Background oriented schlieren for flow visualisation in hypersonic impulse facilities

Experiments to demonstrate the use of the background-oriented schlieren (BOS) technique in hypersonic impulse facilities are reported. BOS uses a simple optical set-up consisting of a structured background pattern, an electronic camera with a high shutter speed and a high intensity light source. The visualization technique is demonstrated in a small reflected shock tunnel with a Mach 4 conical nozzle, nozzle supply pressure of 2.2 MPa and nozzle supply enthalpy of 1.8 MJ/kg. A 20° sharp circular cone and a model of the MUSES-C re-entry body were tested. Images captured were processed using PIV-style image analysis to visualize variations in the density field. The shock angle on the cone measured from the BOS images agreed with theoretical calculations to within 0.5°. Shock standoff distances could be measured from the BOS image for the re-entry body. Preliminary experiments are also reported in higher enthalpy facilities where flow luminosity can interfere with imaging of the background pattern. A version of this paper was presented at the 25th International Symposium on Shock Waves in Bangalore in July 2005.     

A Measuring System for Bulk and Shear Characterization of Polymers

This paper describes a novel measuring system for investigating the influence of pressure and temperature on the mechanical properties of time-dependent polymer materials. The system can measure the volume and the shear relaxation moduli of solid polymer specimens simultaneously subjected to temperatures from −50 to +120°C with a precision of ±0.01°C, and pressures from atmospheric to 500 MPa with a precision of ±0.1 MPa. The paper demonstrates the measuring capabilities of the apparatus. For poly(vinyl) acetate (PVAc) are presented sample measurements of the shear relaxation modulus as function of time, pressure and temperature; specific volume; the bulk creep compliance; the coefficient of thermal expansion; the bulk modulus; and the pressure drop experiments which simulate conditions to which a material is exposed during the injection molding process. The shear moduli may be measured in the range from 1 to 4,000 MPa with the relative error of 3%.The error of volumetric measurements is 0.05%, which corresponds to 0.00005 cm³/g. In all cases results are shown as measured, no additional smoothing or filtering was employed. This paper is dedicated to Professor Nicholas W. Tschoegl on the occasion of his 87th birthday, for his contributions to the field of time-dependent bulk properties of polymeric materials.     

A comparative study of high‐order variable‐property segregated algorithms for unsteady low Mach number flows

In this paper, five different algorithms are presented for the simulation of low Mach flows with large temperature variations, based on second‐order central‐difference or fourth‐order compact spatial discretization and a pressure projection‐type method. A semi‐implicit three‐step Runge–Kutta/Crank–Nicolson or second‐order iterative scheme is used for time integration. The different algorithms solve the coupled set of governing scalar equations in a decoupled segregate manner. In the first algorithm, a temperature equation is solved and density is calculated from the equation of state, while the second algorithm advances the density using the differential form of the equation of state. The third algorithm solves the continuity equation and the fourth algorithm solves both the continuity and enthalpy equation in conservative form. An iterative decoupled algorithm is also proposed, which allows the computation of the fully coupled solution. All five algorithms solve the momentum equation in conservative form and use a constant‐ or variable‐coefficient Poisson equation for the pressure. The efficiency of the fourth‐order compact scheme and the performances of the decoupling algorithms are demonstrated in three flow problems with large temperature variations: non‐Boussinesq natural convection, channel flow instability, flame–vortex interaction. Copyright © 2010 John Wiley & Sons, Ltd.     

Fluidization of particles in SCW fluidized bed: Voidage distribution of emulsion phase

Supercritical water (SCW) fluidized bed reactors convert biomass to fuels without pollutants emission. In this work, experimental studies were carried out to investigate voidage distribution in an SCW fluidized bed by capacitance probes. Quartz sands with different particle sizes were fluidized by SCW under system pressure of 20–27 MPa and temperature of 410–570 °C. The effect of operation conditions on voidage distributions of the emulsion phase (e.g. averaged voidage and probability density) is discussed. A predicting correlation between voidage and superficial velocity in emulsion phase is proposed. The relative error of the correlation is within ±25%. These research results provide useful guidance for the optimization of supercritical water gasification technology.     

