Infrared dipole-coupled bolometer response on a hemispherical silicon immersion lens

Response of an infrared (λ = 10.6 μm) dipole antenna-coupled bolometer fabricated at the center of the flat side of a hemispherical silicon immersion lens is presented. Predicted and measured antenna patterns as well as the ratio of power from the lens-side to the air-side are provided as a function of illumination F/#. The power-division ratio, Φ_lens/Φ_air, is shown to be given by the square root of the lens dielectric constant, ${?}_{\text{Si}}^{1/2}=3.4$, for F/# larger than F/2 whereas as F/# decreases to F/1 the ratio increases to 5 due to off-axis features in the radiation pattern.     

Orientation relationship between α-Fe precipitate and α-Al2O3 matrix in iron-implanted sapphire

Fe ions were implanted into α-Al₂O₃ single crystals (sapphire) at room temperature and annealed in a reducing atmosphere. The orientation relationships (ORs) between α-Fe particles and sapphire matrix were investigated using transmission electron microscopy (TEM). All the α-Fe particles have the orientation relationship (OR) of (1 1 1)_α-Fe || (0 0 0 1)_sapphire and ${[1\overline{1}0]}_{\alpha \text{-Fe}}\left|\right|{[11\overline{2}0]}_{\text{sapphire}}$ with sapphire. This OR is predicted precisely by the coincidence of reciprocal lattice points (CRLP) method. The other OR of (1 1 0)_α-Fe || (0 0 0 1)_sapphire and ${[111]}_{\alpha \text{-Fe}}\left|\right|{[5\overline{1}\overline{4}0]}_{\text{sapphire}}$ reported before is confirmed by the same method to be one of the secondary preferred orientation relationships in the α-Fe/sapphire system.     

Ultrasound-assisted preparation of alkaline graphite intercalation compounds

Alkaline graphite intercalation compounds were prepared by flake graphite, potassium dichromate, concentrated sulfur acid and sodium hydroxide under ultrasound irradiation and characterized by scanning electron microscopy and X-ray diffraction. The influences of solution alkalinity, bath temperature and reaction time on the expansion volume were also investigated. The results show that alkaline graphite intercalation compounds were prepared when ${\text{SO}}_4^{2-}$ and OH^? ions were inserted into the spaces between the graphene planes, producing a flake morphology and multilevel structure. At the same time that the interlayer volume expanded, the oxidizing ability of the solid increased. When the bath temperature, the reaction time and the solution alkalinity were at 33–36 °C, at 60 min and for pH = 13, the top expansion volume was 35 mL g^?1.     

Growth of infinite-layer (Sr,Nd)CuO2 films by MBE

Single phase, c-axis oriented infinite layer (IL) Sr_1?xNd_xCuO₂ thin films were epitaxially grown on (1 1 0) DyScO₃ substrates by molecular beam epitaxy (MBE). Electron impact emission spectroscopy (EIES) is the tool of choice for a stringent stoichiometry control which is essential for Sr_1?xNd_xCuO₂ thin film preparation. As-grown films contain excess oxygen and therefore a reduction process is necessary to induce superconductivity. In the present study special attention was paid to the underdoped region since the optimization of the reduction process becomes more difficult for lower doping levels x. Sr_0.95Nd_0.05CuO₂ films (underdoped) became superconducting with $T_c^{\text{onset}}$ = 30 K and $T_c^{\text{zero}}$ = 11.4 K after an annealing procedure.     

Negative thermal expansion property of Er0.7Sr0.3NiO3 − δ

A new kind of negative thermal expansion (NTE) material of Er_0.7Sr_0.3NiO_3 − δ is synthesized by solid-state method and investigated. It is found that Er_0.7Sr_0.3NiO_3 − δ crystallizes in orthorhombic structure with rod-shaped grains. Ceramic Er_0.7Sr_0.3NiO_3 − δ exhibits NTE coefficient of $-39.0\times {10}^{-6}{\text{K}}^{-1}$ from 655 to 780 K. The results of X-ray diffraction, temperature dependence of Raman spectroscopy and differential scanning calorimetry (DSC) suggest that the NTE phenomenon relates to its phase transition from orthorhombic to rhombohedral.