高温合金材料热机械疲劳实验技术

本文以ＡＩＳＩ３１６Ｌ不锈钢材料为例介绍了高温低周应变控制热机械疲劳（ＴｈｅｒｍｏｍｅｃｈａｎｉｃａｌＦａｔｉｇｕｅ）试验，温度循环和机械应变循环为相同频率，它们间的相位关系分为同相位和反相位两种．温度循环范围选为２５０～５００℃和２５０～６５０℃两种．通过计算机自动控制的实验系统所得到的试验数据，探讨了热机械疲劳应力－应变响应，裂纹萌发和扩展的性质，材料微观损伤分析和温度范围变化对疲劳性能和寿命的影响．对疲劳试验过程中循环回滞曲线的分析，给出了材料硬化阶段和循环稳定阶段的特性．     

金属材料多轴非比例低周疲劳寿命预测概述

工程中的大多数构件承受着比例或非比例多轴疲劳荷载作用,而非比例强化效应会大大影响其多轴疲劳寿命。精确预测金属材料在多轴非比例荷载下的低周疲劳寿命需要同时考虑等向强化、随动强化及非比例强化效应下的材料本构关系,并在临界面上计算出相应应力应变值,根据不同疲劳失效形式选取不同类型的失效模型来确定疲劳寿命．本文针对这一过程中重要知识点进行阐述,并介绍了相关模型与理论．     

Tensile and Tensile-Mode Fatigue Testing of Microscale Specimens in Constant Humidity Environment

A tensile and tensile-mode-fatigue tester has been developed for testing microscale specimens in high humidity environments in order to investigate the fracture mechanisms of microelectromechanical materials. A humidity control system was installed on a tensile-mode fatigue tester equipped with an electrostatic force grip. A specimen and a griping device were inserted into a small chamber and the humidity was controlled by air flow from a temperature and humidity chamber. The humidity stability was within ±2%RH for humidities in the range 25–90%RH for eight hours of testing. Fatigue tests were performed on single-crystal silicon (SCS) specimens in constant humidity environments and laboratory air for up to 10⁶ cycles. The gauge length, width, and thickness of the SCS specimens were 100 or 500 μm, 13.0 μm, and 3.3 μm, respectively. The average tensile strength was 3.68 GPa in laboratory air; this value decreased in high humidity environments. Fatigue failure was observed during cyclic loading at stresses lower than the average strength. A reduction in the fatigue strength was observed at high relative humidities. Different fracture origins and fracture behaviors were observed in tensile tests and fatigue tests, which indicates that the water vapor in air affects the fatigue properties of SCS specimens.     

Q345低周疲劳性能与疲劳寿命预测分析

本文对结构用钢Q345的低周疲劳性能进行了试验研究。试验在常温下岛津电液伺服疲劳试验机上进行,采用轴向应变控制方法,恒定应变速率为0.005s-1,应变比为-1。试验结果表明,初始阶段,Q345在高应变幅值(0.6%)循环作用下出现循环硬化效应,而在低应变幅值(0.6%)作用下出现循环软化效应;随着加载应变幅的增加,硬化和软化率呈直线上升趋势。Q345疲劳裂纹萌生阶段占其整个寿命的60%以上,其裂纹萌生寿命与应变幅存在幂函数关系。根据Coffin-Manson公式得到了Q345的应变-寿命关系公式;采用能量预测法得到了材料的塑性应变能与疲劳寿命的关系表达式。上述结果对钢结构的设计、评估具有重要的工程应用参考价值。     

Two scale damage model and related numerical issues for thermo-mechanical High Cycle Fatigue

On the idea that fatigue damage is localized at the microscopic scale, a scale smaller than the mesoscopic one of the Representative Volume Element (RVE), a three-dimensional two scale damage model has been proposed for High Cycle Fatigue applications. It is extended here to anisothermal cases and then to thermo-mechanical fatigue. The modeling consists in the micromechanics analysis of a weak micro-inclusion subjected to plasticity and damage embedded in an elastic meso-element (the RVE of continuum mechanics). The consideration of plasticity coupled with damage equations at microscale, altogether with Eshelby–Kröner localization law, allows to compute the value of microscopic damage up to failure for any kind of loading, 1D or 3D, cyclic or random, isothermal or anisothermal, mechanical, thermal or thermo-mechanical. A robust numerical scheme is proposed in order to make the computations fast. A post-processor for damage and fatigue (DAMAGE_2005) has been developed. It applies to complex thermo-mechanical loadings. Examples of the representation by the two scale damage model of physical phenomena related to High Cycle Fatigue are given such as the mean stress effect, the non-linear accumulation of damage. Examples of thermal and thermo-mechanical fatigue as well as complex applications on real size testing structure subjected to thermo-mechanical fatigue are detailed.     

