Erratum to: Experimental Investigation on Mechanical Behavior of Coarse Marble Under Six Different Loading Paths

A series of triaxial compression experiments were preformed for the coarse marble samples under different loading paths by the rock mechanics servo-controlled testing system. Based on the experimental results of complete stress-strain curves, the influence of loading path on the strength and deformation failure behavior of coarse marble is made a detailed analysis. Three loading paths (Paths I–III) are put forward to confirm the strength parameters (cohesion and internal friction angle) of coarse marble in accordance with linear Mohr-Coulomb criterion. Compared among the strength parameters, two loading paths (i.e. Path II by stepping up the confining pressure and Path III by reducing the confining pressure after peak strength) are suggested to confirm the triaxial strengths of rock under different confining pressures by only one sample, which is very applicable for a kind of rock that has obvious plastic and ductile deformation behavior (e.g. marble, chalk, mudstone, etc.). In order to investigate re-fracture mechanical behavior of rock material, three loading paths (Paths IV–VI) are also put forward for flawed coarse marble. The peak strength and deformation failure mode of flawed coarse marble are found depending on the loading paths (Paths IV–VI). Under lower confining pressures, the peak strength and Young’s modulus of damage sample (compressed until post-peak stress under higher confining pressure) are all lower compared with that of flawed sample; moreover mechanical parameter of damage sample is lower for the larger compressed post-peak plastic deformation of coarse marble. However under higher confining pressures (e.g. σ ₃ = 30 MPa), the axial supporting capacity and elastic modulus of damage coarse marble (compressed until post-peak stress under lower confining pressure) is not related to the loading path, while the deformation modulus and peak strain of damage sample depend on the difference of initial confining pressure and post-peak plastic deformation. The friction among crystal grains determines the strength behavior of flawed coarse marble under various loading paths. In the end, the effect of loading path on failure mode of intact and flawed coarse marble is also investigated. The present research provides increased understanding of the fundamental nature of rock failure under different loading paths.     

Experimental Investigation on Mechanical Behavior of Coarse Marble Under Six Different Loading Paths

A series of triaxial compression experiments were preformed for the coarse marble samples under different loading paths by the rock mechanics servo-controlled testing system. Based on the experimental results of complete stress-strain curves, the influence of loading path on the strength and deformation failure behavior of coarse marble is made a detailed analysis. Three loading paths (Paths I–III) are put forward to confirm the strength parameters (cohesion and internal friction angle) of coarse marble in accordance with linear Mohr-Coulomb criterion. Compared among the strength parameters, two loading paths (i.e. Path II by stepping up the confining pressure and Path III by reducing the confining pressure after peak strength) are suggested to confirm the triaxial strengths of rock under different confining pressures by only one sample, which is very applicable for a kind of rock that has obvious plastic and ductile deformation behavior (e.g. marble, chalk, mudstone, etc.). In order to investigate re-fracture mechanical behavior of rock material, three loading paths (Paths IV–VI) are also put forward for flawed coarse marble. The peak strength and deformation failure mode of flawed coarse marble are found depending on the loading paths (Paths IV–VI). Under lower confining pressures, the peak strength and Young’s modulus of damage sample (compressed until post-peak stress under higher confining pressure) are all lower compared with that of flawed sample; moreover mechanical parameter of damage sample is lower for the larger compressed post-peak plastic deformation of coarse marble. However under higher confining pressures (e.g. σ ₃?=?30 MPa), the axial supporting capacity and elastic modulus of damage coarse marble (compressed until post-peak stress under lower confining pressure) is not related to the loading path, while the deformation modulus and peak strain of damage sample depend on the difference of initial confining pressure and post-peak plastic deformation. The friction among crystal grains determines the strength behavior of flawed coarse marble under various loading paths. In the end, the effect of loading path on failure mode of intact and flawed coarse marble is also investigated. The present research provides increased understanding of the fundamental nature of rock failure under different loading paths.     

