Increase in the efficiency of energy injection into discharge plasma and the luminous efficiency of luminescent lamps during high-frequency pumping

It is experimentally justified for the first time that electrodeless induction pump of plasma of standard cylindrical luminescent lamps provides optimization of the high-frequency inductive–capacitive (HFI) discharge conditions. The acceptable frequency range and the effect of the capacitance between the inductor and plasma on the efficiency of resonant energy injection into discharge plasma are revealed. An increase in the luminous efficiency to 25% in the range of pump powers multiple of the lowest nominal power for the lamp under standard operating conditions is detected. Physics of the found phenomenon and the range of application of the power saving technology for electrodeless pumping of luminescent lamps with increased operation life are discussed.     

Impact of pulsed ultrasound on bacteria reduction of natural waters

There is a limited work on the use of pulsed ultrasound for water disinfection particularly the case of natural water. Hence, pulsed ultrasound disinfection of natural water was thoroughly investigated in this study along with continuous ultrasound as a standard for comparison. Total coliform measurements were applied to evaluate treatment efficiency. Factorial design of 2³ for the tested experimental factors such as power, treatment time and operational mode was applied. Two levels of power with 40% and 70% amplitudes, treatment time of 5 and 15 min and operational modes of continuous and pulsed with On to Off ratio (R) of 0.1:0.6 s were investigated. Results showed that increasing power and treatment time or both increases total coliform reduction, whereas switching from continuous to pulsed mode in combination with power and treatment time has negative effect on total coliform reduction. A regression model for predicting total coliform reduction under different operating conditions was developed and validated. Energy and cost analyses applying electrical and calorimetric powers were conducted to serve as selection guidelines for the choosing optimum parameters of ultrasound disinfection. The outcome of these analyses indicated that low power level, short treatment time, and high R ratios are the most effective operating parameters.     

绝对吸收式激光能量计高准确度校准技术研究

采用量热法的高能激光能量计用于测量能量大于50 kJ的连续波高能激光能量,通常用已知功率的连续激光开展激光能量计的光电校准需要激光照射时间超过20 min,而由于热损失等原因,进行长时间激光能量校准时,校准不确定度高达12%。以量热式平面吸收高能激光能量计为模型,从理论上分析了热辐射、热对流对连续波高能激光能量测量结果的影响,得到了较准确的平面吸收腔激光能量计冷却数学模型,实现了能量计热损失补偿,并通过建立相应的实验装置验证了该模型,用其对装置的测量结果加以修正,可使光电校准的测量不确定度减小到1%以下。     

Design of the Upgraded TJ-II Quasi-optical Transmission Line

TJ-II plasma start-up and heating are made by electron cyclotron resonance waves at the second harmonic of the electron cyclotron frequency. Two quasi-optical transmission lines transmit the microwave power of the gyrotrons to the vacuum vessel. The first line launches the microwave power under fixed injection geometry, i.e. there is no possibility to change the launching angle and the wave polarization. The second line has a moveable mirror installed inside the TJ-II vessel. To get high absorption efficiency and a narrow energy deposition profile the internal mirror focuses the wave beam at plasma center.To get more flexibility in the experiments on heating and current drive the first transmission line needs to be upgraded. The design is presented in this paper. The new launching antenna includes an internal mirror to focus the beam and to change the injection angle. Both launchers are then symmetrical. A polarizer consisting of two corrugated mirrors is used to get any wave polarization. Two mirrors with an array of coupling holes and calorimetric measurements of the energy absorbed in the barrier window allow the estimation of the microwave power launched into the TJ-II.     

Characterization of an atmospheric pressure plasma jet for surface modification and thin film deposition

In this paper, an experimental study is presented to characterize a commercially available atmospheric pressure plasma jet (APPJ) kINPen which can be used for local surface modification, e.g. changing the wettability as well as for thin film deposition with silicon-organic and metal-organic precursors to enhance scratch resistance or to lower the gas permeability. Characterization of the jet discharge has been carried out by three methods: (i) measurement of the energy influx from the jet plasma to a substrate by a calorimetric probe, (ii) spatial resolved investigation of the plasma beam by optical emission spectroscopy (OES) and (iii) observation of the plasma jet by video imaging. The deposited SiO _x and AlO _x films were analyzed by XPS measurements.     

