Microplastic deformation of polycrystalline and submicrocrystalline titanium during static and cyclic loading

A study is made of the laws governing the accumulation of microplastic strain during the static and cyclic loading of polycrystalline and submicrocrystalline titanium. It is shown that a change from the polycrystalline structure to the submicrocrystalline structure does not change the character of development of microplastic strain for either type of loading, but it does increase fatigue strength and fatigue limit. A correlation between the fatigue strength based on 10⁶ cycles and the macroscopic elastic limit was found to exist for both types of loading. Siberian Physico-Technical Institute (at Tomsk University), Institute of the Physics of Strength and Materials Science (in the Siberian Division of the Russian Academy of Sciences), and the Institute of the Physics of Promising Materials (at Ufa State University of Aeronautical Engineering). Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, Vol. 41, No. 12, pp. 20–25, December, 1998.     

Cellular dislocation substructures in polycrystals of FCC solid solutions based on copper: Holt’s relation and the size effect

The cellular dislocation substructures (CDSes) of Cu-Mn polycrystalline solid solutions upon plastic deformation is studied by means of TEM. It is determined that Holt??s relation holds for alloys with different grain sizes, solid solution concentrations, and deformation temperatures. The dependence of Holt??s coefficient C on the main polycrystalline parameters and deformation conditions is studied. Regularities of the fraction of closed cell boundaries and disoriented boundaries in CDS that emerge upon deformation are determined.     

Effect of chromium on structure,strength, and plasticity of high-temperature intermetallide Ni3Al

The effect of chromium on structure, strength characteristics, plasticity, and failure principles in the polycrystalline intermetallide Ni₃Al, produced by self-propagating high-temperature synthesis, is studied over the temperature range 290–1270 K. It is shown that the effect of chromium depends upon which element (nickel or aluminum) it is introduced in place of, although failure of alloys with various chromium contents at all deformation temperatures remains intercrystallite in nature.V. D. Kuznetsov Siberian Physicotechnical Institute at Tomsk State University. Institute of Strength Physics and Materials Science, Siberian Branch, Russian Academy of Sciences. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 6, pp. 30–36, June, 1993.     

Defect microstructure in titanium nitride submicrocrystals

Transmission electron microscopy has been applied to the defect structure of titanium nitride in the submicrocrystalline (SMC) state produced under conditions of deviation from equilibrium in ion-plasma synthesis. The submicrocrystals contain a new type of defect substructure having a continuum disclination density up to 2.5 rad/μm². Direct structure methods give evidence for a high density of partial disclinations at the SMC grain boundaries in the nitride phase. A novel method has been used to examine substructures having a high defect density, which has been used to estimate the partial disclination density at the submicrocrystal boundaries. The origin of this highly defective state and the effects of it on the properties of SMC materials is discussed. Kuznetsov Siberian Technical Physics Institute, Tomsk State University. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 7, pp. 3–12, July, 1998.     

Micromechanical model of deformation-induced surface roughening in polycrystalline materials

A micromechanical model has been developed to describe deformation-induced surface roughening in polycrystalline materials. The three-dimensional polycrystalline structure is taken into account in an explicit form with regard to the crystallographic orientation of grains to simulate the micro- and mesoscale deformation processes. Constitutive relations for describing the grain response are derived on the basis of crystal plasticity theory that accounts for the anisotropy of elastic-plastic properties governed by the crystal lattice structure. The micromechanical model is used to numerically study surface roughening in microvolumes of polycrystalline aluminum and titanium under uniaxial tensile deformation. Two characteristic roughness scales are distinguished in the both cases. At the microscale, normal displacements relative to the free surface are caused by the formation of dislocation steps in grains emerging on the surface and by the displacement of neighboring grains relative to each other. Microscale roughness is more pronounced in titanium, which is due to the high level of elastic-plastic anisotropy typical of hcp crystals. The mesoscale roughness includes undulations and cluster structures formed with the involvement of groups of grains. The roughness is quantitatively evaluated using a dimensionless parameter, called the degree of roughness, which reflects the degree of surface shape deviation from a plane. An exponential dependence of the roughness degree on the strain degree is obtained.     

Variation of apparent creep activation energy in plastic deformation of molybdenum in diffusion contact with nickel

The variation of the apparent creep activation energy as a function of the state of grain boundaries is investigated in the deformation of molybdenum in the presence of diffusion fluxes of nickel at the grain boundaries. It is shown that this energy varies in the same way as in the plastic deformation of classical superplastic materials.Physics Institute of Strength and Materials Science, Siberian Branch, Russian Academy of Sciences. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 5, pp. 110–113, May, 1993.     

