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1.
Syntheses of 5,6-Diamino-1,3-Dihydrobenzo[<Emphasis Type="Italic">c</Emphasis>]thiophene 2,2-Dioxide
5,6-Diamino-1,3-dihydrobenzo[c]thiophene 2,2-dioxide was obtained by two methods from 5-amino-6-nitro- and 5-acylamino-1,3-dihydrobenzo[c]thiophene 2,2-dioxide.__________Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 522–523, April, 2005. 相似文献
2.
S. L. Bogza S. Yu. Suikov N. M. Bogdan Yu. A. Nikolyukin V. I. Dulenko 《Chemistry of Heterocyclic Compounds》2004,40(11):1421-1426
The recyclization reactions of 4-cyanobenzo[c]pyrylium salts with ammonia, primary amines, and hydrazines have been studied. New derivatives of isoquinoline, benzo-2,3-diazepine, and pyrazolo-[ 5,4-c]isoquinoline have been obtained.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, pp. 1645–1651, November, 2004. 相似文献
3.
T. E. Khoshtariya M. M. Matnadze N. T. Mirziashvili L. N. Kurkovskaya M. I. Sikharulidze T. O. Dzhashi 《Chemistry of Heterocyclic Compounds》2004,40(11):1454-1459
The Sandmeyer reaction was used to prepare 2,3-dioxo-2,3-dihydrobenzo[b]furoindoles which could be reduced with diborane or with complex hydrides to give the corresponding unsubstituted as well as the 3-hydroxybenzo[b]furoindoles.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No 11, pp. 1683–1689, November, 2004. 相似文献
4.
S. L. Bogza S. Yu. Suikov N. M. Bogdan K. I. Kobrakov 《Chemistry of Heterocyclic Compounds》2004,40(10):1300-1304
The reaction of 3-acylamino- and 3-alkoxybenzo[c]pyrilium perchlorates with hydrazine has been studied. It was discovered that the direction of the recyclization of the pyran ring depends on the type of substituent in position 3 and on the ratio of reactants. Derivatives of isoquinoline and benzo-2,3-diazepine were obtained.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No.10, pp. 1507–1511, October, 2004. 相似文献
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A. D. Dubonosov V. P. Rybalkin Ya. Yu. Vorob’eva V. A. Bren’ V. I. Minkin S. M. Aldoshin V. V. Tkachev A. V. Tsukanov 《Russian Chemical Bulletin》2004,53(10):2248-2252
It was shown by electron absorption spectroscopy and X-ray diffraction analysis that steric strains in photochromic 2-(N-acyl-N-arylaminomethylene) benzo[b]thiophen-3(2H)-one molecules ortho-substituted in the N-phenyl ring increase the quantum yield of the N→O photoinduced rearrangement in accord with an increase in the steric constant of the ortho-substituent.__________Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 10, pp. 2151–2155, October, 2004. 相似文献
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V. I. Terenin M. A. Butkevich A. P. Pleshkova 《Chemistry of Heterocyclic Compounds》2005,41(10):1327-1333
We have synthesized nitro derivatives of pyrrolo[1,2-a]pyrazines using a nitrating mixture and acetyl nitrate. We have obtained
the products of oxidation of the side chain of 1,6-substituted pyrrolo[1,2-a]-pyrazines.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 10, pp. 1579–1586, October, 2005. 相似文献
9.
A. T. Soldatenkov S. V. Volkov S. A. Soldatova 《Chemistry of Heterocyclic Compounds》2007,43(4):508-509
10.
V. S. Tolkunov Yu. B. Vysotsky O. A. Gorban’ S. V. Shishkina O. V. Shishkin V. I. Dulenko 《Chemistry of Heterocyclic Compounds》2005,41(4):515-525
We have studied the reactions of 3-arylaminobenzofuro-, 3-arylaminobenzothieno-, and 3-arylaminoindolo[2,3-c]pyrylium salts with ammonium acetate, primary amines, and hydrazine hydrate. In an alcoholic medium, primary amines and hydrazine hydrate open up the pyrylium ring to form arylamides of 2-(N-benzylmethylketimine)hetaryl-3-acetic acids or the corresponding hydrazones, where further heterocyclization does not occur. Upon treatment with ammonium acetate in acetic acid, 2-aryl-1-methylhetero[2,3-c]pyridin-3-(2H)-ones are formed along with their 2-unsubstituted analogs.__________Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 601–612, April, 2005. 相似文献
11.
