共查询到20条相似文献,搜索用时 78 毫秒
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David Cáceres-CastilloRubén M. Carballo Jorge A. Tzec-InteriánGonzalo J. Mena-Rejón 《Tetrahedron letters》2012,53(30):3934-3936
2-Amino-4-arylthiazoles were prepared in a one-pot solvent-free procedure by reaction of p-substituted acetophenones with thiourea and iodine under microwave irradiation. 相似文献
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Kasmi-Mir S Djafri A Paquin L Hamelin J Rahmouni M 《Molecules (Basel, Switzerland)》2006,11(8):597-602
A rapid and easy solvent free one-pot synthesis of 5-arylidene-2-imino-4-thiazolidinones by condensation of the thioureas with chloroacetic acid and an aldehyde under microwave-irradiation is described. 相似文献
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<正>A facile and efficient method for the preparation of 2-non-substituted quinoline-4-carboxylic acids is described via the Pfitzinger reaction of isatins with sodium pyruvate following consequent decarboxylation under microwave irradiation. 相似文献
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[formula: see text] 4-Aryl phenylalanines were prepared as free amino acids from the Suzuki coupling of 4-borono phenylalanine with aryl halides in high yields within 5-10 min under microwave irradiation. 相似文献
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Seijas JA Vázquez-Tato MP Carballido-Reboredo R 《The Journal of organic chemistry》2005,70(7):2855-2858
[reaction: see text] Eco-friendly direct solvent-free synthesis of flavones is achieved by microwave irradiation of phloroglucinol and beta-ketoesters. Heating with microwaves versus under classical conditions was shown to be higher yielding, cleaner, and faster. The reaction goes through a cycloaddition of an alpha-oxo ketene intermediate followed by an uncatalyzed thermal Fries rearrangement. 相似文献
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[reaction: see text]. Alpha-carbolines are interesting core structures for designing DNA-interacting small molecules. However, these compounds are not commercially available and their synthetic methods are low yielding or time consuming. The shortest synthetic route, the modified Graebe-Ullmann reaction, has been optimized by using microwave heating in four different types of apparatus to give shorter reaction times and enhanced yields. Optimized conditions enabled the preparation of a small library of alpha-carbolines. 相似文献
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分别以无水氯化锌、对甲苯磺酸为催化剂,采用微波辐射法,在无溶剂条件下由4-氯间苯二酚与三氟乙酰乙酸乙酯缩合制备标题化合物;优化了反应条件.结果表明,在微波辐射下,无水氯化锌对该反应有较好的催化活性,相应的4-三氟甲基-7-羟基-6-氯香豆素的产率可达73.0%.优化的反应条件为:4-氯间苯二酚、三氟乙酰乙酸乙酯和无水ZnCl2的摩尔比为1∶1.1∶0.9,微波辐射功率800W,辐射时间20min,反应温度85℃. 相似文献
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A new and efficient method for the synthesis of multi-substituted oxazoles from various carbonyl compounds has been developed using sequential treatment of carbonyl compounds with HDNIB and amides such as acetamide or benzamide under solvent-free microwave irradiation conditions. 相似文献