High-energy directly diode-pumped Q-switched 1617 nm Er:YAG laser at room temperature

We describe high-energy Erbium-doped yttrium aluminum garnet (Er:YAG) lasers operating at 1617?nm, resonantly pumped using 1532?nm fiber-coupled laser diodes. A maximum continuous wave output power of 4.3?W at 1617?nm was achieved with an output coupler of 20% transmission under incident pump power of 29.7?W, resulting in an optical conversion of 14% with respect to the incident pump power. In Q-switched operation, the pulse energy of 11.8?mJ at 100?Hz pulse repetition frequency and 81?ns pulse duration was obtained. This energy is the highest pulse energy reported for a directly diode-pumped Q-switched Er:YAG laser operating at 1617?nm.     

Optical transmission and reflection of aluminum film irradiated by nanosecond laser beam and experimental studying of phase-explosion

In this paper we present evidence for a phase explosion during the laser-induced ablation process by studying the optical reflectivity of the ablated plume. The ablation was produced by irradiating thin film aluminum coated on a quartz substrate with a single pulse laser beam in ambient air. The laser pulse was provided by the second harmonic of a Q-switched Nd:YAG laser with ∼10 ns pulse duration. The transmission of a low power He–Ne laser beam through the hot ablated material plume and its reflection (from the front surface, and rear surface of aluminum film) were also monitored during the duration of the ablation event. The results show that the front surface reflectivity is enhanced at an early time of ablation which is described as strong evidence for the creation of a phase explosion in this process.     

Hard tissue ablation with a free running Er:YAG and a Q-switched CO2 laser: a comparative study

The Er:YAG and the CO₂ laser are competitors in the field of hard tissue ablation. The use of Er:YAG lasers (2.94 μm, pulse length _L of 100 to 200 μs) show smaller areas of thermal defects then ‘‘superpulsed’’ CO₂ lasers with pulse lengths of approximately 100 μs. Only the development of a Q-switched CO₂ laser (9.6 μm, τ_L=250 ns) allowed for similar results. In this paper new results for the Er:YAG and the Q-switched CO₂ laser under the influence of water spray will be presented. Several parameters are of special interest for these investigations: the specific ablation energy, which shows a minimum for the CO₂ laser at an energy density of 9 J/cm ² and a broad shallow minimum in the range of 10 to 70 J/cm² for the Er:YAG laser, and comparison of the cut-shape and depth. Surface effects and cutting velocity are discussed based on SEM pictures. Received: 19 July 2000 / Revised version: 1 November 2000 / Published online: 30 November 2000     

Effect of ZnO plasma plume dynamics on laser ablation

The dynamic behaviors and optical properties of a ZnO plasma plume produced by pulsed laser ablation using a Nd:YAG laser (wavelength: 532 nm, pulse width: 3 ns) were studied by fast photography using a commercial gated charge coupled device (CCD) camera linked with a delay circuit and by optical emission spectroscopy at various ambient oxygen pressures. Fast photography was conducted with a resolving power of 0.25 μs and the expansion behaviors of the laser ablation plume were observed. Plasma plume expansion velocity decreased with oxygen partial pressure. The flow of the plasma plume in the early stage of expansion of up to 3 ms agreed well with the drag model.     

Resonantly pumped 1.645 μm high repetition rate Er:YAG laser Q-switched by a graphene as a saturable absorber

A fiber laser resonantly pumped 1.645 μm passively Q-switched Er:YAG laser is reported. Graphene on a silicon carbide was used as the saturable absorber for the Q-switching. The pulse energy of the 1.645 μm Q-switched Er:YAG laser was 7.05 μJ, with a pulse repetition rate of 35.6 kHz and an average output power of 251 mW.     