Strength and deformation behaviors of veined marble specimens after vacuum heat treatment under conventional triaxial compression

The mechanical behaviors of rocks affected by high temperature and stress are generally believed to be significant for the stability of certain projects involving rocks, such as nuclear waste storage and geothermal resource exploitation. In this paper, veined marble specimens were treated to high temperature treatment and then used in conventional triaxial compression tests to investigate the effect of temperature, confining pressure, and vein angle on strength and deformation behaviors. The results show that the strength and deformation parameters of the veined marble specimens changed with the temperature, presenting a critical temperature of 600℃. The triaxial compression strength of a horizontal vein(β = 90°) is obviously larger than that of a vertical vein(β = 0°). The triaxial compression strength,elasticity modulus, and secant modulus have an approximately linear relation to the confining pressure. Finally,Mohr–Coulomb and Hoek–Brown criteria were respectively used to analyze the effect of confining pressure on triaxial compression strength.     

Experimental analysis of concrete behavior under high confinement: Effect of the saturation ratio

This study focuses on the identification of concrete behavior under severe triaxial loading in order to better evaluate the vulnerability of sensitive infrastructure to near-field detonations or ballistic impacts. For the purpose of reproducing high stress levels with well-controlled loading paths, static tests have been conducted on concrete samples using a triaxial press offering very high capacities (stress levels of around 1 GPa). It is a well-known fact that the concrete drying process is a slow phenomenon. Massive concrete structures, such as bridge piers, dams and nuclear reactors, could retain a quasi-saturated core throughout most of their lifetime, even though their facing dries very quickly. The objective of this article is to evaluate the effect of the saturation ratio on concrete behavior under high confinement; this article will present triaxial test results on concrete samples over a saturation ratio range extending from dried to quasi-saturated concretes. The subsequent analysis of results will show that the saturation ratio exerts a major influence on concrete behavior, particularly on both the concrete strength capacity and shape of the limit state curve for saturation ratios above 50%. This analysis also highlights that while the strength of dried concrete strongly increases with confining pressure, it remains constant over a given confining pressure range for either wet or saturated samples.     

High strain-rate behavior of ice under uniaxial compression

In the present study, a modified split Hopkinson pressure bar (SHPB) is employed to investigate the dynamic response of ice under uniaxial compression in the range of strain rates from 60 to 1400 s^?1 and at initial test temperatures of ?10 and ?30 °C. The compressive strength of ice shows positive strain-rate sensitivity over the range of strain rates employed; a slight influence of ice microstructure is observed, but it is much less than that reported previously for ice deformation under quasi-static loading conditions [Schulson, E.M., IIiescu, D., Frott, A., 2005. Characterization of ice for return-to-flight of the space shuttle. Part 1 – Hard ice. NASA CR-2005-213643-Part 1]. Specimen thickness, within the range studied, was found to have little or no effect on the peak (failure) strength of ice, while lowering the test temperature from ?10 to ?30 °C had a considerable effect, with ice behaving stronger at the lower test temperature. Moreover, unlike in the case of uniaxial quasi-static compression of ice, the effect of specimen end-constraint during the high rate compression was found to be negligible. One important result of these experiments, which may have important implications in modeling ice impacts, involves the post “peak-stress” behavior of the ice in that the ice samples do not catastrophically lose their load carrying capacity even after the attainment of peak stress during dynamic compression. This residual (tail) strength of the damaged/fragmented ice is sizable, and in some cases is larger than the quasi-static compression strength reported for ice. Moreover, this residual strength is observed to be dependent on sample thickness and the strain rate, being higher for thinner samples and at higher strain-rates during dynamic compression.     

