激光同步辐射作为阿秒X射线辐射源的特性研究

 研究了逆流相对论电子与激光脉冲相互作用获得激光同步辐射的频率上移、微分散射截面等特性。发现逆流相对论电子与短脉冲激光相互作用，可以获得阿秒X射线辐射脉冲。短脉冲激光条件下得到的后向散射光的频率上移与长脉冲激光条件下得到的后向散射光的频率上移是完全一致的，同时发现随着入射电子初始能量的增加，散射光的准直性越来越好，后向散射光脉冲的脉宽越来越短。     

高能电子在强激光场中的同步辐射获得超短X射线脉冲

 研究了逆流相对论高能电子与强激光脉冲相互作用的同步辐射过程,当电子具有合适的初速度且传播方向与激光的传播方向相反时,电子在激光脉冲中心作圆周运动。由于电子的运动半径比传统同步辐射环中电子的运动半径小几个数量级,因此电子的辐射能量大大增加。研究发现此过程可以获得阿秒和泽秒X射线脉冲;同时发现随着入射电子初能量的增加和激光能量的增强,获得X射线脉冲脉宽越来越短,强度越来越大。这使得激光同步辐射可以成为一种强大的短波长短脉宽的辐射光源。     

Polycapillary X-ray lens for the secondary focusing Beijing synchrotron radiation source

According to intensity distribution of the synchrotron radiation source focused by a toroidal mirror at the Beijing synchrotron radiation biological macromolecule station, theoretical modeling of the Beijing synchrotron radiation source is developed for capillary optics. Using this theoretical modeling, the influences of the configuration curve of the polycapillary X-ray lens on transmission efficiency and working distance are analyzed. The experimental results of the transmission efficiency and working distance at the biological macromolecule station are in good agreement with the theoretical results.     

第三代同步辐射光源X射线相干性测量研究

随着高性能第三代同步辐射光源的建成开放,基于X射线相干特性的实验方法得到了快速发展和广泛应用.作为一个典型的例子,X射线相位衬度成像已经成为常规的X射线实验方法并向用户开放.相干散射、相干衍射成像、光子关联谱等X射线实验方法正日益受到重视,在高空间分辨、时间分辨等研究领域已显示出其独特的优越性.因此,研究和测量第三代同步辐射的空间相干特性对进一步发展这些新的实验方法具有重要意义.基于Talbot自成像原理成功测量了上海光源X射线成像线站发射的X射线的空间相干长度,并进而测得了相应光源的空间尺度.光子能量为33.2 keV时,测得的X射线光束垂直方向空间相干长度为8.84μm,对应的光源尺寸为23μm,测量结果与理论分析相符.     

同步辐射X射线光源在高压科学研究中的应用

同步辐射X射线光源已经成功地应用到高压科学研究的诸多领域.文章简要回顾了同步辐射高压技术的发展历史,简要介绍了同步辐射X射线衍射技术在高压状态方程、强关联体系、地球内部物质以及早期生命起源等研究中的应用.介绍了同步辐射X射线光谱技术(包括晶格振动声子谱的测量)在高压研究中的应用,此外,还介绍了时间分辨的同步辐射技术在冲击压缩研究中的应用,最后展望了未来先进光源应用于高压科学研究的前景.     

基于同步辐射的快速扫描X射线微束荧光成像方法

在上海光源硬X射线微聚焦光束线站(BL15U1)上, 基于EPICS软件平台, 集成运动控制, 光强探测, 荧光探测等功能, 实现了"飞行"模式 (on-the-fly) X射线扫描微束荧光成像方法. 用"飞行"扫描X射线荧光成像法获得了标准镍网, 以及微量元素Cu, Zn,K, Fe在样品老鼠脾内的分布图像, 结果显示该方法不但在速度上有了极大的提高, 而且获得的元素分布图像具有高质量. 关键词： 快速扫描X射线微束荧光成像 同步辐射 微量元素分布     

Confocal three-dimensional micro X-ray fluorescence based on synchrotron radiation for mineral analysis

The confocal three-dimensional micro X-ray fluorescence using polycapillary optics and a synchrotron radiation was applied to nondestructively analyze elemental compositions of minerals, and thereby obtain the three-dimensional distributions of elements in the minerals. Such confocal micro X-ray fluorescence had potential applications in the mineral prospecting, identification of jades, differentiation of stones.     

X-ray synchrotron radiation in medium

Energy and angular distributions of X-ray synchrotron radiation produced by an ultra relativistic electron moving in a medium are discussed. Calculations show that the medium suppresses strongly the yield of the radiation for the electron Lorentz factor smaller than some cut-off value depending on the medium electron density and magnetic field applied.     

Investigation of craze development using small-angle X-ray scattering of synchrotron radiation

The development of crazes in polycarbonate was investigated with the method of ultra-small-angle X-ray scattering (USAXS) of synchrotron radiation. Measurements at different temperatures and with different draw rates were carried out. The two-dimensional scattering patterns were analyzed by means of a fibrillar model of the craze. The geometrical parameters of the craze as a function of the macroscopic draw ratio were determined by using a curve-fitting procedure. From the measured values of the diameter and the mean distance of the fibrils, it is possible to calculate the volume fraction v_f of the fibrils directly. Additional scattering caused by submicrocracks is discussed.     

X-ray lithography with synchrotron radiation

Manufactures of silicon integrated circuits increasingly rely on high resolution, high throughput, and litography techniques based on parallel mask projection. The once simple technique of projecting an image of a mask on a wafer, however, is now being replaced by more elaborate systems at an ever faster rate. Of the possible successors to photolithography in the production of structures smaller than 0.7 m, the most promising appears to be X-ray litography with synchrotron radiation. The development problems of this new technique are related to the mask technology, alignment systems, resist materials, and compact, low-cost storage rings.     