多晶银纳米线拉伸变形的分子动力学模拟研究

纳米尺度金属Ag以其独特的导电和导热性,广泛应用于微电子、光电子学、催化等领域,特别是在纳米微电极和纳米器件方面的应用.本文采用分子动力学方法模拟了不同晶粒尺寸下多晶银纳米线的拉伸变形行为,详细分析了晶粒尺寸对多晶银纳米线弹性模量、屈服强度、塑性变形机理的影响.发现当晶粒尺寸小于13.49 nm时,多晶Ag纳米线呈现软化现象,出现反Hall-Petch关系,此时的塑性变形机理主要以晶界滑移、晶粒转动为主,变形后期形成五重孪晶;当晶粒尺寸大于13.49 nm时,塑性变形以位错滑移为主,变形后期产生大量的孪晶组织.     

Control of grain boundary microstructures in molybdenum polycrystals by thermomechanical processing of single crystals

The formation of grain structures and grain boundary microstructures in polycrystalline molybdenum, produced by thermomechanical processing from cylindrical single crystals with different initial surface normal orientations of ?110?, ?111? and ?112?, were investigated with the objective of controlling grain boundary microstructures. The polycrystalline specimens displayed different microstructures depending on the initial orientation of the single crystal and the deformed microstructure. The recrystallized microstructure was composed of some oriented-grain clusters, in which grains possessing a similar orientation were assembled. The frequency of low-angle boundaries was very high in the oriented-grain clusters. A close relationship also existed between the grain boundary character distribution (GBCD) and the triple junction distribution. Grain boundary microstructures were compared of bcc molybdenum and fcc polycrystalline materials with reference to path-dependent percolation resistance.     

Nature of the temperature dependence of plasticity in the polycrystalline intermetallic compound Ni3Al

The effect of temperature on the plasticity, the type of failure, and the fractions of brittle intercrystallite and viscous transcrystallite failure of the intermetallic compound Ni-24 at. % Al have been studied with boron and without boron. A method is proposed for determining the cohesive strength of the grain boundaries by using the parameters of the flow curve and taking account of the local plastic deformation at the tip of the crack. It is shown that the cohesive strength of the grain boundaries is quite high in Ni₃Al and it is not the cause of the low-temperature embrittlement. The temperature dependence of the plasticity in the Ni-25 at. % Al alloy with boron and without boron in the region of the anomalous temperature dependence of the flow limit is determined by the change in the deformational hardening coefficient and at higher temperatures by a lowering of the cohesive strength of the grain boundaries.V. D. Kuznetsov Siberian Physicotechnical Institute, Tomsk University. Institute for Strength and Materials Science, Siberian Branch, Russian Academy of Sciences. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 11, pp. 80–89, November, 1994.     

Transformations of Dislocation Substructures under Fatigue Loading

Research literature on dislocation substructures formed in fcc metals and alloys under fatigue loading is reviewed. The materials are classified into three groups according to the types of dislocation substructures formed at the onset of fatigue loading and transformation sequences occurring on further loading. Quantitative results obtained from investigations of the evolution pattern of the defect subsystem formed under fatigue loading are examined.     

纳米单晶与多晶铜薄膜力学行为的数值模拟研究

通过对不同温度下单晶薄膜的拉伸性能的分子动力学模拟，从微观角度揭示了温度效应对材料性能的影响. 结果表明温度效应对材料的变形机理影响很大.0K温度下由于缺乏热激活软化的影响, 粒子运动所受到的阻碍较大, 薄膜的强度较高, 塑性变形主要来自于粒子的短程滑移.温度升高，粒子的热运动加剧，屈服强度降低, 塑性变形将主要来自于大范围的位错长程扩展.多晶薄膜的模拟结果表明, 虽然其晶粒形状较为特殊, 但是它仍然遵循反Hall-Petch关系.在模拟过程中，侧向应力最大值比拉伸方向应力的最大值滞后出现.位错只会从晶界产生并向晶粒内部传播，晶粒间界滑移是多晶薄膜塑性变形的主要来源. 关键词： 纳米薄膜 变形机理 温度效应 分子动力学     

A study on anomalous yield drop behaviour in modified beta titanium alloys

ABSTRACT

The yield drop phenomenon observed in the Ti–15V-3Al–3Sn-3Cr (Ti–15–3) beta-titanium alloy and its anomalous behaviour in the boron and carbon added Ti–15–3 alloys have been studied. While the base and the carbon containing alloys exhibit yield drop, the boron containing alloy with smaller grain size than base alloy does not appear to show this phenomenon. Tensile tests were interrupted at different stress levels followed by analyses of slip lines and sub-structural characteristics using scanning and transmission electron microscopes to understand this anomalous yield point phenomenon. Infrared thermal imaging technique was used to map the strain localisation and the spatiotemporal evolution of deformation along the gauge length of the specimens during the tensile tests. Deformation in these alloys initiates only in a few grains. Pile-up of dislocations in these grains subsequently triggers the formation of dislocations in other grains and their rapid multiplications. The spreading of deformation by the generation of dislocations from pile up dislocations in one grain to neighbouring un-deformed grains and their rapid multiplication to new regions influence the yield drop phenomenon and its characteristics. It is shown in this study that microscopic instability in the grain level is a necessary, but not the sufficient condition for the manifestation of macroscopic instability during tensile deformation in polycrystalline materials. The presence of boride particles at grain boundaries restricts the slip transfer across the grains as well as the spreading of deformation to new regions, which causes the suppression of yield drop in the boron containing alloy.     