Mohamed E. El-Sadek Mansour Aboukull Osama I. El-Sabbagh Hassan M. Shallal 《Monatshefte für Chemie / Chemical Monthly》2007,138(3):219-225
Summary.
Michael addition reaction of 3-(4-fluorophenylamino)-2-cyclohexenone and its 5,5-dimethyl derivative to the acrylonitrile derivatives
afforded the novel hexahydroquinolines. The target hexahydro-1H-pyrido[3,2-c]azepine derivatives were obtained via ring enlargement of the corresponding hexahydroquinolines under Schmedt conditions.
Some novel pyrido[3,2-c]azepines showed hypotensive activity in vivo on normotensive anaesthetized male adult albino rats and their effects on the ventricular contraction and auricular rate
of isolated rabbit hearts using Langendorff’s method and nefidipine as a reference drug were studied. Compounds 29 and 36 which bear some structural similarities to nefidipine exhibited the highest hypotensive activity and negative inotropic as
well as chronotropic activities. 相似文献
12.
N. V. Abramova S. M. Peregudova A. O. Emel’yanova A. P. Pleshkova V. I. Sokolov 《Russian Chemical Bulletin》2007,56(2):361-363
New cymantrenyl derivatives of 1-methyl[60]fullereno[c]pyrrolidine were obtained. According to electrochemical data, the cymantrenyl and phenyl fragments show close electron-donating
effects in the presence of the strong acceptor fullerene.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 2, pp. 349–351, February, 2007. 相似文献
13.
L. G. Voskressensky T. N. Borisova T. A. Vorob’eva A. I. Chernyshev A. V. Varlamov 《Russian Chemical Bulletin》2005,54(11):2594-2601
Reactions of substituted tetrahydropyrrolo[3,2-c]pyridines with dimethyl acetylenedicarboxylate in protic and aprotic solvents were studied. A novel single-step method for
the synthesis of pyrrolo[2,3-d]azocine derivatives was developed.
Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 11, pp. 2513–2519, November, 2005. 相似文献
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M. V. Vovk N. V. Mel’nichenko V. A. Sukach N. G. Chubaruk 《Chemistry of Heterocyclic Compounds》2004,40(11):1485-1489
6-Azido-1H-pyrazolo[3,4-b]pyridino-5-carbaldehydes react with aromatic amines to give the corresponding N-arylimines which cyclize on heating in boiling toluene to give 6-aryl-1,6-dihydrodipyrazolo[3,4-b:4,3-e]pyridines.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 11, 1717–1722, November, 2004. 相似文献
16.
J. Meuche-Albeny P. Rathelot M. P. Crozet P. Vanelle 《Chemistry of Heterocyclic Compounds》2003,39(8):989-997
5-Chloromethyl-6-nitrobenzo[1,3]dioxole has been shown to react with 2-nitropropane anion to give C-alkylation by an S
RN1 mechanism. The reaction was extended to various aliphatic, cyclic, and heterocyclic nitronate anions, leading to a new series of nitrobenzo[1,3]dioxole derivatives. 相似文献
17.
A. Šačkus E. Valaitytė V. Amankavičienė U. Berg C. Schicktanz K. Schlothauer 《Chemistry of Heterocyclic Compounds》2007,43(9):1118-1123
Condensation of 1-cyanomethyl-2,3,3-trimethyl-3H-indolium perchlorate with ortho-hydroxy-substituted aromatic aldehydes afforded
1-cyanomethylindoline spiropyrans. The latter underwent rearrangement to bridged 1,3-benzoxazepino[3,2-a]indoles on treatment
with a base. The mechanism of the rearrangement includes generation of a carbanion stabilized by a cyano group.
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 9, pp. 1322–1328, September, 2007. 相似文献
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Ahmad Shaabani Ebrahim Soleimani Maria Darvishi 《Monatshefte für Chemie / Chemical Monthly》2007,138(1):43-46
Summary. The three-component condensation of aldehyde, N,N′-dimethylbarbituric acid and alkyl or aryl isocyanide afforded the corresponding furo[2,3-d]pyrimidine-2,4(1H,3H)-diones in 1-butyl-3-methylimidazolium bromide as an ionic liquid in high yields at room temperature within several minutes. 相似文献
20.
Summary. Alkylation of Reissert compounds with certain benzoquinolizinone derivatives followed by hydrolytic cleavage afforded the core of the title compounds
in a two step sequence. Finally, the lactam intermediates were reduced with DIBAH giving the target compounds, the structural and stereochemical assignments of which were achieved by 13C NMR spectroscopy.
Part of PhD thesis, LMU München, D 相似文献