影响同步辐射X射线螺旋显微CT的若干因素研究

同步辐射X射线是扁平光, 传统显微CT难以对长样品实现快速、高分辨、低剂量三维成像, 螺旋扫描的引入可以很好地解决这一难题. 本文采用数字模拟和实验的方法较为系统地研究了螺距、光斑竖直高度和180° 投影数对成像质量、速度的影响. 模拟结果表明, 在螺距不大于2的前提下, 180° 投影数增大, 误差减小, CT成像速度变慢; 光斑竖直高度增大, 速度加快; 螺距增大, 速度加快, 且误差在允许范围内; 选取合适的参数值使旋转平移比为整数, 误差最小. 同时, 优化参数并在上海光源实现螺旋显微CT, 从实验上验证了模拟结果. 研究表明, 通过优化各参数, 同步辐射螺旋显微CT可以实现快速高质量三维成像, 为以后的实际应用提供了依据.     

同步辐射软X射线显微成像

软X射线显微成像是同步辐射最主要的应用之一,本文简明介绍软X射线显微成像的衬度机制,光源,成像方法和一些应用结果。     

X-ray magnetooptics based on synchrotron radiation

The conditions for obtaining a maximum magnetic signal in different experiment geometries have been analyzed on the basis of the general theory of reflection from a layered anisotropic medium. It is shown that, in the equatorial geometry in Bragg reflections from a periodic structure with antiferromagnetic interlayer ordering, amplification of linear dichroism arises, which can be observed even in the grazing geometry.     

用同步辐射X射线衍射技术分析GaN/Si外延膜的结构与应变

选用有AlN和AlGaN缓冲层的GaN/Si作为测试样品,采用同步辐射X射线衍射(SRXRD)技术对样品外延膜(GaN)的几何结构、晶格常量及其应变进行了分析.结果表明,同步辐射X射线衍射实验可以作为一种有效的技术手段,测试固体结构及应变.     

Investigation of nanostructured Fe3O4 polypyrrole core-shell composites by X-ray absorbtion spectroscopy and X-ray diffraction using synchrotron radiation

In this article, we focus on the structural peculiarities of nanosized Fe₃O₄ in the core-shell nanocomposites obtained by polymerization of conducting polypyrrole shell around Fe₃O₄ nanoparticles. The local structure of Fe atoms was determined from the Extended X-ray Absorption Fine Structure analysis using our own package computer programs. An X-ray diffraction method that is capable to determine average particle size, microstrains, as the particle size distribution of Fe₃O₄ nanoparticles is presented. The method is based on the Fourier analysis of a single X-ray diffraction profile using a new fitting method based on the generalized Fermi function facilities. The crystallites size obtained by X-ray diffraction spectra analysis was estimated between 3.2 and 10.3 nm. Significant changes in the first and the second Fe coordination shell in comparison with standard bulk were observed. The global and local structure of the nanosized Fe₃O₄ are correlated with the synthesis conditions of the core-shell polypyrrole nanocomposites.     

北京同步辐射装置上的位相衬度成像

在北京同步辐射装置上首次用位相衬度成像方法对生物样品和复合材料进行研究,得到了非常清晰而精细的材料内部细观结构.其图像的清晰度和分辨率明显地优于吸收衬度成像 关键词： 位相衬度成像 相干光源 同步辐射硬X射线     

Coplanar three-beam X-ray diffraction study in TeO<Subscript>2</Subscript> single crystal using synchrotron radiation

The results of the first experimental study of coplanar three-beam X-ray diffraction in a paratellurite (TeO₂) single crystal using synchrotron radiation on a Kurchatov synchrotron radiation source are presented. Four cases with (220, 371), (220, 464), (220, 370), and (110, 557) indices have been investigated. In all cases the change of the rocking curve shape of the weak reflection has been observed due to the multibeam interaction resulting in the appearance of two peaks in the reflection curve corresponding to two scattering mechanisms: amplitude and resonance. The origin of the insufficient resolution in the experiments has been considered. It has been shown that the obtained data correspond to the results of the computer simulation.     

Spatial and spectral characteristics of laser-field synchrotron radiation

The spatial and spectral characteristics of laser-field synchrotron radiation (LSR) are investigated. The results show that LSR is emitted normal to the laser axis and emission in the X-ray wavelength can be obtained by increasing the intensity of the laser pulse and the initial energy of the electron. The unique feature offered by the laser-field synchrotron radiation (LSR) makes them a promising compact source of light at shorter wavelengths.     

空间谐振式陀螺谐振腔的失调分析

为了克服平面谐振腔调节精度高、损耗大的困难,提出了一种新型空间谐振式陀螺的谐振腔结构。并利用光学变换矩阵和菲涅尔-基尔霍夫衍射积分公式建立数学模型,通过MATLAB仿真计算谐振腔各腔镜因失调引起的衍射损耗。计算结果表明当谐振腔边长为4cm,入射光束束腰半径为0.25mm时,凹面镜的曲率半径为0.397m,反射镜失调引起的衍射损耗近似为0,即失调对陀螺的性能没有影响。得到陀螺的极限灵敏度为1.54°/h。     

Diagnostics of gold-containing surgical-dressing materials with X-ray and synchrotron radiation

An analysis of biocompatible and antibacterial Au-gauze nanocomposites for medical purposes using X-ray and synchrotron radiation is conducted. The samples are produced by the modification of medical cotton gauze by Au organosol in isopropanol, which is synthesized via the metal-vapor method. The nanocomposites are examined with X-ray photoelectron spectroscopy, as well as with X-ray adsorption diffraction spectroscopy (EXAFS/XANES) and small-angle X-ray scattering using synchrotron radiation.