Wireless strain and temperature measurement with radio telemetry

A line of miniature strain and temperature telemetry transmitters have been developed for measurements in areas where direct-wire connections are not possible. The units described are 8–16 cu cm in volume (0.5–1.0 cu in.) and operate over a 0°C to 150°C ambient-temperature range with up to 30,000g′s acceleration. Battery life with a battery about the same size as the transmitter ranges from 50 to 200 hr. There is no degradation in accuracy for a 25-percent variation in battery voltage. Two types of strain transmitters have been developed. Both have full-scale ranges adjustable from 500 to 5000 microstrain and accuracies of ±2 percent. The “static” unit has response from dc to 1 KHz and the “dynamic” transmitter handles 30 Hz to 20 KHz. There are also two types of temperature transmitters. One accepts a variety of thermistor sensors for various measurement ranges between ?100°C and +600°C with accuracies of ±1°C. The other accepts various thermocouple inputs and has an accuracy of ±2 percent of range. These transmitters have been employed for a variety of industrial and scientific measurements. Some of the successful applications include transmission of strain and temperature data directly from pistons of reciprocating engines and from the compressor turbines of fan-jet engines.     

A New Cell for Electrical Conductivity Measurement on Saturated Samples at Upper Crust Conditions

Electrical resistivity soundings are used by geophysicists to determine the structure and composition of the Earth’s crust and mantle and to explore natural resources (ore, oil, gas, water). Their interpretations in terms of composition and in-situ physical conditions depend mainly on laboratory measurements of electrical conductivity of rocks at simulated crustal conditions of temperature, pressure, saturation and pore pressures. These measurements present a numbers of limitations, in particular, in the case where conductive pore fluids are present, as in the case of deep reservoir conditions, where temperature exceeds 250 °C. Here, we present a new cell capable of measuring electrical conductivity of large saturated samples at confining pressure up to 200 MPa, pore pressure up to 50 MPa, and temperature up to 500 °C. The measurement cell has been developed in a commercial, internally heated, gas pressure apparatus (Paterson press). It is based on the concept of “guard ring” electrode, which is adapted to samples that are jacketed by a very conductive, metallic material. Numerical modeling of the current flow in the electrical cell allowed defining the optimal cell geometry. Calibration tests have been performed on Fontainebleau sandstones saturated with electrolytes of different conductivities, up to 350 °C. The resulting electrical formation factor and temperature dependence of electrical conductivity are in very good agreement with previous studies. This new cell will improve the exploration and exploitation of deep fluid reservoirs, as in unconventional, high enthalpy geothermal fields. In particular, the investigations address possible effects of fluid-rock interactions on electrical resistivity of a reservoir host rock.     

Mechanical Properties of Transparent Polycrystalline Alumina Ceramics Processed Using an Environmentally Benign Thermal Gel Casting Process

Technological advancements in ceramic powder synthesis, shaping and sintering have made it possible to tailor the microstructural, mechanical and optical property relationships in the case of advanced transparent ceramic materials. Transparent polycrystalline alumina (TPCA) is the hardest known transparent ceramic and one of the emerging candidate materials for transparent armour applications. The prerequisites for obtaining transparency with the high hardness, is to achieve the sintered average grain sizes <1 μm in combination with density close to the theoretical value. This paper outlines the processing of TPCA by an environmentally benign methyl cellulose based thermal gel casting (MCTG) process, which is employed for the first time in shaping of the TPCA. The green specimens shaped through this technique were pressureless sintered (PLS) to >96 % density at an optimum temperature of 1350 °C. The post sintering by Hot Isostatic Pressing (HIP) at an optimum temperature of 1350 °C and a pressure of 195 MPa resulted in >99.5 % of the theoretical density and a grain size of 0.7 μm. For the sake of comparison, conventional polycrystalline alumina samples (non-transparent) were also processed by sintering at 1550 °C under PLS condition with nearly the same densities (designated as PCA). The TPCA thus developed exhibit a combination of high hardness of 21 GPa, flexural strength of 550 MPa and excellent fracture resistance properties as compared to conventional PCA samples.     

