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According to intensity distribution of the synchrotron radiation source focused by a toroidal mirror at the Beijing synchrotron radiation biological macromolecule station, theoretical modeling of the Beijing synchrotron radiation source is developed for capillary optics. Using this theoretical modeling, the influences of the configuration curve of the polycapillary X-ray lens on transmission efficiency and working distance are analyzed. The experimental results of the transmission efficiency and working distance at the biological macromolecule station are in good agreement with the theoretical results. 相似文献
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Investigation of the topological shape of bovine serum albumin in solution by small-angle x-ray scattering at Beijing synchrotron radiation facility 下载免费PDF全文
This paper reports that at a newly constructed small-angle x-ray scattering station of Beijing Synchrotron Radia- tion Facility, the topological shape of ligand-free bovine serum albumin in solution has been investigated. An appropriate scattering curve is obtained and the calculated value of the gyration radius is 31.2~=t=0.25 ~_ (11=0.1 nm) which is co- incident with other ones' results. It finds that the low-resolution structure models obtained by making use of ab initio reconstruction methods are fitting the crystal structure of human serum albumin very well. All of these results perform the potential of the beamline to apply to structural biology studies. The characteristics, the defects, and the improving measures of the station in future are also discussed. 相似文献
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This article summarizes the developments of experimental techniques for high pressure x-ray diffraction(XRD) in diamond anvil cells(DACs) using synchrotron radiation. Basic principles and experimental methods for various diffraction geometry are described, including powder diffraction, single crystal diffraction, radial diffraction, as well as coupling with laser heating system. Resolution in d-spacing of different diffraction modes is discussed. More recent progress, such as extended application of single crystal diffraction for measurements of multigrain and electron density distribution, timeresolved diffraction with dynamic DAC and development of modulated heating techniques are briefly introduced. The current status of the high pressure beamline at BSRF(Beijing Synchrotron Radiation Facility) and some results are also presented. 相似文献
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高能X射线组合透镜是一种基于折射效应的新型X射线光学元件。报道了这种新型X射线光学元件聚焦性能的最新实验结果。设计的高能X射线组合透镜为聚甲基丙烯酸甲酯(PMMA)材料,包括40个相同的、顺序排布的平凹折射单元,折射单元的球面半径为200μm,组合透镜的几何口径约为500μm,长度约为8 mm,焦距约为1.3 m。简要描述了PMMA材料X射线组合透镜的制作技术和制作过程。并给出了X射线组合透镜聚焦性能测试实验系统和实验条件。最后给出8 keV单色X射线辐射下,PMMA材料X射线组合透镜的聚焦性能的测试结果,对实际测试结果进行了分析和讨论,得出结论,焦距等参量与理论计算结果基本吻合。 相似文献
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Fernando Sannibale Augusto Marcelli Plinio Innocenzi 《Journal of synchrotron radiation》2008,15(6):655-659
IKNO (Innovation and KNOwledge) is a proposal for a multi‐user facility based on an electron storage ring optimized for the generation of coherent synchrotron radiation (CSR) in the terahertz frequency range, and of broadband incoherent synchrotron radiation ranging from the IR to the VUV. IKNO can be operated in an ultra‐stable CSR mode with photon flux in the terahertz frequency region up to nine orders of magnitude higher than in existing third‐generation light sources. Simultaneously to the CSR operation, broadband incoherent synchrotron radiation up to VUV frequencies is available at the beamline ports. The main characteristics of the IKNO storage and its performance in terms of CSR and incoherent synchrotron radiation are described in this paper. The proposed location for the infrastructure facility is Sardinia, Italy. 相似文献
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A toroidal grating monochromator (TGM) based beamline was designed earlier and it is being setup on the 450 MeV Indus-1 synchrotron radiation source. This beamline operates in 40–1000 Å wavelength range and gives a moderate resolution (~500) at high throughput. Now-a-days, spherical gratings are giving very high resolution in some complex monochromators. We have evaluated the use of spherical gratings in the simple rotation mount of a TGM. The motivation has been to evaluate if the existing TGM beamline, without any hardware changes, can be used with the much cheaper spherical gratings. The two monochromators, employing toroidal and spherical gratings respectively, have been compared by performing detailed ray tracing calculations. Our study shows that, with the same mechanical hardware, a real spherical grating monochromator gives better performance compared to the conventional TGM with respect to the spectral resolution and the flux. Furthermore, for moderate resolution this improvement is realized even when the exit slit is not moved to keep the spherical grating in-focus. 相似文献
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本文主要介绍对X射线组合折射透镜的制作工艺误差对其聚焦性能影响的研究结果. 首先给出采用深度X射线光刻技术制作的PMMA材料圆柱面型X组合折射透镜的工艺测试结果,得出制作工艺误差值,定性分析制作工艺误差对X射线组合折射透镜聚焦性能的影响. 然后根据实际的制作工艺误差建模,给出详尽的理论分析和定量的理论模拟结果. 最后在北京同步辐射装置(BSRF)上,构建基于PMMA材料的圆柱面型X射线组合折射透镜的微束聚焦实验系统,实际测试了有明显工艺误差和尽量消除工艺误差的两种X射线组合折射透镜的聚焦性能,给出实测结果
关键词:
X射线组合折射透镜
制作工艺误差
X射线聚焦性能
同步辐射 相似文献
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The present study describes the potential of the synchrotron radiation based X-ray fluorescence spectroscopy technique for the rapid, sensitive, user friendly and simultaneous monitoring of the changes in the elemental profile of the wheat seedlings stressed by excess manganese (Mn). For this, X-ray fluorescence spectra of the leaves of the control and Mn treated wheat seedlings have been recorded by synchrotron radiation X-ray of energy 15?keV. The analyses of the recorded spectra show the presence of elements chlorine, potassium, calcium, manganese, iron, copper, nickel, and zinc. A calibration-free approach, PyMca has been used for the quantitative estimation of the detected elements in the leaves of the control and Mn treated wheat seedlings. The excess supply of Mn to wheat seedlings results in the accumulation of manganese in the leaves of the seedlings. The accumulation of manganese in wheat seedlings negatively affects the uptake and translocation of calcium, potassium, and iron while it has stimulating effect on the uptake of copper and zinc. 相似文献