共查询到20条相似文献,搜索用时 68 毫秒
1.
一、前言摄谱法发射光谱分析中摄谱曝光的计时一般用秒表,但人为差错较多;用电动时间继电器计时,精度低,而且故障多。采用微机可编程序计时控制摄谱中的预燃、曝光、移板等步骤,经过调试试验,并投产运行,效果非常好,各步骤控制定时准确,故障少。实践证明,用微机可编程序控制摄谱过程是完全准确可靠的,值得推广应用。 相似文献
2.
颜长铭 《光谱学与光谱分析》1996,16(6):75-78
本文研究了AA3003铝合金微量铅0.005%的光谱分析方法。本法利用沸点4200℃的光谱纯碳电极为辅助电极;采用E601,E603,E605,E607多元素标样组成工作曲线。在相适应的电弧温度的作用下,以交流电弧为光源的分析间隙的发光蒸气云中,形成了Al-C为主体的二元主体组分浓度,使多元素标样与3003合金样品与蒸发与激发行为趋于一致,消除了组分和晶体结构的影响,解决了微量铅0.005%分析准 相似文献
3.
本文分析了五种摄谱法检出限的测定方法,总结了其优缺点和可行性,并进行了实验,在比较的基础上。作者认为采用log(I_0/I_B)/-log C_0作图法,无论是从理论上,还是从实践上,都较其余四种方法优越,是一种值得推荐的方法。 相似文献
4.
5.
采用高压火花光源,一次预烧,连续摄谱的发射光谱法定量分析铸铁中硅,锰、镁三元素,加快了分析速度,可测定质量百分数为1.50%-3.50%的硅、0.40%-1.10%的锰,0.010%-0.090%的镁,其相对标准偏差分别为硅1.9%,锰3.0%,镁10.4%。 相似文献
6.
本文用PC-1500微机以三次多项式拟合的方法处理稀土元素ICP-AES法摄谱数据,讨论了实验方面的有关问题,提出了一套较为简便的实验方法。通过人工合成样分析及磷矿基体中的加料回收实验,证明本法符合实用要求。 相似文献
7.
8.
9.
以六次甲基四胺为沉淀剂宿主、Cu(NO3)2为铜源在乙醇-水(1∶1,φ)体系中采用均匀沉淀法合成了前驱体Cu2(NO3)(OH)3,然后在不同温度下锻烧获得系列纳米CuO粉体,借助XRD,FTIR,XPS,FT-Raman和UV-Vis等测试手段对其谱学特性进行了系统研究。XRD分析表明,所得粉体为单斜晶系的纳米CuO,随锻烧温度的升高,粉体的粒径增大;XPS图谱表明,随热处理温度的升高CuO粉体的表面氧空位减少,导致表面吸附氧含量降低;FTIR图谱表明,随晶粒粒径的减小,在525cm-1附近处Cu—O键特征吸收峰明显宽化,且发生劈裂,劈裂小峰出现双移现象;FT-Raman谱图表明,随着粒径的减小,样品的拉曼散射峰出现宽化现象,并向低波数方向移动;UV-Vis吸收光谱表明,粉体在300~400nm之间有强的吸收,随着粒径的减小最大吸收发生蓝移。探讨了上述谱学规律的成因,对氧化物纳米粒子的谱学特性研究具有重要的借鉴意义。 相似文献
10.
11.
12.
13.
利用汞光谱简单而又分布于整个可见光区的特点,作为标记谱,辅助标准铁光谱,先按顺序分区再识谱(读谱)。该方法使得应用棱镜摄谱仪进行摄谱、读谱变得简单、准确,大大节省了时间,实验设备同时也简化。 相似文献
14.
15.
Equations for the large deflection of thin plate established by Th. von Karman has been well known for many years. But so far there have been only a few iproblems studied with numerical certainty. S. Way was the first to apply these equations to solve the problem of a clamped plate under uniform pressure by the method of power series. After this, S. Levy found the solution of the simply supported rectangular plate under uniform load by the method of double trigonometric series. Both methods are too labourious to be applicable to other more important cases. Lately, Chien Wei-zang treated Way's problem again by means of the perturbation method and obtained excellent results. By the method as given by Chien Wei-zang, Yeh Kai-yuan worked out the problem of circular plate with a central hole under central concentrated load.In this paper, more results are given for various circular plates under various edge conditions. These include uniformly loaded circular plate under various edge conditions (section 2) and central concentrated loaded circular plate under various edge conditions (section 3). Such edge conditions are: (1) simply supported, (2) simply hinged, (3) rigidly clamped, (4) clamped but free to slip, (5) edge clamped but with possible slipping in horizontal direction, (6) edge simply supported but elastically fastened, and (7) edge clamped in elastic wall.All these results are presented in such a form that direct application in design problem is possible. In particular cases, under edge conditions (1) to (4), as σ=0.3, design formulae and curves for central deflection, radial tensile stress and radial bending stress are presented. 相似文献
16.
17.
宋敏 《光谱学与光谱分析》1993,13(3):11-14,62
我们用HRD-1型双光栅单色仪记录了碘分子在可见光区域的吸收光谱。确定了大量的带头,由此得出了碘分子的离解限、离解能、力常数和振动基频。实验结果与理论结果很符合。 相似文献
18.
19.