Drag force on a free surface-piercing yawed circular cylinder in steady flow

The force distribution on a surface-piercing yawed cylinder surface differs significantly from that on a surface-piercing vertical cylinder. The established numerical model for flow past the surface-piercing yawed cylinder with yaw angles from −45° to 45° was solved by the standard large-eddy simulation (LES) methodology. Six cases at intervals of ±15° relative to the vertical were studied at the Reynolds number of 27 000 and the Froude number of 0.8 based on the cylinder diameter and free-stream velocity, among which the drag forces on four cylinders with yaw angles from −15° to 30° were tested for the validation of the LES approach. The results revealed that the time-averaged total drag coefficient for all cases increases with the increase of yaw angle compared to that of the surface-piercing vertical cylinder, even over 2.5 for the ±45°-yawed cylinders. The sectional drag coefficients for the negatively yawed cylinders are much greater than that for the vertical cylinder, and much less for the positively yawed cylinders. The unbalanced hydrostatic pressures on the inclined section are mainly responsible for those increment and decrement. Once the hydrostatic pressure was removed, the sectional drag coefficient on the mid-span of the positively yawed cylinder increases from the top section to the bottom, and decreases for the negatively yawed cylinder. The corresponding integrated total drag coefficient decreases with the increase of the yaw angle to ±15°, then increases with the further increase of the magnitude of yaw angle.     

High-temperature test facility for repeated pressure loading of cylinders

A test facility capable of subjecting cylindrical specimens to repeated pressure loadings at high temperatures is described. The loading rates range from 480 to 600 cycles per minute. The test pressures range from 310 to 447 MN/m² and the test temperatures are 260°C, 538°C and 816°C. Testing was performed at two strain rates. A “low” strain rate of about 4 per second and a “high” strain rate of about 9.6 per second. The uniqueness of the facility lies in the choice of a solid loading medium to transmit pressure to the specimen. Some typical results are presented.     

Free convective heat transfer and criterion of onset of free convection in a horizontal melt layer of ice heated by upper rigid surface

An experimental and analytical investigation pertaining to the effect of density inversion of water on the free convective heat transfer and the onset of free convection in a horizontal melt layer of ice heated by upper rigid surface is carried out. Temperatures of the upper surface are varied from 1°C to 15°C, with Rayleigh number ranging from 2 × 10² to 1 × 10⁵. From the present study, it can be demonstrated both experimentally and analytically that the density inversion of water plays an influential role in such a melt layer and the onset of free convection and the free convective heat transfer are considerably affected by the temperature of upper rigid surface T₂, in the case of T₂ ≤ 8° C, unlike the results obtained for common fluids without density inversion.     

Photoelastic technique to investigate the effect of temperature and strain rate on plastic flow in mild steel

Dynamic photoelastic-coating technique was used to observe successive developments of plastic flow in tension at a temperature ranging from ?157°C to 20°C. A type of plastic flow occurred which was determined by a combination of temperature and strain rate. A correlation was found to exist between photoelastic observations and the equation of thermal activation.     