Numerical study on coalescence of two pre-existing coplanar flaws in rock

Crack propagation and coalescence processes are the fundamental mechanisms leading to progressive failure processes in rock masses, in which parallel non-persistent rock joints are commonly involved. The coalescence behavior of the latter, which are represented as pre-existing coplanar flaws (cracks), is numerically investigated in the present study. By using AUTODYN as the numerical tool, the present study systematically simulates the coalescence of two pre-existing coplanar flaws in rock under compression. The cumulative damage failure criterion is adopted in the numerical models to simulate the cumulative damage process in the crack initiation and propagation. The crack types (shear or tensile) are identified by analyzing the mechanics information associated with the crack initiation and propagation processes. The simulation results, which are generally in a good accordance with physical experimental results, indicate that the ligament length and the flaw inclination angle have a great influence on the coalescence pattern. The coalescence pattern is relatively simple for the flaw arrangements with a short ligament length, which becomes more complicated for those with a long ligament length. The coalescence trajectory is composed of shear cracks only when the flaw inclination angle is small (such as β ? 30°). When the pre-existing flaws are steep (such as β ? 75°), the coalescence trajectory is composed of tensile cracks as well as shear cracks. When the inclination angle is close to the failure angle of the corresponding intact rock material, and the ligament length is not long (such as L ? 2a), the direct shear coalescence is the more favorable coalescence pattern. In the special case that the two pre-existing flaws are vertical, the model will have a direct tensile coalescence pattern when the ligament length is short (L ? a), while the coalescence between the two inner flaw tips is not easy to achieve if the ligament length is long (L ? 2a).     

Relating inhomogeneous deformation to local texture in zirconium through grain-scale digital image correlation strain mapping experiments

The effect of local texture on inhomogeneous plastic deformation is studied in zirconium subjected to uniaxial compression. Cross-rolled commercially pure Zr 702 plate that had a strong basal (0 0 0 1) texture through the plate thickness, and a non-basal texture in cross-section, was obtained. At a compressive strain rate of 1 s^?1, samples loaded either in the through-thickness or in-plane directions exhibited significant differences in yield strength, hardening response and failure mechanisms. These macroscopic differences are related to microstructural features by combining information from electron backscattered diffraction with real time in situ imaging and subsequent full-field strain measurements obtained using digital image correlation. Experimental results indicate that the through-thickness loaded zirconium samples, which show a strong basal-texture in the loading direction, do not deform homogeneously – implying the lack of a representative volume element. The detailed surface deformation fields provided by digital image correlation allow for a qualitative and quantitative analysis of the relationship between grain orientation and patterns of deformation bands that form as the precursors to development of an adiabatic shear band in the through-thickness loaded sample. For the in-plane loaded samples, inhomogeneities still exist at the microscale, but the collective behavior of several grains leads to a homogeneous response at the macroscale. It is observed that local texture for hcp polycrystals, which are significantly slip restricted, can directly affect both local and global response, even at low to moderate plastic strains.     

Experimental study on the compressive behaviors of CFRP tube-encased concrete columns

Nine square concrete columns including 6 CFRP/ECCs and 3 concrete columns are prepared, which have cross-section of 200 mm × 200 mm and height of 600 mm. The CFRP tubes with fibers oriented at hoop direction were manufactured to have 3 or 5 layers of CFRP with 10 mm, 20 mm, or 40 mm rounding corner radii at vertical edges. A 100 mm overlap in the direction of fibers was provided to ensure proper bond. Uniaxial compression tests were conducted to investigate the compressive behavior. It is evident that the CFRP tube confinement can improve the behavior of concrete core, in terms of axial compressive strength or axial deformability. Test results show that the stress-strain behavior of CFRP/ECCs vary with different confinement parameters, such as the number of confinement layers and the rounding corner radius.     

Pressure and friction dependent mechanical strength – cracks and plastic flow

The mechanical properties of a polymer composite plastic bonded explosive, EDC37, have been investigated as a function of hydrostatic confining pressure between 0.1 and 138 MPa. The results indicate different failure processes in two pressure ranges, a low pressure range between about 0.1 and 7 MPa and a higher pressure range between about 7 and 138 MPa. In the low pressure range slow crack processes are important in failure while in the higher pressure range plastic flow dominates. The pressure dependence of the compressive strength in the low pressure range is attributed to coulomb friction between surfaces of closed shear cracks and from the observed linear increase of the strength with pressure and the angle of the fracture plane a friction coefficient is obtained. Friction coefficients can also be obtained from the ratio of the compressive to tensile strength and directly from the above angle. The friction coefficients obtained from these separate observations are in agreement and this is taken as strong evidence for the importance of this friction in determining strength and mechanical failure. These results clearly establish experimentally the role of friction in determining strength with or without applied pressure. An empirical relationship between strength, pressure and strain rate is also obtained for this pressure range and the failure strength of EDC37 is more sensitive to pressure than strain rate.     