Laser irradiation effects on gold

Investigations on the laser irradiation effects on gold are explored in terms of plasma-plume dynamics and morphological and crystallographic changes. Annealed 4N gold samples were irradiated with a Q-switched Nd:YAG laser (53 mJ, 21 MW, 532 nm, and pulse width 6–8 ns) for plume dynamics using 10-ns gated fast photography. A Q-switched pulsed Nd:YAG laser (10 mJ, 1.1 MW, 1064 nm, and pulse width 9 ns) was used to irradiate the surface of the samples for morphological and crystallographic studies of laser-irradiated gold in a vacuum ～10^?3 Torr. The annealed samples were exposed to 50 shots of a Nd:YAG laser (10 mJ, 1.1 MW, 1064 nm, and pulse width 9 ns). The investigation on the plume was done by using an intensified charged-couple device ICCD-5760/IR-UV camera. The morphological investigation of the irradiated surface was carried out by analyzing micrographs obtained using an Hitachi S 3000 H scanning-electron microscope (SEM). The crystallographic studies of the irradiated samples were performed by analyzing the XRD patterns obtained using an X’ Pert Pro Pan Analytical X-ray diffractometer. The investigation on gated ICCD images of the plume reveal that, at very earlier times, the plasma-plume expansion has a linear trend, whereas, at later times, the plasma-plume expansion is nonuniform. SEM micrographs exhibit the primary mechanisms of pulsed-laser ablation (PLA), such as hydrodynamic sputtering, thermal sputtering, exfoliation sputtering, and splashing. The surface morphology was explained in terms of crater formation, swelling, burning, nucleation, grain growth, and nonsymmetric heat conduction. The nonuniform thermal expansion of gold due to thermal-energy transfer is also studied by SEM micrographs, which was supported by XRD analysis. The structural analysis on the basis of XRD shows that the composition of the irradiated samples is not disturbed even after laser irradiation. The grain sizes also changed due to laser irradiation.     

1645 nm Q-Switched resonantly pumped Er:YAG laser

A resonantly pumped Q-switched Er:YAG laser at 1645 nm was reported. 1 mJ of output pulse energy was achieved for Q-switched operation at 100 Hz repetition rate under total incident pump power of 4 W. An output peak power of 14 kW and pulse width of 60.6 ns were obtained.     

High-energy Q-switched operation of a fiber-laser-pumped Er:YAG laser

A high-energy Q-switched Er:YAG laser in-band pumped by an Er,Yb co-doped fiber laser is reported. A simple two-mirror multi-mode resonator incorporating an electro-optic Q-switch and a multi-Brewster-plate polarizer was employed, together with a simple compensation scheme to reduce the depolarization loss due to thermally induced stress birefringence in the Er:YAG crystal at high pump powers. The laser yielded Q-switched pulses at 1617 nm with 30.5-mJ pulse energy and <20-ns pulse duration (FWHM) at 20-Hz repetition rate, corresponding to a peak power of >1.5 MW for 55 W of pump power at 1532 nm. The prospects for further improvement in Q-switched performance are discussed.     

Plasma-mediated ablation of brain tissue with picosecond laser pulses

Plasma-mediated ablations of brain tissue have been performed using picosecond laser pulses obtained from a Nd:YLF oscillator/regenerative amplifier system. The laser pulses had a pulse duration of 35 ps at a wavelength of 1.053 µm. The pulse energy varied from 90 µJ to 550 µJ at a repetition rate of 400 Hz. The energy density at the ablation threshold was measured to be 20 J/cm². Comparisons have been made to 19 ps laser pulses at 1.68 µm and 2.92 µm from an OPG/OPA system and to microsecond pulse trains at 2.94 µm from a free running Er:YAG laser. Light microscopy and scanning electron microscopy were performed to judge the depth and the quality of the ablated cavities. No thermal damage was induced by either of the picosecond laser systems. The Er:YAG laser, on the other hand, showed 20 µm wide lateral damage zones due to the longer pulse durations and the higher pulse energies.     

Thermo-mechanical laser ablation of soft biological tissue: modeling the micro-explosions

Characteristics of thermo-mechanical laser ablation process are investigated using an original numerical model. In contrast with previous models, it is based on a microscopic physical model of the micro-explosion process, which combines thermodynamic behavior of tissue water with elastic response of the solid tissue components. Diffusion of dissipated heat is treated in one dimension, and the amount of thermal damage is assessed using the Arrhenius model of the protein denaturation kinetics. Influence of the pulse fluence and duration on temperature profile development, ablation threshold, and depth of thermal damage is analyzed for the case of Er:YAG laser irradiation of human skin. Influence of mechanical properties on the ablation threshold of soft tissue is predicted theoretically for the first time. In addition, feasibility of deep tissue coagulation with a repetitively pulsed Er:YAG laser is indicated from the model. Received: 9 July 1998 / Revised version: 26 February 1999 / Published online: 26 May 1999     

Comparative ablation rate from a Er: YAG laser on enamel and dentin of primary and permanent teeth

