The temperature profile in the molten layer of a semi-infinite target induced by irradiation using a pulsed laser

The two-dimensional Laplace integral transform technique has been used to compute the temperature profile of the molten layer on the surface of a semi-infinite target when irradiated by a pulsed laser. Mathematical expressions for the temperature distribution in the molten layer thickness and the solid part of the target, taking cooling and the temperature-dependent absorption coefficient of the irradiated surface into account, were obtained. As an illustrative example computations were carried out on a semi-infinite aluminum (Al) target.     

A theoretical study on the melting of a finite slab with a pulsed laser

Calculations of the spatial and temporal temperature distributions in the molten layer thickness, the still solid part and in the backward surface of the finite slab were carried out during the irradiation with a pulsed laser. The two-dimensional Laplace integral transform technique has been applied to obtain the mathematical expressions for these temperature distributions and the molten layer thickness as a function of the melting time. The derivations have taken into account the temperature-dependent absorption coefficient of the irradiated surface and the cooling. As an illustrative example, computations were carried out on a finite aluminum (Al) target.     

The temperature profile in the molten layer of a thin-film coated on a substrate induced by irradiation with a pulsed laser

The two-dimensional Laplace integral transform technique has been applied to get the temperature distributions in the molten layer of a thin-film coated on a substrate, the solid part of the film and the substrate during the irradiation with a pulsed laser. The derivation has taken into account the cooling and the temperature-dependent absorption coefficient of the irradiated surface. As an illustrative example computations were carried out on an aluminum thin-film coated on a glass substrate.     

A theoretical study of the evaporation induced by a pulsed laser in a finite slab

The two-dimensional integral Laplace transform technique has been applied to get the temperature distributions in the molten layer, the solid part and in the backward surface of a finite target irradiated with a pulsed laser. Formulas for the time dependence of the evaporated part and the molten layer thicknesses of the target were found. This is accomplished by considering the temperature dependence of the absorption coefficient of the irradiated surface as well as the chemical reaction. As an illustrative example computations were carried out on an aluminum (Al) target.     

On the evaporation of a semi-infinite target induced by a pulsed laser

The two-dimensional Laplace integral transform technique has been applied to get the temperature distributions in the molten and the solid parts of a semi-infinite target irradiated with a pulsed laser. Formulas for the time dependence of the evaporated part and the molten layer thicknesses of the target were found considering the temperature dependence of the absorption coefficient of the irradiated surface as well as the chemical reaction. As the illustrative example computations were carried out on an aluminum target.     

On melting a semi-infinite target using a pulsed laser

The two-dimensional Laplace integral transform technique is used to solve the problem of melting a semi-infinite target induced by surface absorption of a laser pulse.Mathematical expressions for the temperature distribution within the solid part of the target and the thickness of its liquified part were obtained considering cooling, temperature dependent absorption coefficient of the irradiated surface and constant temperature in the molten layer. As an illustrative example computations were carried out on a semi-infinite aluminium (Al) target.     

Characteristics of indirect laser-induced plasma from a thin film of oil on a metallic substrate

Optical emissions from the major and trace elements embodied in a transparent gel prepared from cooking oil were detected after the gel was spread in a thin film on a metallic substrate. Such emissions are due to the indirect breakdown of the coating layer. The generated plasma, a mixture of substances from the substrate, the layer, and the ambient gas, was characterized using emission spectroscopy. The characteristics of the plasma formed on the metal with and without the coating layer were investigated. The results showed that Al emission induced from the aluminum substrates coated with oil films extends away from the target surface to ablate the oil film. This finally formed a bifurcating circulation of aluminum vapor against a spherical confinement wall in the front of the plume, which differed from the evolution of the plasma induced from the uncoated aluminum target. The strongest emissions of elements from the oil films can be observed at 2 mm above the target after a detection delay of 1.0 μs. A high temperature zone has been observed in the plasma after the delay of 1.0 μs for the plasma induced from the coated metal. This higher temperature determined in the plasma allows the consideration of the sensitive detection of trace elements in liquids, gels, biological samples, or thin films.     

矩形折射率调制型薄膜长周期光纤光栅特性研究

镀膜长周期光纤光栅传感器是目前光纤光栅传感研究的一个热点,但关于此类传感器模型的全面的理论分析目前还很少。本文基于严格的四层模型,从理论上对芯层折射率调制为矩形波调制的薄膜长周期光纤光栅的特性进行了详细的分析。在充分考虑材料色散对光纤芯层和包层的影响后,对薄膜参数、占空比和环境折射率的变化对镀膜长周期光纤光栅的谱特性的影响进行了数值研究。研究结果表明,薄膜参数对透射谱有重要影响,合理设计薄膜厚度可以获得较佳的损耗峰。研究还发现,镀膜后占空比对透射谱的影响减小,而对环境折射率变化的敏感度增加。在占空比为0.5时光栅具有最大的损耗峰值。     

