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A. S. Gordetsov S. V. Zimina V. F. Ur’yash E. M. Moseeva 《Russian Journal of General Chemistry》2013,83(2):299-302
At the interaction of bis (η5-cyclopentadienyl)vanadium with iodobenzoic acid or trimethylsilyl o-iodobenzoate in toluene depending on the ratio of the initial reagents bis(η5-cyclopentadienyl)vanadium(o-iodobenzoate) or η5-cyclopentadienylvanadium-bis-o-iodobenzoate were obtained in high yields. The latter was also formed in the reaction of bis(η5-cyclopentadiene)vanadium dihloride with trimethylsilyl o-iodobenzoate. 相似文献
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A. S. Gordetsov V. N. Latyaeva S. V. Zimina E. Yu. Levakova V. K. Cherkasov E. M. Moseeva S. E. Skobeleva 《Russian Chemical Bulletin》1996,45(5):1214-1217
The reactions of Cp2V and Cp2VCl withp-toluenesulfonyl chloride were studied. Depending on the ratio of the reagents, the solvent, and other reaction conditions, the compoundsp-MeC6H4S02VCp2Cl, (p-MeC6H4S02VCp)n or (p-MeC6H4S02VO)m are formed.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 5, pp. 1275–1278, May, 1996. 相似文献
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Gordetsov A. S. Zimina S. V. Kulagina N. V. Moseeva E. M. Kurskii Yu. A. Lopatin M. A. 《Russian Journal of General Chemistry》2003,73(10):1557-1560
Phenylurea and N-trimethylsilyl-N'-phenylurea react with vanadocene (Cp2V) in toluene to give N-(5-cyclopentadienyl)vanadio-N'-phenylurea as a major product and Cp2VN = C = O and aniline as byproducts. The reaction of N-trimethylsilyl-N'-phenylurea with N-bromosuccinimide in THF produces, instead of expected N-phenylureidosuccinimide and bromotrimethylsilane, succinimide and N-(p-bromophenyl)-N-trimethylsilylurea which hydrolyzes to form (p-bromophenyl)urea. 相似文献
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A. S. Gordetsov L. N. Martynova S. V. Zimina E. M. Moseeva S. E. Skobeleva N. V. Kulagina 《Russian Chemical Bulletin》1994,43(3):458-460
N,N-Bis(trimethylsilyl)dicyandiamide was prepared for the first time by the reaction of dicyandiamide with hexamethyldisilazane in boiling tetrahydrofuran. Thermal transformations of this compound were studied by DTA. The novel compound may be used in the synthesis of bis(trimethylsilyl)carbodiimide.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 3, pp. 498–500, March, 1994. 相似文献
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A. S. Gordetsov S. V. Zimina S. V. Saprykina L. B. Loginova A. V. Piskunov V. F. Ur’yash E. M. Moseeva 《Russian Journal of General Chemistry》2011,81(4):658-662
1,3,5-Tris[bis(η5-cyclopentadienyl)chlorovanadium]melamin is prepared in high yield by the reaction of N,N′-bis(trimethylsilyl)dicyandiamide with bis(η5-cyclopentadienylvanadium) dichloride in tetrahydrofuran. As side products, trimethylchlorosilane and cyclopentadiene formed.
Reaction of N,N′-bis(trimethylsilyl) dicyandiamide with benzoyl chloride results in the formation of tris(benzoyl)melamin. 相似文献
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A. S. Gordetsov S. V. Zimina E. M. Moseeva S. E. Skobeleva N. V. Kulagina V. V. Pereshein 《Russian Chemical Bulletin》1993,42(12):2021-2023
N-(5-Cyclopentadienylvanadium)benzenesulfonamide has been synthesized for the first time by treating benzenesulfonamide orN-(tributylstannyl)benzenesulfonamide with vanadocene.Deceased.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 12, pp. 2107–2109, December, 1993. 相似文献
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