This study was conducted to analyze the ablation rate and micromorphological aspects of microcavities in enamel and dentin of primary and permanent teeth using a Er: YAG laser system. Micromorphological evaluation has been performed in terms of permanent teeth; however, little information about Er: YAG laser interaction with primary teeth can be found in the literature. Because children have been the most beneficiary patients with laser therapy in our offices, it is extremely necessary to compare the effects of this kind of laser system on the enamel and dentin of permanent and primary teeth. In this study, we used eleven intact primary anterior exfoliated teeth and six extracted permanent molar teeth. We used a commercial laser system: a Er: YAG Twin Light laser system (Fotona Medical Lasers, Slovenia) at 2940 nm, changing average energy levels per pulse (100, 200, 300, and 400 mJ) producing 48 microcavities in enamel and dentin of primary and permanent teeth. Primary teeth are more easily ablated than are permanent teeth, when related to enamel or dentin. However, while this laser system is capable of slowly revealing the enamel’s microstructure, in dentin only the lowest laser energies permit this kind of observation, more easily decomposing the original tissue aspect, when related to primary or permanent teeth. Statistically, the only different factor at the 5% level was an energy per pulse of 400 mJ, confirming the results found in SEM. Our results showed that dentin in both primary and permanent teeth is less resistant to Er: YAG laser ablation; this fact is easily observed under SEM observation and through the ablation rate evaluation.     

The first-stokes pulse generation in Nd:KGW intracavity driven by a diode-pumped passively Q-switched Nd:YAG/Cr<Superscript>4+</Superscript>:YAG laser

The operation of an all solid-state pulsed Nd:KGW Raman laser pumped by compact passively Q-switched Nd:YAG/Cr:YAG laser is demonstrated. The first-Stokes radiation of stimulated Nd:KGW Raman scattering at the 1178 nm is generated. The average output power of 336 mW at Stokes wavelength was obtained under the laser diode pump power of 5.74 W. The corresponding optical efficiency from the diode light to the Raman output is 9.85%. The pulse width of 1.65 ns and a pulse repetition rate of 10 kHz were also obtained.     

Self-cleaning effect of sealing caps for infrared hollow fiber delivering pulsed Er:YAG laser light

A sealing cap had been proposed as an output device for hollow optical fibers in delivering laser light underwater. Properties of sealing cap were experimentally discussed when used in ablation on soft tissue for Er:YAG laser. A self-cleaning effect of the sealing cap was observed when various targets were used for different laser light power. Debris from pork fat formed a uniform oil layer on the output surface of the cap, and the oil layer is relatively transparent in Er:YAG laser light wavelength band. When the target was pork muscle, almost no debris could attach on the surface of the cap. The self-cleaning effect was more obvious when ablation was conducted underwater because of the protection of the water film between the target and the cap's surface.     

Laser backwriting process on glass via ablation of metal targets

Ablation of metal targets onto pyrex glass substrates, using a Q-switched Nd:YAG laser working at 355 nm, was used to study the potential of a laser backwriting process for the fabrication of optical waveguides via an index of refraction change. Metal foils of stainless steel, aluminum, copper, brass and gold have been used as blanks and irradiated by focusing the laser beam through a cylindrical lens under continuous movement in a direction perpendicular to the irradiation. An horizontal setup was found suitable to improve the effect of the plume in the sample. Results were obtained for two different configurations. Transversal profiles were analysed using a contact profilometer, comparing results obtained for the different configurations, traverse speeds and metal targets used. Two ablation regimes were identified, which are related to a critical laser fluence value of 2.7 J/cm². Surface micrographs obtained by scanning electron microscopy are discussed, together with the characteristics of the structures attained, taking into account the optical and thermal properties of the ablated metal blanks.     

Diode end-pumped passively Q-switched Nd:YAG ceramic laser with Cr4+:YAG saturable absorber

We report on a diode end-pumped passively Q-switched Nd:YAG ceramic laser. By using a Cr⁴⁺:YAG single crystal with an 80% initial transmission as the saturable absorber, stable Q-switched pulses with a 126-μJ pulse energy, a 12-ns pulse width, and an 8.4-kHz pulse repetition rate have been obtained. The Q-switching performance of the laser under different saturable absorption strengths and output couplings was experimentally investigated.     

Wavelength dependence of soft tissue ablation by using pulsed lasers

Pulsed laser ablation of soft biological tissue was studied at 10.6-, 2.94-, and 2.08-μm wavelengths. The ablation effects were assessed by means of optical microscope, the ablation crater depths were measured with reading microscope. It was shown that Er:YAG laser produced the highest quality ablation with clear,sharp cuts following closely the patial contour of the incident beam and the lowest fluence threshold. The pulsed CO2 laser presented the moderate quality ablation with the highest ablation efficiency. The craters drilled with Ho:YAG laser were generally larger than the incident laser beam spot, irregular in shape, and clearly dependent on the local morphology of biotissue. The blation characteristics, including fluence threshold and ablation efficiency, varied substantially with wavelength. It is not evident that water is the only dominant chromophore in tissue.     