Integral-based constitutive equation for rubber at high strain rates

High-speed experiments were conducted to characterize the deformation and failure of Styrene Butadiene Rubber at impact rates. Dynamic tensile stress–strain curves of uniaxial strip specimens and force–extension curves of thin sheets were obtained from a Charpy tensile impact apparatus. Results from the uniaxial tension tests indicated that although the rubber became stiffer with increasing strain rates, the stress–strain curves remained virtually the same above 280 s⁻¹. Above this critical strain rate, strength, fracture strain and toughness decreased with increasing strain rates. When strain rates were below 180 s⁻¹, the initial modulus, tensile strength and breaking extension increased as the strain rate increased. Between strain rates of 180 and 280 s⁻¹, the initial modulus and tensile strength increased with increasing strain rates but the extension at break decreased with increasing strain rates. A hyper-viscoelastic constitutive relation of integral form was used to describe the rate-dependent material behavior of the rubber. Two characteristic relaxation times, 5 ms and 0.25 ms, were needed to fit the proposed constitutive equation to the data. The proposed constitutive equation was implemented in ABAQUS Explicit via a user-defined subroutine and used to predict the dynamic response of the rubber sheets in the experiments. Numerical predictions for the transient deformation and failure of the rubber sheet were within 10% of experimental results.     

The high strain mechanical response of the wet Kelvin model for open-cell foams

Surface Evolver software was used to create the three-dimensional geometry of a Kelvin open-cell foam, to simulate that of polyurethane flexible foams. Finite Element Analysis (FEA) with 3D elements was used to model large compressive deformation in the [0 0 1] and [1 1 1] directions, using cyclic boundary conditions when necessary, treating the polyurethane as an elastic or elastic–plastic material. The predicted foam Young’s moduli in the [0 0 1] direction are double those of foams with uniform Plateau border cross-section edges, for the same foam density and material properties. For compression in the [1 1 1] direction, the normalized Young’s modulus increases from 0.9 to 1.1 with foam relative density, and the predicted stress–strain relationship can have a plateau, even for a linearly-elastic polymer. As the foam density increases, the predicted effects of material plasticity become larger. For foam of relative density 0.028, edge-to-edge contact is predicted to occur at a 66% strain for [1 1 1] direction compression. The foam is predicted to contract laterally when the [1 1 1] direction compressive strain exceeds 25%.     

Spall strength of glass fiber reinforced polymer composites

In the present paper results of a series of plate impact experiments designed to study spall strength in glass–fiber reinforced polymer composites (GRP) are presented. Two GRP architectures are investigated—S2 glass woven roving in Cycom 4102 polyester resin matrix and a balanced 5-harness satin weave E-glass in a Ciba epoxy (LY564) matrix. The GRP specimens were shock loaded using an 82.5 mm bore single-stage gas-gun. A velocity interferometer was used to measure the particle velocity profile at the rear (free) surface of the target plate. The spall strength of the GRP was obtained as a function of the normal component of the impact stress and the applied shear-strain by subjecting the GRP specimens to normal shock compression and combined shock compression and shear loading, respectively. The spall strengths of the two GRP composites were observed to decrease with increasing levels of normal shock compression. Moreover, superposition of shear-strain on the normal shock compression was found to be highly detrimental to the spall strength. The E-glass reinforced GRP composite was found to have a much higher level of spall strength under both normal shock compression and combined compression and shear loading when compared to the S2-glass GRP composite. The maximum spall strength of the E-glass GRP composite was found to be 119.5 MPa, while the maximum spall strength for the S2 glass GRP composite was only 53.7 MPa. These relatively low spall strength levels of the S2-glass and the E-glass fiber reinforced composites have important implications to the design and development of GRP-based light-weight integral armor.     