New Experimental Techniques for <Emphasis Type="Italic">In-situ</Emphasis> Measurement of the Damage Characteristics of Piezoelectric Ceramics under High Cycle Fatigue Testing

To better understand the failure characteristics of lead titanate zirconate (PZT) piezoelectric ceramics, in-situ measurements of displacement and crack growth rates were conducted during high cycle fatigue testing, e.g., 5 kHz. A commercial PZT ceramic (used in a buzzer) was employed as the specimen. To examine the failure characteristics, two newly proposed systems were used: (i) a high speed camera system and (ii) a condenser microphone system. The former system consisted of two high speed cameras with an analytical system, which could measure the displacement of the PZT ceramic during the cyclic loading. The maximum displacement value of the ceramic was found to be approximately 20 μm at 0.5 kHz. The three-dimensional shape of the PZT ceramic during cyclic loading could be clearly observed. With the latter system, the displacement intensity arising from the ceramic vibration was detected continuously. It was found that the crack growth rate was not correlated with the fatigue frequency due to the resonance caused by the ceramic oscillation. There is a linear relationship between the crack growth rate and sonar intensity. On the basis of the crack growth behavior, the failure characteristics of the PZT ceramic could be clearly determined.     

大型汽轮机部件低周疲劳安全寿命的设计和评定

文中提出了汽轮机部件低周疲劳安全寿命的设计和评定方法。介绍了汽轮机部件低周疲劳安全寿命的含义和计算方法。该方法以概率论和统计学为基础，把汽轮机部件的低周疲劳寿命处理为随机变量，对低周疲劳试验数据进行统计分析来确定材料低周疲劳寿命的分布参数，使用可靠性理论来确定汽轮机部件的低周疲劳安全寿命。文中给出了低周疲劳寿命服从正态分布和对数正态分布时汽轮机部件低周疲劳安全寿命的计算方法和应用实例。该方法考虑了汽轮机运行参数随机性和材料低周疲劳特性离散性的影响，为汽轮机部件低周疲劳寿命的设计、评定和诊断提供了科学的依据。     

高周疲劳损伤的演化和Lognormal性统计的统一理论

建立了高周疲劳损伤的演化和Ｌｏｇｎｏｒｍａｌ性统计的统一理论，给出了循环次数变量和损伤变量的联合概率密度的Ｆｏｃｋ－Ｐｌａｎｃｋ方程，获得了该方程系数的高阶修正表示，解得了该方程的解析解，讨论了不同条件下概率密度的分布性质，得到其损伤值取失效临界值时寿命的分布满足Ｌｏｇｎｏｒｍａｌ性分布，所有结论与实验相符     

飞机壁板结构的高温声疲劳试验方法

本文对飞机发动机部位常用典型壁板结构的高温声疲劳试验进行了论述．其内容涉及环境模拟、声场测量、声疲劳载荷谱的确定、高温环境下裂纹监测、高温下一阶频率确定等问题．并给出了ＧＨ１４０材料典型壁板结构件的试验结果     

一种形成高—低周复合载荷的方法

根据工程科研试验和生产的实际需要，本文提出了一种产生低周载荷，并把高周载荷与低周载荷复合起来的方法。     

高温超声拉压疲劳试件设计与温度自动控制

本文较深入地开展了高温环境条件下的超声拉压疲劳实验系统研究,深入分析了试件温度高精测量与自动控制和高温试件设计的关键问题。实验系统可以实现高温环境条件下大于1010周次超高周次的疲劳加载。本实验系统利用传统超声疲劳试验机,使用非接触式红外测温仪对试件温度进行实时动态监测,采用间歇振动的方法保证温度波动小于±3℃。实验结果显示,采用本系统得到的实验结果与传统疲劳加载方式的结果一致性很好。本文工作为进一步开展高温环境条件下金属材料高温超高周(1010周次)疲劳损伤和疲劳破坏机理研究提供了新的有效的平台。     