Measurement of the Hydrodynamic Efficiency of Laser Plasma at the “Kanal-2” Installation using Aluminum and Copper Targets

The results of experimental measurements of the hydrodynamic efficiency of laser plasma for aluminum and copper targets are presented. The studies were performed on the “Kanal-2” laser setup system using the ballistic pendulum method. The pressure in the interaction chamber was 10^?4 Torr, the pendulum length was 145 mm, the mass of the pendulum with a target was 7.2 g. At the half-height pulse duration of 2.5 ns, the power density on the target surface was ～10¹³ W/cm². In the case of aluminum target, the hydrodynamic efficiency coefficient increased from 1.5% to 4.5% with increasing laser pulse energy from 5 J to 10 J, whereas it remained at the level of 5% for the copper target.     

Ultra‐thin optical grade scCVD diamond as X‐ray beam position monitor

Results of measurements made at the SIRIUS beamline of the SOLEIL synchrotron for a new X‐ray beam position monitor based on a super‐thin single crystal of diamond grown by chemical vapor deposition (CVD) are presented. This detector is a quadrant electrode design processed on a 3 µm‐thick membrane obtained by argon–oxygen plasma etching the central area of a CVD‐grown diamond plate of 60 µm thickness. The membrane transmits more than 50% of the incident 1.3 keV energy X‐ray beam. The diamond plate was of moderate purity (～1 p.p.m. nitrogen), but the X‐ray beam induced current (XBIC) measurements nevertheless showed a photo‐charge collection efficiency approaching 100% for an electric field of 2 V µm^?1, corresponding to an applied bias voltage of only 6 V. XBIC mapping of the membrane showed an inhomogeneity of more than 10% across the membrane, corresponding to the measured variation in the thickness of the diamond plate before the plasma etching process. The measured XBIC signal‐to‐dark‐current ratio of the device was greater than 10⁵, and the X‐ray beam position resolution of the device was better than a micrometer for a 1 kHz sampling rate.     

Magnetic properties of the ferrimagnetic glass-ceramics for hyperthermia

Magnetic materials play a key-role in magnetic induction hyperthermia for the treatment of cancer. In this paper, we analyse the magnetic properties of ferrimagnetic glass-ceramics with the composition in the system SiO₂–Na₂O–CaO–P₂O₅–FeO–Fe₂O₃, as a function of the melting temperature. These materials were obtained by melting of commercial reagents in the temperature range of 1400–1550 °C. Room-temperature magnetic measurements were performed by means of a vibrating sample magnetometer at room temperature. The power loss was determined from calorimetric measurements, using a magnetic induction furnace. The highest power loss (61 W/g) has been obtained for samples melted at 1500 °C. The heat generation of the ferrimagnetic glass-ceramics prepared by two different synthesis methods (traditional melting and coprecipitation-derived) will be compared. These materials are expected to be useful in the localised treatment of cancer.     

Simulation and Experimental Study for Degradation of Organic Dyes Using Dual pin‐to‐plate Corona Discharge Plasma reactors for Industrial Wastewater Treatment