Dynamic response and energy dissipation characteristics of balsa wood: experiment and analysis

Dynamic response of a cellular sandwich core material, balsa wood, is investigated over its entire density spectrum ranging from 55 to 380 kg/m³. Specimens were compression loaded along the grain direction at a nominal strain rate of 3 × 10³ s⁻¹ using a modified Kolsky (split Hopkinson) bar. The dynamic data are discussed and compared to those of quasi-static experiments reported in a previous study (Mech. Mater. 35 (2003) 523). Results show that while the initial failure stress is very sensitive to the rate of loading, plateau (crushing) stress remains unaffected by the strain rate. As in quasi-static loading, buckling and kink band formation were identified to be two major failure modes in dynamic loading as well. However, the degree of dynamic strength enhancement was observed to be different for these two distinct modes. Kinematics of deformation of the observed failure modes and associated micro-inertial effects are modeled to explain this different behavior. Specific energy dissipation capacity of balsa wood was computed and is found to be comparable with those of fiber-reinforced polymer composites.     

Micro-scale behavior of granular materials during cyclic loading

This study presents the micro-scale behavior of granular materials under biaxial cyclic loading for different confining pressures using the two-dimensional (2D) discrete element method (DEM). Initially, 8450 ovals were generated in a rectangular frame without any overlap. Four dense samples having confining pressures of 15, 25, 50, and 100 kPa were prepared from the initially generated sparse sample. Numerical simulations were performed under biaxial cyclic loading using these isotropically compressed dense samples. The numerical results depict stress–strain–dilatancy behavior that was similar to that observed in experimental studies. The relationship between the stress ratio and dilatancy rate is almost independent of confining pressures during loading but significantly dependent on the confining pressures during unloading. The evolution of the coordination number, effective coordination number and slip coordination number depends on both the confining pressures and cyclic loading. The cyclic loading significantly affects the microtopology of the granular assembly. The contact fabric and the fabric-related anisotropy are reported, as well. A strong correlation between the stress ratio and the fabric related to contact normals is observed during cyclic loading, irrespective of confining pressures.     

Comment on “Stress boundary conditions for plate bending” by F.Y.M. Wan [Int. J. Solids Struct. 40 (2003) 4107–4123]

By using the reciprocal theorem of elasticity, the author obtained the appropriate stress boundary conditions for the Levy solution for plate bending accurate to all order for plates of general edge geometry and loading. Two special cases of k = 0 (axisymmetric deformation of a circular plate) and k ⩾ 2 (unsymmetric deformation of a circular plate) were discussed in detail in the paper.     

Interaction between Weibull parameters and mechanical strength reliability of industrial-scale water gas shift catalysts

A fundamental step in the production of an industrial catalyst is its crushing strength assessment. Limited literature exists in which the strength reliability of supported catalysts is investigated from production to their application in a reactor. In this work, cylindrical supports were prepared by pelletizing high porosity γ-alumina powder, and Cu–Zn/γ-Al₂O₃ catalysts were prepared by impregnation of the pelletized γ-alumina supports with an aqueous solution of copper and zinc nitrates. The support-forming variables, such as binder concentration, compaction pressure, calcination temperature, and drying procedure were investigated. The Weibull method was used to analyze the crushing strength data of the supports, and the fresh and used catalysts before and after the low-temperature water gas shift reaction. Support formation at a 50 wt% binder concentration, 1148 MPa compaction pressure, 500 °C calcination temperature, and rapid drying (100 °C, 8 h) led to the maximum support mechanical reliability. The most reliable catalyst with respect to simultaneous appropriate catalytic performance and mechanical strength was prepared from a support with the lowest mean crushing strength (26.25 MPa). This work illustrates the importance of the Weibull modulus as a useful mechanical reliability index in manufacturing a supported solid catalyst.     

In-plane free vibration of a single-crystal silicon ring

In this paper the natural frequencies and the associated mode shapes of in-plane free vibration of a single-crystal silicon ring are analyzed. It is found that the Si(1 1 1) ring is two-dimensionally isotropic in the (1 1 1) plane for elastic constants but three-dimensionally anisotropic, while the Si(1 0 0) ring is fully anisotropic. Hamilton’s principle is used to derive the equations of vibration, which is a set of partial differential equations with coefficients being periodic in polar variable. Expressing the radial and tangential displacements in sinusoidal form with non-predetermined amplitudes, and through the integration with respect to the circumferential variable, the original governing equations in partial differential form can be converted into the amplitude equations in ordinary differential form. The exact expressions for frequencies and mode shapes are obtained. It is found that for Si(1 0 0) rings the frequencies of a pair of modes, which are equal for an isotropic ring, split due to the anisotropic effect only for the second in-plane vibration mode. The phenomena of frequency splitting and degenerate modes can be proved either based on the conservation of averaged mechanical energy or by the concept of crystallographic symmetry groups. When the single-crystal silicon is replaced by the polycrystalline silicon, which is isotropic in elastic constants, the derived equations for frequencies correctly predict the vanishing of the phenomenon of frequency splitting.     