Bireflectance thin film in a high beat frequency laser

This paper investigates a kind of bireflectance thin film on the window plate of a 633 nm He–Ne laser. The film is coated on the substrate with the application of external load on it. The load on the substrate is removed after the coating has been accomplished, then the strain on the substrate will be transferred to the multilayer coatings. Due to photoelastic effect, the multilayer film becomes an anisotropic film. Selecting appropriate film structure and suitable center wavelength, a high phase dispersion with nearly constant reflectivity around the working wavelength will be obtained. For normal incidence, a sufficient phase shift difference between the two orthogonal polarization states of the reflected wave will be produced. As a result, a dual-frequency laser with a beat frequency of 5 MHz can be carried out by using this kind of multilayer film. The theory of designing such a film is emphasized and an example of bireflectance thin film is proposed.     

声表面波生物传感器质量灵敏度的理论与实验验证

针对声表面波传感器在生物检测中的性能评价与优化,提出一种快捷验证适用于生物传感器的声表面波器件质量负载灵敏度的实时检测方法.首先基于二维近似假设和周期性边界条件,建立了以石英为压电基底材料、SiO2为波导层的Love波传感器的三维有限元分析模型,从理论上验证了波导层对Love波传感器灵敏度的影响.在实验上,通过MEMS...     

ZnO thin film characterization by X-ray reflectivity optimization using genetic algorithm and Fourier transformation

Zinc oxide (ZnO) thin film was fabricated by sol-gel spin coating method on glass substrate. X-ray reflectivity (XRR) and its optimization have been used for characterization and extracting physical parameters of the film. Genetic algorithm (GA) has been applied for this optimization process. The model independent information was needed to establish data analyzing process for X-ray reflectivity before optimization process. Independent information was exploited from Fourier transform of Fresnel reflectivity normalized X-ray reflectivity. This Fourier transformation (Auto Correlation Function) yields thickness of each coated layer on substrate. This information is a keynote for constructing optimization process. Specular X-ray reflectivity optimization yields structural parameters such as thickness, roughness of surface and interface and electron density profile of the film. Acceptable agreement exists between results obtained from Fourier transformation and X-ray reflectivity fitting.     

Synthesis of TiN thin films by a new combined laser/sol-gel processing technique

In this work a novel method for synthesising TiN coatings is reported. A high-power diode laser at different powers and traverse speeds was applied to a mild steel substrate, coated with a slurry of titania sol-gel, urea and graphite. The reaction chemical thermodynamics was investigated to estimate the compositions, temperature range, and the required reaction enthalpy for producing TiN. A one-dimensional heat transfer model was used to optimise the processing parameters. Surface morphology and microstructure of the deposited coatings and substrate surface layers were examined using optical microscopy, scanning electron microscope, and field emission gun scanning electron microscope which reveals deposition of very thin layer about 0.3 μm of pure TiN and the presence of sub-micron crystalline structure of TiN forming a metal matrix composite inter-layer with the substrate below the film which suggest a good metallurgically bonding with the substrate. Chemical composition was determined by energy dispersive X-ray analysis. The phases were identified by X-ray diffraction which confirms the synthesis of TiN film for all the samples. Results of nano-hardness measurements revealed a hardness value of the order of 22-27 GPa.     

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利用微波电子回旋共振等离子体增强型化学气相沉积(ECR-PECVD)采用一步法直接在K9玻璃上低温沉积制备了多晶硅薄膜.研究了不同实验参数对薄膜沉积的影响,采用X射线衍射(XRD)、拉曼光谱、扫描电子显微镜(SEM)等实验分析方法对不同条件下制备的样品进行了晶体结构和表面形貌分析,并讨论了多晶硅薄膜沉积的最佳条件.实验结果表明,玻璃衬底上多晶硅薄膜呈柱状生长,并有一定厚度的非晶孵化层;较高氢气比例和衬底温度有利于结晶,薄膜的结晶率达到了62％;晶粒团簇的最大尺寸约为500nm.     

Simulation of the interface characterization of thin film on substrate system by bending creep tests

In the present paper, the finite element simulation of the bending creep tests of the thin film on substrate system is carried out. The purpose of the investigation is to understand the creep stress characterization of the thin film on substrate system with the three points bending creep test method, which plays an important role in the bending creep testing characterization, so as to provide some foundation on determination of interface properties of the thin film on substrate system by a bending creep testing. Finite element results shows that the influences of the thickness of thin film and the modulus ratio of thin film to substrate on stress distribution are important.     

