共振波长对导模共振生物传感器灵敏度的影响

导模共振生物传感器由于具有微型化、免标签、高通量和实时检测等优势被广泛研究。利用严格耦合波理论分析了该生物传感器对样品折射率和厚度的灵敏度随共振波长的变化规律。当样品厚度和共振波长一定时,其折射率灵敏度恒定;随着共振波长的增大,折射率灵敏度显著提高。当样品折射率和共振波长一定时,厚度灵敏度随着厚度的增加而降低,最后趋近于0;当共振波长增加时,厚度灵敏度明显提高,厚度测量范围增大。结果表明:选取较长的共振波长有利于样品的检测和分析。     

Integrated photonic glucose biosensor using a vertically coupled microring resonator in polymers

A photonic glucose biosensor incorporating a vertically coupled polymeric microring resonator was proposed and accomplished. The concentration of a glucose solution was estimated by observing the shift in the resonant wavelength of the resonator. For achieving higher sensitivity the contrast between the effective refractive index of the polymeric waveguide and that of the analyte was minimized. Actually, the effective refractive index of the polymeric waveguide (n = ∼1.390) was substantially close to that (n = ∼1.333) of the fresh solution with no glucose. The fabricated resonator sensor with the free spectral range of 0.66 nm yielded a sensitivity of ∼280 pm/(g/dL), which corresponds to ∼200 nm/RIU (refractive index units) as a refractometric sensor, and provided a detection limit of refractive index change on the order of 10⁻⁵ RIU.     

波长调制型表面等离子体共振的传感特性研究

表面等离子体共振(SPR)光学传感器能实现生物医学的快速、 无标记、 高精度检测,是生物化学分析的重要方法。 研制了基于波长调制型的Kretschmann结构表面等离子体共振(SPR)生物传感系统,研究了在体溶液传感方式下的传感性能。 利用不同浓度的乙醇和乙二醇溶液进行体溶液传感测试。 实验结果表明,在折射率低时共振波长对折射率变化响应的灵敏度低,但响应的线性度高;随着折射率增大,共振波长对折射率的响应变化的灵敏度提高。 在1.407 0～1.430 RIU折射率范围内,灵敏度高达11 487 nm·RIU-1。 传感器的共振波长的稳定性为0.213 8 nm,可分辨最小折射率趋近10-6 RIU。 所研制的波长调制型表面等离子共振传感器操作简单、 灵敏度高、 检测范围大,可实现浓度极低生物标记物的有效检测,在化学、 生物传感领域有重要的应用。     

Slot-waveguide biochemical sensor

We report an experimental demonstration of an integrated biochemical sensor based on a slot-waveguide microring resonator. The microresonator is fabricated on a Si3N4-SiO2 platform and operates at a wavelength of 1.3 microm. The transmission spectrum of the sensor is measured with different ambient refractive indices ranging from n=1.33 to 1.42. A linear shift of the resonant wavelength with increasing ambient refractive index of 212 nm/refractive index units (RIU) is observed. The sensor detects a minimal refractive index variation of 2x10(-4) RIU.     

基于表面等离子体共振的新型超宽带微结构光纤传感器研究

基于表面等离子体共振的微结构光纤传感器具有高灵敏、免标记和实时监控等优点.如今,由于此类传感器广泛应用于食品安全控制、环境检测、生物分子分析物检测等诸多领域而受到大量研究.然而,目前所报道的绝大多数此类传感器只能应用于可见光或近中红外传感.因此,对可应用于中红外传感的表面等离子体共振微结构光纤传感器的研究是一项极具挑战性的工作.基于此,本文设计了一种可以工作在近红外和中红外区域的新型高灵敏表面等离子体共振微结构光纤传感器.传感器采用双芯单样品通道结构,该结构不仅可以消除相邻样品通道间的相互干扰和提高传感器的信噪比,还可以在超宽带波长范围内实现高灵敏检测.采用全矢量有限元法对其传感特性进行了系统的研究,研究结果表明:当待测样品折射率分布在1.423—1.513范围内时,传感器不仅可以在1.548—2.796μm的超宽带波长范围内进行工作,而且其平均灵敏度高达13964 nm/RIU.此外,传感器的最高波长灵敏度和折射率分辨率分别为17900 nm/RIU,5.59×10^–7 RIU.     