This work researches the possibility of increasing the dye removal efficiency from wastewater using nonthermal plasma. A study for the optimal air gap distance between dual pin and surface of Acid Blue 25 dye solution and thickness of ground plate is carried out using 3D‐EM simulator to find maximum electric field intensity at the tip of both pins. The consequences display that the best gap for corona discharge is approximately 5 mm using 15 kV source. In addition, the optimum plate thickness is 0.1 mm. These distance and thickness were mentioned are constant during the study of other factors. Dual pin‐to‐plate high‐voltage corona discharge plasma system is presented to investigation experimentally the gap distance, thickness of ground plate, initial dye concentration, pH solution and conductivity on the amount of Acid Blue 25 dye color removal efficiency from wastewater. There is a large consensus among the simulation and experimental work in the air gap and thickness of ground plate. Where the decolorization for air gap 5 mm is 95.74 at time 35 min compared with 91% and 17% for 1 mm and 20 mm gap distance respectively. Also, the discharge energy at each air gap are calculated. Measurement results for the impact of thickness of an Aluminum ground plate on color removal competence showed color removal efficiencies of 86.3%, 90.78% and 98.06%, after treatment time 15 min for thicknesses of 2, 0.5 and 0.1 mm respectively. The decolorization behavior utilizing dual pin‐to‐plate corona discharge plasma system display 82% pigment evacuation proficiency inside 11min. The complete decolorization was accomplished within 28min for distinctive examined introductory color focuses 5 ppm up to 100 ppm. Likewise, the impacts of conductivity by utilizing diverse salts as AlCl3, CaCl2, KCl and NaCl and with distinctive focuses have been explored. The rising of the solution conductivity leads to the reduction of decolorization efficiency. The decolorization efficiency and discharge energy are calculated at different concentration molarity for AlCl3, CaCl2, KCl and NaCl. It was observed that the presence of salts at the same concentration level substantially decreased the rate and the extent of decolorization. The results indicate that the optimum pH for the decolorization of Acid Blue 25 dye is in the range between 3 and 6. Furthermore the conductivity and discharge energy were measurement at each value of pH. Energy yield for decolorization and Electrical Energy per Order (EE/O) under different initial pH value were calculated. A kinetic model is used to define the performance of corona discharge system under different value of pH. The model of pseudo ‐zero, pseudo‐first order, and pseudo‐second order reactions kinetic are utilized to investigate the decolorization of Acid Blue 25 dye. The rate of degradation of Acid Blue 25 dye follows the pseudo‐first order kinetics in the dye concentration. Energy consumption requirements for decolorization was considered. The outcomes will be useful for designing the plasma treatment systems suitable for industrial wastewaters. (© 2016 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)     

Energetic balance in an ultrasonic reactor using focused or flat high frequency transducers

In order to undertake irradiation of polymer blocks or films by ultrasound, this paper deals with the measurements of ultrasonic power and its distribution within the cell by several methods. The electric power measured at the transducer input is compared to the ultrasonic power input to the cell evaluated by calorimetry and radiation force measurement for different generator settings. Results obtained in the specific case of new transducer types (composites and focused composites i.e., HIFU: high intensity focused ultrasound) provide an opportunity to conduct a discussion about measurement methods. It has thus been confirmed that these measurement techniques can be applied to HIFU transducers. For all cases, results underlined the fact that measurement of radiation pressure for power evaluation is more adapted to low powers (<15 W) and that measurement by calorimetry is a valid technique for global energy measurements. Composites and monocomponent transducers were compared and it appears that the presence of an adaptation glass plate reduces the efficiency of the monocomponent transducers. The distribution of ultrasonic intensity is qualitatively depicted by sono-chemiluminescence of luminol. Finally, the quantity of energy absorbed by samples placed in the sound field is determined and the temperature distribution monitored as a function of wall distance. This energetic balance allows us to understand the global behaviour of all experimental set-ups made up of a generator–transducer–liquid and sample.     

Numerical modeling of low-pressure RF plasmas

A particle-in-cell simulation is used to model the plasma generated in a parallel plate RF reactor at low pressure. Nonperiodic boundary conditions are used, and the electric field and particle motion are obtained by finite-difference methods leading to the self-consistent creation of sheaths on the boundaries. Model cross sections are used to describe collisions between particles. Ionization is included, and the plasma is maintained by fast electrons generated in the RF sheaths. Most of the power dissipation is due to the acceleration of ions in the time-average sheath fields. At high applied voltage, the power dissipation is described well by the power law P∝V^5/2. Simple scaling laws for the density and plasma potential are obtained. The effect of ion mass and charge-exchange colisions on the ion energy spectrum collected by the electrodes is examined. The ion loss rate drops in the presence of charge-exchange collisions, and this leads to an increase in the density. The collisions also markedly alter the ion energy distribution function     

Experimental investigation of AC losses and effective time constant in the high current cable

The report is dedicated to the results of AC-loss measurements in the ITER (International Thermonuclear Experimental Reactor) Nb₃Sn strand and ITER design subsize cable samples. The test facility described below includes the set of superconducting magnet systems furnished with boil-off calorimetric inserts and calorimetric schemes including gas-flow meters. The calorimetric method and the magnetization loop recording method were used simultaneously for the AC-loss measurements. The coincidence between the results of both measuring techniques was confirmed. The original calorimetric scheme makes it possible to measure the released energy during one pulse of the magnet field. The results of AC loss measurements in ITER subsize conductor samples manufactured in Russia are given as an example.     