焊接接头低周疲劳裂纹扩展的统计分析与可靠性最弱环模型

在相同的试验条件下,对１６ＭｎＲ压力容器用钢焊接接头焊缝区、热影响区和母材区,分别做了１５ 根试样的低周疲劳试验,获得了三个区的低周疲劳寿命分布与裂纹扩展规律。试验表明,Ｐａｒｉｓ公式中的两个参数ｍ 和ｃ 分别服从正态分布和对数正态分布,ｍ 和ｌｏｇ ｃ 呈现统计线性关系。根据文中的统计结果,采用蒙特卡洛法对给定的两个裂纹长度间的扩展寿命进行了预测,预测结果与试验结果符合良好。文中还对焊接接头三个区的低周疲劳寿命进行了统计分析,获得了相应的概率密度函数,初步提出了整个焊接接头的可靠性最弱环模型。     

The Development of a High Rate Tensile Testing System for Micro Scaled Single Crystal Silicon Specimens

Structures have been built at micro scales with unique failure mechanisms that are not yet understood, in particular, under high-rate loading conditions. Consequently, microelectromechanical systems (MEMS) devices can suffer from inconsistent performance and insufficient reliability. This research aims to understand the failure mechanisms in micro-scaled specimens deforming at high rates. Single-crystal silicon (SCS) micro specimens that are 4 μm thick are subjected to tensile loading at an average strain rate of 92 s^?1 using a miniature Hopkinson tension bar. A capacitance displacement system and piezoelectric load cell are incorporated to directly measure the strain and stress of the silicon micro specimens. The average dynamic elastic modulus of the silicon micro specimens is measured to be 226.8?±?18.50 GPa and the average dynamic tensile strength of the silicon is measured to be 1.26?±?0.310 GPa. High-speed images show that extensive fragmentation of the specimens occurs during tensile failure.     

Synchronous Full-Field Strain and Temperature Measurement in Tensile Tests at Low,Intermediate and High Strain Rates

Tensile tests with simultaneous full-field strain and temperature measurements at the nominal strain rates of 0.01, 0.1, 1, 200 and 3000 s^?1 are presented. Three different testing methods with specimens of the same thin and flat gage-section geometry are utilized. The full-field deformation is measured on one side of the specimen, using the DIC technique with low and high speed visible cameras, and the full-field temperature is measured on the opposite side using an IR camera. Austenitic stainless steel is used as the test material. The results show that a similar deformation pattern evolves at all strain rates with an initial uniform deformation up to the strain of 0.25–0.35, followed by necking with localized deformation with a maximum strain of 0.7–0.95. The strain rate in the necking regions can exceed three times the nominal strain rate. The duration of the tests vary from 57 s at the lowest strain rate to 197 μs at the highest strain rate. The results show temperature rise at all strain rates. The temperature rise increases with strain rate as the test duration shortens and there is less time for the heat to dissipate. At a strain rate of 0.01 s^?1 the temperature rise is small (up to 48 °C) but noticeable. At a strain rate of 0.1 the temperature rises up to 140 °C and at a strain rate of 1 s^?1 up to 260 °C. The temperature increase in the tests at strain rates of 200 s^?1 and 3000 s^?1 is nearly the same with the maximum temperature reaching 375 °C.     

45CrNiMoVA钢的低周疲劳特性和表面疲劳裂纹的在位观测

利用MTS810材料试验机对带中心圆孔的45CrNiMoVA钢低周疲劳特性进行了研究,并借助长焦显微镜和CCD摄像头对试样表面裂纹的演化规律进行了在位停机观测和在位不停机连续观测尝试,试验发现,裂纹均萌生于与拉伸应力垂直的圆孔边缘;疲劳裂纹的萌生与Lueders形变带密切相关,萌生期超过整个疲劳寿命的70%,主裂纹的发展既可以共面扩展的方式向前连续延伸,也可以裂纹连接的方式向前跳跃传播,应力控制的低周疲劳条件下,疲劳寿命与应力面形貌图像,频闪光源照明可以实现表面疲劳裂纹的在位不停机观测。     

