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Fu Fang Xin Shan Xi Lin Fu Yu Jie Huade Pan Bernard Mahieu Marcel Gielen Franois Kayser Rudolph Willem 《无机化学与普通化学杂志》1994,620(6):1006-1010
1-Ethynyl-1-cyclohexanol reacts with a triaryltin hydride Ar3SnH (Ar = phenyl, p-tolyl) and generates the corresponding (Z)-1-[2-(triarylstannyl)vinyl]-1-cyclohexanol. The product obtained reacts with one or two equivalents of halogen (ICl or I2) to form the associated (Z)-1-[2-(diarylhalostannyl)-vinyl]-1-cyclohexanol or (Z)-1-[2-(aryldihalostannyl)vinyl]-1-cyclohexanol, respectively. All compounds were characterized by elemental analysis, 1H, 13C, 119Sn NMR and Mössbauer spectroscopy. 相似文献
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LI Wen-Ming WANG Jian-Guo ② GUO Wan-Cheng LI Zheng-Ming SONG Hai-Bin 《结构化学》2008,27(6):691-696
The title compounds (S)-methyl-2-(4-R-phenylsulfonamido)-3-(1H-indol-3- yl)propanoate (R = H (1), Cl (2)) have been synthesized and their crystal structures also have been determined by X-ray single-crystal diffraction. Compound 1 (C18H18N2O4S) belongs to orthorhombic, space group P212121 with a = 9.6348(14), b = 11.1517(17), c = 16.412(3) A, V = 1763.4(5) A^3, Mr = 358.40, Z = 4, De = 1.350 g/cm^3,/t = 0.209 mm^-1, F(000) = 752, R = 0.0348 and wR = 0.0714. Compound 2 (CI8H17ClN2O4S) crystallizes in orthorhombic, space group P212121 with a = 9.3128(14), b = 10.9655(16), c = 17.783(3) A, V = 1815.9(5) A^3, Mr = 392.85, Z = 4, De = 1.437 g/cm^3, p = 0.352 mm^-1, F(000) = 816, R = 0.0389 and wR = 0.0845. The absolute structure Flack parameters X of compounds 1 and 2 are -0.03(8) and -0.06(7), respectively. X-ray analysis reveals that the crystal structures of these two compounds both involve two intermolecular N-H…O hydrogen bond's. 相似文献
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SHING T. K. M. 《高等学校化学研究》1993,9(2):152-153
Two styryl-pyrones, (+)-goniotriol (1) and (+)-8-acetylgoniotriol (2), which are cytotoxic to human turnout cells, were isolated from the ethanolic extracts of the stem bark of Goniothalamus giganteus Hook. F., Thomas (Annonaceae), in addition (+)-goniotriol was also isolated from the leaves and twigs of Goniothalamus 相似文献
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