Texturing effects in molybdenum and aluminum nitride films correlated to energetic bombardment during sputter deposition

Molybdenum films sputter-deposited at low pressure show a (110) to (211) texture turnover with increasing film thickness, which is accompanied by a transition from a fiber texture to a mosaic-like texture. The degree of (002) texturing of sputtered aluminum nitride (AlN) films strongly depends on nitrogen pressure in Ar/N₂ or in a pure N₂ atmosphere. For the understanding of these phenomena, the power density at the substrate during sputter deposition was measured by a calorimetric method and normalized to the flux of deposited atoms. For the deposition of Mo films and various other elemental films, the results of the calorimetric measurements are well described by a model. This model takes into account the contributions of plasma irradiation, the heat of condensation and the kinetic energy of sputtered atoms and reflected Ar neutrals. The latter two were calculated by TRIM.SP Monte Carlo simulations. An empirical rule is established showing that the total energy input during sputter deposition is proportional to the ratio of target atomic mass to sputtering yield. For the special case of a circular planar magnetron the radial dependence of the Mo and Ar fluxes and related momentum components at the substrate were calculated. It is concluded that mainly the lateral inhomogeneous radial momentum component of the Mo atoms is the cause of the in-plane texturing. For AlN films, maximum (002) texturing appears at about 250 eV per atom energy input. Received: 23 June 2000 / Accepted: 12 December 2000 / Published online: 3 April 2001     

Effect of atmospheric pressure dielectric barrier discharge air plasma on electrode surface

In order to study the influence of plasma on electrode, atmospheric pressure dielectric barrier discharge (DBD) air plasma is employed here to treat copper electrode surface. Plasma is generated between the parallel plate electrodes by means of high voltage produced by a high-frequency power supply with transformer. Electrode surface alterations induced by air plasma are investigated by using field emission scanning electron microscope (FE-SEM), X-ray energy dispersion spectroscopy (EDS) and contact angle measurement. The results show that DBD air plasma removes the organic contaminant on surface and causes electrode surface roughness, oxidization and nitridation. In addition, surface wettability is also improved, as concluded from contact angle measurements.     

等离子体合成射流能量效率及工作特性研究

基于等离子体激励器工作过程中气体放电的焦耳加热作用, 并结合局部热力学平衡等离子体物理假设, 开展了等离子体合成射流三维唯象数值研究, 获得了完整工作周期内等离子体合成射流流场发展演变过程. 研究结果表明, 单次能量沉积建立的自维持周期性射流中存在有实现激励器腔体"充分" 回填的最大脉冲工作频率––饱和频率. 大的能量沉积、小的激励器出口直径和相同腔体体积下大的径高比都可以产生速度更高的射流, 而射流速度的提高会伴随有饱和频率的降低. 一个饱和周期内, 最多约有16%的初始腔内气体喷出, 吸气复原仅能实现初始腔体质量90%左右的回填.一个大气压条件下, 容性电源供能的等离子体合成射流激励器电能向气体热能和射流动能的转化效率分别约为5%和1.6%. 关键词： 等离子体激励器 合成射流 能量效率 饱和频率     

托卡马克等离子体不同运行模式下的电子回旋波电流驱动

在给定等离子体密度分布下，从电子、离子的能量方程出发，根据不同运行模式下等离子体的热传导率不同，分别求出了中心负剪切模式，常规剪切H模式和L模式下的等离子体温度分布，然后通过求解波迹方程与相对论情况下的Fokker-Planck方程，分别计算了这些模式下的电子回旋波电流驱动和波功率沉积.得到在中心负剪切下，驱动电流最大，驱动效率最高，功率沉积和电流分布区间跨度大；在常规剪切H模式下，驱动电流较小，分布区间跨度比较窄，驱动效率相对较低；在常规剪切L模式，驱动电流效率最低，分布区间跨度也非常集中. 关键词： 托卡马克 电子回旋波电流驱动 中心负剪切 常规剪切     