Tribological characterization of TiCN coatings deposited by two crossed laser ablation plasma beams

The simultaneous laser ablation of two targets (graphite and titanium) in an Ar-N₂ gas mixture was carried out to deposit thin films of the ternary compound TiCN at room temperature. The base conditions used to produce the TiN without carbon were taken from our previous studies. The experimental conditions for the ablation of the carbon target were varied so that the carbon content in the films could be changed depending on the carbon ion energy. The control of the experimental conditions was carried out using a Langmuir planar probe which permitted the determination of the mean kinetic ion energy. The maximum hardness value of 35 GPa, was obtained with a carbon ion energy of about 250 eV, which corresponds to a film with 5 at% carbon content. In order to perform tribological and scratch tests, two types of substrate were used: nitrided AISI 316 stainless steel and AISI 316 stainless steel previously coated with a thin titanium layer (～50 nm). Values of the wear rate in the range of 1.39×10^?6 to 7.45×10^?5 mm³?N^?1?m^?1, friction coefficient from 0.21 to 0.28 and adhesion from scratch test measurements up to 80 N for final critical load, were obtained.     

Modeling of femtosecond laser damage threshold on the two-layer metal films

The heating processes of the single-layer gold thin film and the two-layer film assembly of gold padded with other metal (silver, copper and nickel) irradiated by femtosecond laser pulse are studied by the two-temperature model. It is found that the substrate metal can change energy transport, which is corresponding to the temperature changing process, and the thermal equilibrium time. Compared with the single-layer gold film at the same laser fluence, the two-layer film structure can change the damage threshold of the gold surface. Our results indicate that we can maximize the damage threshold of the gold film surface by altering the thickness ratio of the gold layer and the substrate layer in the two-layer film assembly.     

Fabrication and analysis of ZnO thin film bulk acoustic resonators

This study employs RF magnetron sputter technique to deposit high C-axis preferred orientation ZnO thin film on silicon substrate, which is then used as the piezoelectric thin film for a thin film bulk acoustic resonator (FBAR). Electrical properties of the FBAR component were investigated by sputtering a ZnO thin film on various bottom electrode materials, as well as varying sputter power, sputter pressure, substrate temperature, argon and oxygen flow rate ratio, so that structural parameters of each layer were changed. The experimental results show that when sputter power is 200 W, sputter pressure is 10 mTorr, substrate temperature is 300 °C, and argon to oxygen ratio is 4:6, the ZnO thin film has high C-axis preferred orientation. The FBAR component made in this experiment show that different bottom electrode materials have great impact on components. In the experiment, the Pt bottom electrode resonant frequency was clearly lower than the Mo bottom electrode resonant frequency, because Pt has higher mass density and lower acoustic wave rate. The component resonant frequency will decrease as ZnO thin film thickness increases; when top electrode thickness is higher, its resonant frequency also drops, due to top electrode mass loading effect and increased acoustic wave path. Therefore, ZnO thin film and top/bottom electrode thickness can be fine-tuned according to the required resonant frequency.     

ZnO nanorods/plates on Si substrate grown by low-temperature hydrothermal reaction

The zinc oxide (ZnO) nanorods/plates are obtained via hydrothermal method assisted by etched porous Al film on Si substrate. The products consist of nanorods with average diameter of 100 nm and nanoplates with thickness of 200-300 nm, which are uniformly distributed widely and grown perpendicularly to the substrate. The ZnO nanoplates with thickness of 150-300 nm were grown on Si substrate coated with a thin continuous Al film (without etching) in the same aqueous solution. The growth mechanism and room temperature photoluminescence (PL) properties of ZnO nanorods/plates and nanoplates were investigated. It is found that the introduction of the etched Al film plays a key role in the formation of ZnO nanorods/plates. The annealing process is favorable to enhance the UV PL emissions of the ZnO nanorods/plates.     

Optimal design for extending the lifetime of thin film luminescent solar concentrators

This study is concerned with the enhancement of the molecular, weathering stability of two models of thin film luminescent solar concentrators (LSCs). Two model systems of thin film LSCs had been proposed; the first model consists of a transparent PMMA/SiO₂ nanohybrid layer coated on a coumarin doped PMMA substrate. The second model designed as the ordinary configuration in which coumarin dye is dissolved in PMMA/SiO₂ nanohybrid layer then coated on a transparent PMMA substrate. The effect of nanosilica concentration on the prepared models was studied by TEM, SEM, DSC, FT-IR, UV–vis absorption and indoor photodegradation test. The obtained results suggested the first model for a durable design of thin film LSC applications specially in hot regions.     

nm量级薄膜厚度测量

 为了获得nm量级薄膜样品的精确厚度,采用软X射线反射率拟合方法、Bragg衍射方程方法和反射率Fourier变换方法分析了常规Cu靶X射线衍射数据及软X射线反射率数据。对厚度测量结果进行比较,3种方法得到的结果一致性很好。其中,软X射线反射率拟合和Bragg衍射方程方法精度很高,优于1 nm,Fourier变换方法精度稍低。对于单层W薄膜样品,3种方法获得厚度分别为(15.21±0.60) nm,(14.0±1.0) nm和(13.8±1.5) nm;对于双层W/C薄膜样品,W层厚度分别为(12.64±0.60) nm,(13.0±1.0) nm和(13.9±1.5) nm。这3种方法测量结果精度主要取决于反射率数据测量精度,而Fourier变换方法精度随着能量升高而提高,随着掠入射角范围增大而提高。