Plasticity and strength of solids

This article reviews research conducted over the past 15 years at the intersection of the physics and mechanics of a deformable solid on the basis of the concept that plastic deformation and failure represent the evolution of shear-stability loss of a loaded material at various scale levels. This research has led to the founding of a new scientific discipline: the physical mesomechanics of materials, in which a deformable solid is regarded as a multilevel self-organizing system. The development of mechanisms and stages of plastic deformation at different scale levels conforms to the principle of scale invariance. This qualitatively changes the methods of describing the plastic deformation and failure of solids. The most pressing areas of research in the physical mesomechanics of materials are noted; these will determine the basic trends in research on the strength of solids in the next decade. Institute of Strength Physics and Materials Science, Siberian Branch, Russian Academy of Sciences. Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 1, pp. 7–34, January, 1998.     

High-speed superplasticity of microcrystalline alloys under conditions of local grain boundary melting

A model is proposed for the high-speed superplasticity of materials under conditions of local grain boundary melting at temperatures close to solidus. It is shown that the local melting of grain boundaries containing segregations of impurity atoms, results in the formation of a structure consisting of liquid-phase regions and solid intergranular bridges which provide cohesion of the grains during the deformation process. The equilibrium concentration, dimensions, and activation energy for the formation of solid bridges are determined as a function of the temperature, initial impurity concentration in the boundary, and the boundary thickness. A mechanism is proposed for grain-boundary slip under conditions of local grain boundary at anomalously high strain rates. Zh. Tekh. Fiz. 68, 38–42 (December 1998)     

High‐energy transmission Laue micro‐beam X‐ray diffraction: a probe for intra‐granular lattice orientation and elastic strain in thicker samples

An understanding of the mechanical response of modern engineering alloys to complex loading conditions is essential for the design of load‐bearing components in high‐performance safety‐critical aerospace applications. A detailed knowledge of how material behaviour is modified by fatigue and the ability to predict failure reliably are vital for enhanced component performance. Unlike macroscopic bulk properties (e.g. stiffness, yield stress, etc.) that depend on the average behaviour of many grains, material failure is governed by `weakest link'‐type mechanisms. It is strongly dependent on the anisotropic single‐crystal elastic–plastic behaviour, local morphology and microstructure, and grain‐to‐grain interactions. For the development and validation of models that capture these complex phenomena, the ability to probe deformation behaviour at the micro‐scale is key. The diffraction of highly penetrating synchrotron X‐rays is well suited to this purpose and micro‐beam Laue diffraction is a particularly powerful tool that has emerged in recent years. Typically it uses photon energies of 5–25 keV, limiting penetration into the material, so that only thin samples or near‐surface regions can be studied. In this paper the development of high‐energy transmission Laue (HETL) micro‐beam X‐ray diffraction is described, extending the micro‐beam Laue technique to significantly higher photon energies (50–150 keV). It allows the probing of thicker sample sections, with the potential for grain‐level characterization of real engineering components. The new HETL technique is used to study the deformation behaviour of individual grains in a large‐grained polycrystalline nickel sample during in situ tensile loading. Refinement of the Laue diffraction patterns yields lattice orientations and qualitative information about elastic strains. After deformation, bands of high lattice misorientation can be identified in the sample. Orientation spread within individual scattering volumes is studied using a pattern‐matching approach. The results highlight the inability of a simple Schmid‐factor model to capture the behaviour of individual grains and illustrate the need for complementary mechanical modelling.     

The inhomogeneity of plastic deformation

Considerable local strain differences occur in single crystals as a consequence of slip bands. A significant contribution to this phenomenon is the effect of the deformation rate on the inhomogeneity of its distribution. In polycrystalline materials the plastic deformation is affected by grain boundaries and their vicinity as well as by various orientations of single grains in onephase metals and alloys, and by various component properties in multiphase materials. In some cases it has been possible to describe these phenomena by means of micromechanics. Valuable information has also been acquired by means of three-dimensional stereology.     

Absence of an abrupt phase change from polycrystalline to amorphous in silicon with deposition temperature.

Using fluctuation electron microscopy, we have observed an increase in the mesoscopic spatial fluctuations in the diffracted intensity from vapor-deposited silicon thin films as a function of substrate temperature from the amorphous to polycrystalline regimes. We interpret this increase as an increase in paracrystalline medium-range order in the sample. A paracrystal consists of topologically crystalline grains in a disordered matrix; in this model the increase in ordering is caused by an increase in the grain size or density. Our observations are counter to the previous belief that the amorphous to polycrystalline transition is a discontinuous disorder-order phase transition.