容性耦合射频氩等离子体放电诊断研究及仿真模拟

针对中等气压、中等功率下射频容性耦合(CCRF)等离子体的放电特性,采用基于流体模型的COMSOL软件仿真,建立一维等离子体放电模型,以Ar为工作气体,研究同一气压时不同射频输入功率下等离子体电子温度和电子密度的分布规律。同时依据仿真模型设计制作相同尺寸的密闭玻璃腔体和平板电极,实验测量了不同射频输入功率时放电等离子体的有效电流电压及发射光谱,进而计算等离子体的电子温度及电子密度;利用玻耳兹曼双线测温法,得到光谱法下等离子体的电子温度及电子密度。结果表明:当气体压强为250 Pa、输入功率为100~450 W时,等离子体电压电流呈线性关系,电子密度随功率的增大而增大,而电子温度并未随功率的变化而有明显变化,其与功率无关。运用仿真模拟验证了实验的准确性,通过比较,三种方法所得的结果相近。通过结合等效回路法、光谱法和数值模拟仿真法初步诊断出中等气压下等离子体的放电参数,提出了结合三种方法作为实验研究的方法,使实验结果更具说服力,证明其方法的可靠性,也为进一步的等离子体特性研究提供依据。     

Generation of uniform atmospheric pressure argon glow plasma by dielectric barrier discharge

In this paper, atmospheric pressure glow discharges (APGD) in argon generated in parallel plate dielectric barrier discharge system is investigated by means of electrical and optical measurements. Using a high voltage (0–20 kV) power supply operating at 10–30 kHz, homogeneous and steady APGD has been observed between the electrodes with gap spacing from 0.5 mm to 2 mm and with a dielectric barrier of thickness 2 mm while argon gas is fed at a controlled flow rate of 1 l/min. The electron temperature and electron density of the plasma are determined by means of optical emission spectroscopy. Our results show that the electron density of the discharge obtained is of the order of 10¹⁶ cm^???3 while the electron temperature is estimated to be 0.65 eV. The important result is that electron density determined from the line intensity ratio method and stark broadening method are in very good agreement. The Lissajous figure is used to estimate the energy deposited to the glow discharge. It is found that the energy deposited to the discharge is in the range of 20 to 25 μJ with a discharge voltage of 1.85 kV. The energy deposited to the discharge is observed to be higher at smaller gas spacing. The glow discharge plasma is tested to be effective in reducing the hydrophobicity of polyethylene film significantly.     

CaO–MgO–SiO2 glass ceramics: Transferred arc plasma (TAP) synthesis and microstructural characterization

In this paper, synthesis of CaO–MgO–SiO₂ glass ceramic using transferred arc plasma (TAP) processing method is illustrated. Homogeneous mixture of 51.6% SiO₂, 35.6% CaO and 12.8% MgO prepared by dry mixing in a ball mill was kept in the anode well (which is the melting bed) of the 10 kW transferred arc plasma torch. It was melted in plasma at an operating power of 5 kW (by varying the processing time for 3, 5 and 8 min). The melt was cooled to solidify by applying forced air on it. The resulting samples were characterized for microstructure and phase composition. The phases were identified by scanning electron microscopy (SEM), using the back-scattered electron (BSE) image mode and X-ray diffraction (XRD) and energy dispersive X-ray analysis (EDX). The microstructure was examined using optical microscopy (OM) and scanning electron microscopy. The micro-hardness, density and porosity measurements for the synthesized samples were carried out. Differential thermal analysis (DTA) was performed to study the thermal evolution. The results show the formation of diopside phase in the transferred arc plasma melted CaO–MgO–SiO₂ glass ceramic system achieved with in a quite considerable short time of plasma processing. The method indicated that TAP technique could be a promising, time saving and one-step manufacturing process for the production of functional bulk glass ceramics.     

NOMENCLATURE

Radiant burners are used in drying, preheating, curing, and baking processes in the manufacturing industry. High radiation efficiency is one of the most important performance criteria for these burners. A wide range of radiation efficiencies (varying by more than 200% ) has been reported in the past for similar burners under similar operating conditions. The wide variation in reported radiation efficiencies appears to be due partly to the differences in the measurement techniques. If appropriate calibration source and procedures are used, the differences in data result from (1) nondiffuse emission from the burner and (2) nonuniform burner surface. The present article reports a technique for radiation efficiency measurements of diffuse and directional radiant burner surfaces. The technique is not sensitive to surface nonuniformities, which are common in commercial radiant burners. A calorimetric approach is used as a consistency check on the efficiency data obtained using the present technique. Companion measurements highlight the high degree of variability in the radiation efficiency results deduced from single-point radiation efficiency data, since they are based on the location of the sight tube with respect to the burner surface.