Efficient 1645-nm Er:YAG laser

We report a resonantly fiber-laser-pumped Er:YAG laser operating at the eye-safe wavelength of 1645 nm, exhibiting 43% optical efficiency and 54% incident slope efficiency and emitting 7-W average power when repetitively Q switched at 10 kHz. To our knowledge, this is the best performance (conversion efficiency and average power) obtained from a bulk solid-state Q-switched erbium laser. At a 1.1-kHz pulse repetition frequency the laser produces 3.4-mJ pulses with a corresponding peak power of 162 kW. Frequency doubling to produce 822.5-nm, 4.7-kW pulses at 10 kHz was performed to demonstrate the laser's utility.     

Erbium:YAG (2.94 mum) laser effects on dental tissues

Past trials with soft and calcified tissues have demonstrated that long pulse train (2.5 mus) Er:YAG (2.94 mum) laser may be used to ablate tooth structure of human teeth. Determination of physical and thermal damage to surrounding tissue during removal of enamel and dentin is a primary objective of this study. Extracted human teeth with thermal probes imbedded in the pulp chambers were submitted to cavity preparation using an Erbium YAG laser with water mist. Wavelength selection as well as use of a water mist during the procedure resulted in efficient tissue removal without significant surrounding damage. Ground sections and SEM sections of teeth showed little or no melting or ash formation in adjacent dentin and enamel and no visible change in the pulp chamber. The surfaces produced by laser ablation were rough and irregular with craters and grooves. Average temperature change in the pulp chamber monitored during tooth preparation was 2.2 degrees Centigrade. These findings suggest that constantly available water aids vaporization and microexplosions, increasing the efficiency of tooth structure removal, and aids in cooling of the tooth structures. The long pulse Er:YAG (2.94 mum) laser may be an effective method for tooth reduction applications when used with a water mist.     

A method for rapid measurement of laser ablation rate of hard dental tissue

The aim of the study reported here is the development of a new method which allows rapid and accurate in-vitro measurements of three-dimensional (3D) shape of laser ablated craters in hard dental tissues and the determination of crater volume, ablation rate and speed. The method is based on the optical triangulation principle. A laser sheet projector illuminates the surface of a tooth, mounted on a linear translation stage. As the tooth is moved by the translation stage a fast digital video camera captures series of images of the illuminated surface. The images are analyzed to determine a 3D model of the surface. Custom software is employed to analyze the 3D model and to determine the volume of the ablated craters. Key characteristics of the method are discussed as well as some practical aspects pertinent to its use. The method has been employed in an in-vitro study to examine the ablation rates and speeds of the two main laser types currently employed in dentistry, Er:YAG and Er,Cr:YSGG. Ten samples of extracted human molar teeth were irradiated with laser pulse energies from 80 mJ to the maximum available energy (970 mJ with the Er:YAG, and 260 mJ with the Er,Cr:YSGG). About 2000 images of each ablated tooth surface have been acquired along a translation range of 10 mm, taking about 10 s and providing close to 1 million surface measurement points. Volumes of 170 ablated craters (half of them in dentine and the other half in enamel) were determined from this data and used to examine the ablated volume per pulse energy and ablation speed. The results show that, under the same conditions, the ablated volume per pulse energy achieved by the Er:YAG laser exceeds that of the Er,Cr:YSGG laser in almost all regimes for dentine and enamel. The maximum Er:YAG laser ablation speeds (1.2 mm³/s in dentine and 0.7 mm³/s in enamel) exceed those obtained by the Er,Cr:YSGG laser (0.39 mm³/s in dentine and 0.12 mm³/s in enamel). Since the presented method proves to be easy to use and allows quite rapid measurements it may become a valuable tool to study the influence of various laser parameters on the outcome of laser ablation of dental tissues.     

Mid-infrared radiation transmission through fluoride glass multimode optical fibers

Measurement of the transmission laser radiation from Q-switched and free-running Er:YAG lasers operating at 2.94 μm through fluoride glass multimode optical fibers of 448, 465 and 620 μm core diameter were performed. Attenuation measurements were obtained as a function of the laser energy input, of the bending angle and of the radius of curvature. The fibers exhibited low attenuation under straight and bent conditions. The output beam quality was also studied using the appropriate beam profiler. The output beam profiles showed a central multi-spiked energy distribution.