Development of Tactile Eye Stiffness Sensor

This article describes the design of a novel trans-scleral tonometer based on the use of multiple force sensors forming a mechanical stiffness sensor. The approach is akin to an instrumented form of digital palpation tonometry in which manual paplation is used to infer the stiffness, and hence, the intraocular pressure of the eye. Force indentation data from multiple probes has been shown to correlate with the intraocular pressure (IOP) using encucleated porcine eyes. A noticeable amount of hysteresis has been observed during indentations at higher rate. Analysis of the experimental data indicates that stress relaxation (accommodation) in the visco-elastic corneo-scleral shell is the primary factor of the observed hysteresis. Further tests under different indentation rates show that the novel tonometer is expected to have an accuracy of ±1 mmHg when the indentation rate is kept below 0.5 mm/sec for pressure range of 10–35 mmHg. Using a calibrated finite element model of the measurement, the effect of lateral and angular misalignment is also examined. The results show that the position and orientation of the tactile sensor has to be controlled to within ±1 mm and ±3° in order to achieve a target accuracy of ±1 mmHg.     

Laser Induced Stress Wave Thermometry for <Emphasis Type="Italic">In-Situ</Emphasis> Temperature and Thickness Characterization of Single Crystalline Silicon Wafer Part II – Experimental Results

TAP-NDE is employed to perform an experimental study on silicon wafers of different thicknesses to determine the maximum possible resolution of TAP-NDE towards temperature sensitivity, and to demonstrate the ability to differentiate between wafers of different deposition layer thickness at temperatures up to 600°C. Temperature resolution is demonstrated for ±10°C resolution and for ±5°C resolution; while thickness differentiation is carried out with wafers carrying 4,000?Å and 8,000?Å of aluminum deposition layer. The experimental group velocities of a set of selected frequency components extracted using the Gabor wavelet time-frequency analysis compare favorably to their corresponding theoretical group velocities. It is shown that TAP-NDE is a feasible tool for identifying and characterizing thickness and temperature changes simultaneously during thermal annealing that can replace the current need for separate characterization of these two important parameters in semiconductor fabrication.     

Non-invasive measurement of void fraction and liquid temperature in microchannel flow boiling

Past thermometry research for two-phase microfluidic systems made much progress regarding wall temperature distributions, yet the direct measurement of fluid temperature has received little attention. This paper uses a non-invasive two-dye/two-color fluorescent technique to capture fluid temperature along with local liquid fraction in a two-phase microflow generated by injecting air into a heated microchannel. The fluorescent emission of Rhodamine 110 and Rhodamine B, measured with photodiodes, is used to obtain local liquid temperature (±3°C) and void fraction (±2% full-scale) over a temperature range from 45 to 100°C. Arrays of these sensors can significantly expand the set of measurable flow parameters to include bubble/slug frequency, size, velocity, and growth rates in addition to mapping the local liquid temperature and void fraction.     

Effects of chamber temperature and pressure on the characteristics of high speed diesel jets

This study is an investigation into the effects of temperature and pressure within a test chamber on the dynamic characteristics of injected supersonic diesel fuel jets. These jets were generated by the impact of a projectile driven by a horizontal single stage powder gun. A high speed video camera and a shadowgraph optical system were used to capture their dynamic characteristics. The test chamber had controlled air conditions of temperature and pressure up to 150 °C and 8.2 bar, respectively. It was found experimentally that, at the highest temperature, a maximum jet velocity of around 1,500 m/s was obtained. At this temperature, a narrow pointed jet appeared while at the highest pressure, a thick, blunt headed jet was obtained. Strong shock waves were generated in both cases at the jet head. For analytical prediction, equations of jet tip velocity and penetration from the work of Dent and of Hiroyasu were employed to describe the dynamic characteristics of the experiments at a standard condition of 1 bar, 30 °C. These analytical predictions show reasonable agreement to the experimental results, the experimental trend differing in slope because of the effect of the pressure, density fluctuation of the injection and the shock wave phenomena occurring during the jet generation process.     