高温高应变率下材料拉伸性能测试的一种新方法

为了实现高温环境下材料高应变率动态拉伸实验技术,将分离式Hopkinson杆直接拉伸装置中试样与拉杆的螺纹连接形式变成楔形连接形式,并加装了气动同步装置系统。这样,在对试样加高温时,能使靠近试样的入射和透射杆端处于较低温度。当撞击管向传递法兰运动时,气动同步装置瞬间拖动透射杆和试样,使两者之间的间隙为零,此时沿入射杆传递的入射波同时对试样拉伸加载。经实验验证,此方法可以有效实现材料高温高应变率拉伸加载。     

表面粗糙度对Glidcop和Q345低周疲劳寿命影响的试验研究

为考察表面粗糙度对弥散增强铜合金Glidcop和低合金钢Q345疲劳寿命的影响,对两种材料都加工了不同粗糙度等级的试样,在常温下进行了应力控制的低周疲劳试验,并对断后的试样进行了扫描电镜观察。结果表明,两种材料共有的现象是:粗糙表面削弱了低周疲劳性能,随着表面粗糙度的增大,低周疲劳寿命呈下降趋势;表面粗糙度对主裂纹的形成时间有影响。不同的现象是:低周疲劳寿命与表面粗糙度的关系Glidcop为线性,而Q345则为幂函数;Glidcop的断口有轻微颈缩,疲劳辉纹明显,Q345的主裂纹沿着试样的径向和周向同时扩展,大粗糙度下辉纹支离破碎。因此,表面粗糙度对疲劳寿命的影响既表现出共同的现象,又呈现为材料相关性。本文的结果将为这两种材料制成的承受低周疲劳构件的表面粗糙度选取提供参考。     

Ceramic-Based Speckles and Enhanced Feature-Detecting Algorithm for Deformation Measurement at High Temperature

The mechanical properties of Ni-base alloys have drawn considerable attention owing to their wide application in the hot components of aircrafts and gas turbines. To accurately measure the deformation of Ni-based alloys at high temperatures, a new type of high-temperature speckles is fabricated on the surface of specimens subjected to long heating durations at temperatures up to 1400 °C. Meanwhile, a novel measurement method based on the scale-invariant feature transform algorithm is developed to measure the deformation and obtain a more accurate result. Both of the above proposed methods are used in a creep test of Inconel 713C at 860 °C. The experimental results indicate that the speckles exhibit excellent performance under heating conditions and adhere well to the substrate at high temperatures. Also, the proposed deformation measurement method exhibits superior image processing even when the speckle quality is imperfect with respect to speckle size.     

轴对称构件疲劳损伤演化方程与寿命预估方法的改进

以热力学为基础,引入损伤驱动力构建分式形式的损伤演化方程.进一步针对轴对称问题,引入等效应变和等效应力.根据损伤力学守恒积分原理,得到有损伤情况下和无损伤情况下应力应变与伤度的关系.利用分离变量方法再对损伤演化方程积分,得到棒试件在恒幅应变交变载荷作用下的应力与寿命关系的级数表达式.损伤演化方程中的材质参数由KT=1与KT=3的标准轴对称试件中值疲劳试验数据确定.损伤演化方程与寿命预估方法的正确性由KT=5的疲劳试验结果验证.利用级数解法对扩口管路连接件进行了寿命预估,提供了一种用损伤力学方法来描述构件的疲劳寿命可行的方法.     

SAPH440汽车薄板高低周疲劳特性试验研究

本文通过设计防屈曲装置,对2.3mm厚度汽车薄板SAPH440在室温下进行了单轴拉伸、低周疲劳和高周疲劳等一系列试验．给出该材料静态力学参数,低周疲劳曲线（E-N曲线）、高周疲劳曲线（S-N曲线）以及相关疲劳性能参数．分别得到了在应力比R=0.1和R= -1状态下的疲劳寿命公式．通过考察低周循环应力-应变曲线,发现材料在试验控制的循环应变幅范围内发生了循环软化,具有明显Masing特性．此外,通过对疲劳断口形貌分析,初步给出了疲劳裂纹的扩展机理．