A micro–macro method for predicting the shear strength of brittle rock under compressive loading

Microcracks have great significance for shear strength of brittle rock in compression. A major challenge of this area is to establish the correlation of microcracks and macroscopic shear strength. A new micro–macro method is presented to predict the shear strength of brittle rock in compression. This method incorporates the microcrack model suggested by Ashby, Mohr–Coulomb failure criterion and a crack-strain relation. This crack–strain relation is presented to link the crack growth and axial strain by combining the micro and macro definitions from rock damage. The shear strength and stress–strain relationship of Jinping marble are theoretically investigated in detail. The rationality of this suggested method is verified by using the experimental results founded on Jinping marble. Effects of the initial microcrack size, friction coefficient and confining pressure on internal friction angle, cohesion, and shear strength are also discussed.     

Surface characteristics of spruce veneers and shear strength of plywood as a function of log temperature in peeling process

The objective of this study was to determine the effect of temperature of spruce (Picea orientalis L.) logs during peeling process on surface roughness, adhesive wettability, colour variation of veneer, and shear strength of plywood made from these veneer sheets. Veneer samples were manufactured from the logs after they were kept for 3 h and 24 h to reach to average temperatures of 52 °C and 32 °C, respectively. A fine stylus method was used for surface roughness evaluation of the veneer produced from two types of the logs and it was found that the samples peeled from the logs with a temperature of 52 °C had significantly better roughness values than those of manufactured from the logs with 32 °C at a 95% confidence level. Wettability of veneer samples was determined with contact angle measurements according to the sessile drop method. Urea formaldehyde (UF) and phenol formaldehyde (PF) resin drops were used in contact angle measurements. Contact angles of PF resin drops on veneers were similar for each peeling temperature while the contact angles of UF glue resin on veneers produced from the logs with 32 °C were lower than those of produced from the logs with 52 °C. Small colour difference was measured (indicated by a low ΔE value) on veneer samples depending on the log temperature. The highest shear strength value was determined for the plywood manufactured from veneers obtained from the logs with 52 °C by using UF glue.     

Flow of dilute to semi-dilute polystyrene solutions through a benchmark 8:1 planar abrupt micro-contraction

We have studied the flow of thermodynamically ideal solutions of a high molecular weight (M_w = 6.9 MDa) atactic polystyrene in the θ solvent dioctyl phthalate (aPS in DOP) through a micro-fabricated 8:1 planar abrupt contraction geometry. The channel is much deeper than most micro-scale geometries, providing an aspect ratio of 16:1 and a good approximation to 2D flow in the narrow channel. The solutions span a range of concentration 0.03 wt.% < c < 0.6 wt.%, encompassing the dilute to semi-dilute regimes and providing a range of fluid viscosities and relaxation times such that we achieve a range of Weissenberg numbers (8.7 < Wi < 1562) and Reynolds numbers (0.07 < Re < 11.2), giving elasticity numbers between 31 < El < 295. We study the flow using a combination of micro-particle image velocimetry (μ-PIV) to characterize the flow field, pressure measurements to evaluate the non-Newtonian viscosity, and birefringence measurements to assess macromolecular strain. Flow field observations reveal three broad flow regimes characterized by Newtonian-like flow, unstable flow and vortex growth in the upstream salient corners. Transitions between the flow regimes scale with Wi, independent of El, indicating the dominance of elastic over inertial effects in all the fluids. Transitions in the flow field are also reflected by transitions in the relative viscosity (determined from the pressure drop) and the macromolecular strain (determined from birefringence measurements). The strain through the 8:1 contraction saturates at a value of ～4–5 at high Wi. The results of these experiments broaden the limited set of literature on flow through micro-fluidic planar contractions and should be of significant value for optimizing lab-on-a-chip design and for comparison with modeling studies with elasticity dominated fluids.