Heat transfer,pressure drop and flow patterns during flow boiling of R407C in a horizontal microfin tube

The heat transfer, pressure drop and flow patterns during flow boiling of R407C in a horizontal microfin tube have been investigated. The microfin tube is made of copper with a total fin number of 55 and a helix angle of 15°. The fin height is 0.24 mm and the inner tube diameter at fin root is 8.95 mm. The test tube is 1 m long. It is heated electrically. The experiments have been performed at saturation temperatures between −30°C and +10°C. The mass flux was varied between 25 and 300 kg/m²/s, the heat flux from 20,000 W/m² down to 1,000 W/m². The vapour quality was kept constant at 0.1, 0.3, 0.5, 0.7 at the inlet and 0.8, 1.0 at the outlet, respectively. The measured heat transfer coefficient is compared with the correlations of Cavallini et al., Shah as well as Zhang et al. Cavallini’s correlation contains seven experimental constants. After fitting these constants to our measured values, the correlation achieves good agreement. The measured pressure drop is compared to the correlations of Pierre, Kuo and Wang as well as Müller-Steinhagen and Heck. The best agreement is achieved with the correlation of Kuo and Wang. Almost all values are calculated within an accuracy of ±30%. The flow regimes were observed. It is shown, that changes in the flow regime affect the heat transfer coefficient significantly.     

Temperature dependence of the viscosity of highly starch-filled poly(hydroxy ester ether) biodegradable composites

 The temperature dependence of the viscosity of starch-filled poly(hydroxy ester ether) (PHEE) biodegradable composites was analyzed using Arrhenius and WLF equations. Corn starch/PHEE materials were extruded using a twin screw extruder with starch volume fractions from 0.27 to 0.66. Dynamic strain sweep measurements were carried out at 10 rad/s at six different temperatures from 100 °C to 150 °C. Both Arrhenius and WLF equations model equally well the temperature effect on viscosity of PHEE and starch/PHEE composites with starch volume fractions up to 0.36. Arrhenius equation with stress correction describes the stress dependence of viscosity of starch/PHEE composites with higher starch volume fractions. The activation energy using both Arrhenius equation and Arrhenius equation with stress correction is 62.7 kJ/mol for pure PHEE and starch/PHEE composites. Received: 10 September 1999 Accepted: 27 March 2000     

Free convection effects on the flow of water at 4°C past a semi-infinite inclined plate

Free convection flow of water at its maximum density past a semi-infinite inclined plate has been studied by using an implicit-finite difference technique. The steady-state velocity and temperature profiles, local and average skin friction and the Nusselt number are shown graphically. It is observed that velocity decreases owing to a fall in temperature of water from 20°C to 4°C.     

Aerodynamic force measurement using 3-component accelerometer force balance system in a hypersonic shock tunnel

A new three-component accelerometer force balance has been designed, calibrated and tested in hypersonic shock tunnel (HST2) of Indian Institute of Science. The newly designed balance is able to measure aerodynamic forces (within test time of one millisecond) on test models at angles of attack from 0 to 12°. Two models, a blunt cone with after body and a blunt cone with after body and frustum are used to establish the accuracy of the force balance. The tests were conducted for the above two configurations with a constant Mach number of 8 and total enthalpy of 2.0 MJ/kg. The effectiveness of the balance is demonstrated by comparing the forces and moments of measured data with AGARD models. The flow fields around the test model are simulated using a 3D axisymmetric Navier–Stokes solver and the simulated results were compared with the measured values. Measured and computed force data are matched within ±10% for two different models tested here. The accuracy of the force balance is also estimated with the Newtonian theory and the values are approximately ±10% for the axial component and ±8% for the normal and pitching moment components.      

Gesamtemissionsgrad von Schwärzen

With the method of measurement described in [1], the total emissivity of different black coatings was investigated with regard to their being used as total radiation standard in the temperature range from ?60 ° C to +180° C. The investigations showed that the mat varnish Nextel Velvet Coating 2010 black with an emissivity of 0.951 ± 0.5% is best suited for these purposes. Additional changes of the surface which can easily be made (sprinkling of Cu globules, etching) can increase the total emissivity by a further 0.7% or 1.6%, respectively.