when μ is the 2-disk. These invariants are connected to multiparameter quantum groups whose special properties
are discussed.
Si studiano gli invarianti dei nodi in spazi del tipo μ×[0,1], dove μ è una superficie. Questi invarianti generalizzano gli
invarianti di HOMFLY.
(Conferenza tenuta dal Prof. P. Cotta-Ramusino il 16 maggio 1991) 相似文献
(Conferenza tenuta dal Prof. P. Cotta-Ramusino il 16 maggio 1991) 相似文献
6.
Onofrio Mario Di Vincenzo Plamen Koshlukov Roberto La Scala 《Advances in Applied Mathematics》2006,37(4):541
In this paper we describe completely the involutions of the first kind of the algebra UTn(F) of n×n upper triangular matrices. Every such involution can be extended uniquely to an involution on the full matrix algebra. We describe the equivalence classes of involutions on the upper triangular matrices. There are two distinct classes for UTn(F) when n is even and a single class in the odd case.Furthermore we consider the algebra UT2(F) of the 2×2 upper triangular matrices over an infinite field F of characteristic different from 2. For every involution *, we describe the *-polynomial identities for this algebra. We exhibit bases of the corresponding ideals of identities with involution, and compute the Hilbert (or Poincaré) series and the codimension sequences of the respective relatively free algebras.Then we consider the *-polynomial identities for the algebra UT3(F) over a field of characteristic zero. We describe a finite generating set of the ideal of *-identities for this algebra. These generators are quite a few, and their degrees are relatively large. It seems to us that the problem of describing the *-identities for the algebra UTn(F) of the n×n upper triangular matrices may be much more complicated than in the case of ordinary polynomial identities. 相似文献
7.
Paolo Aluffi 《Rendiconti del Circolo Matematico di Palermo》1938,62(1):3-26
We obtain a precise relation between the Chern–Schwartz–MacPherson class of a subvariety of projective space and the Euler characteristics of its general linear sections. In the case of a hypersurface, this leads to simple proofs of formulas of Dimca–Papadima and Huh for the degrees of the polar map of a homogeneous polynomial, extending these formula to any algebraically closed field of characteristic \(0\), and proving a conjecture of Dolgachev on ‘homaloidal’ polynomials in the same context. We generalize these formulas to subschemes of higher codimension in projective space. We also describe a simple approach to a theory of ‘polynomial Chern classes’ for varieties endowed with a morphism to projective space, recovering properties analogous to the Deligne–Grothendieck axioms from basic properties of the Euler characteristic. We prove that the polynomial Chern class defines homomorphisms from suitable relative Grothendieck rings of varieties to \(\mathbb{Z }[t]\). 相似文献
8.
We prove that there is no functorial universal finite type invariant for braids in Σ×I if the genus of Σ is positive. To cite this article: P. Bellingeri, L. Funar, C. R. Acad. Sci. Paris, Ser. I 338 (2004). 相似文献
9.
Dinesh Topwal U. Manju Sugata Ray S. Raj D. D. Sarma S. R. Krishnakumar M. Bertolo S. La Rosa G. Cautero 《Journal of Chemical Sciences》2006,118(1):87-92
Disordered Sr2FeMoO6 shows a drastic reduction in saturation magnetization compared to highly ordered samples, moreover magnetization as a function
of the temperature for different disordered samples shows qualitatively different behaviours. We investigate the origin of
such diversity by performing spatially resolved photoemission spectroscopy on various disordered samples. Our results establish
that extensive electronic inhomogeneity, arising most probably from an underlying chemical inhomogeneity in disordered samples, is
responsible for the observed magnetic inhomogeneity. It is further pointed out that these inhomogeneities are connected with
composition fluctuations of the type Sr2Fe1+x
Mo1-x
O6 with Fe-rich (x > 0) and Mo-rich (x < 0) regions.
Dedicated to Prof J Gopalakrishnan on his 62nd birthday. 相似文献
10.
A difference between the thermal behaviour of the isotropic and liquid-crystalline state of sonicated DNA in aqueous salt solution containing poly(ethyleneglycol)(PEG) has been demonstrated. On cooling, a different degree of renaturation of thermally denaturated DNA is observed between samples which form the isotropic state and more concentrated samples which on cooling form the cholesteric state. 相似文献