Liquid refractive index sensor with three-cascaded microchannels in single-mode fiber fabricated by femtosecond laser-induced water breakdown

Liquid refractive index sensor with three-cascaded microchannels in single-mode fiber was fabricated by femtosecond laser-induced water breakdown. When the liquid is filled in three microchannels across the fiber core, the transmission spectrum of the sensor shows interference peaks. The refractive index of liquid can be sensed accurately based on both the wavelength shift and loss change of interference peaks. The refractive index sensitivities of wavelength shift and loss change reach to as high as ?2,406.1 nm/RIU and ?156.8 dB/RIU, respectively. The sensor is insensitive to the refractive index change of liquid caused by environmental temperature. It can be used for liquid refractive index sensing with high sensitivity, especially for water pollution monitoring.     

微纳光纤布拉格光栅折射率传感特性研究

利用光纤布拉格光栅方程和光纤基模有效折射率随纤芯半径和环境折射率的函数关系, 建立了微纳光纤布拉格光栅(MNFBG)反射波长随环境折射率变化的数学模型, 给出了波长灵敏度函数, 并指出MNFBG反射波长的变化规律决定于有效折射率随纤芯半径和环境折射率变化的关系. 详细探究了有效折射率及其灵敏度的变化规律, 结果表明: 有效折射率随纤芯半径和环境折射率的减小而非线性减小, 其对环境折射率变化的灵敏度随环境折射率的增大而非线性增加, 而且随纤芯半径减小, 有效折射率的灵敏度、线性度以及线性响应范围均呈递增规律. 通过对纤芯半径为0.5 μm的MNFBG在1.20–1.30和1.33–1.43 环境折射率范围内的波长响应关系拟合, 分别获得了477.33 nm/RIU和856.30 nm/RIU的波长灵敏度以及99.58 %和99.7%的高线性度, 论证了分析结论以及折射率区间划分测量方案的正确性, 为MNFBG折射率传感器的设计、优化以及应用提供了参考依据. 关键词： 微纳光纤 光纤布拉格光栅 折射率传感 数值模拟     

Two-photon induced photorefraction in undoped lithium tantalate crystals with different compositions

Two-photon interband photorefraction in undoped lithium tantalate crystals with composition ranging from 47.95 to 49.6 mol% of lithium oxide was demonstrated at the wavelength of 532 nm. The photorefractive properties were examined with holographic method. Two-photon holograms were recorded with high holographic sensitivity, large refractive index change, and fast hologram writing time. Permanent changes of the refractive index have been obtained. These holograms can be read nondestructively at the wavelength of 660 nm using heterodyne method. Holographic characteristics strongly depend on composition.     

反射式光纤表面等离子体波共振传感器特性研究

研究了一种基于表面等离子体波共振(SPR)光谱分析的折射率检测新方法。研究发现,表面等离子体波共振效应光谱特征的折射率灵敏度会随着液体性质变化而发生改变。根据折射率测量范围不同,分别选择共振波长和共振强度作为检测参量,实现理论折射率分辨力达到10~(-5)数量级以上。在理论分析和实验基础上,设计出一种基于共振光强检测的终端反射式光纤表面等离子体波共振效应传感系统,采用将传感信号和基准光信号的比值作为液体折射率变化的度量值。在1．3325～1．3991的折射率测量范围内,度量值与折射率之间呈现单调递减关系,线性相关系数为0．9983。通过定义耦合系数,还可实现对表面等离子体波共振效应效应强弱和变化趋势的评估。     

A high-sensitive fiber curvature sensor using twin core fiber-based filter

A high-sensitive fiber curvature sensor is proposed and experimentally demonstrated in a large measurement range by using a twin core fiber (TCF)-based filter as sensor head. Applying the coupled-mode theory and equivalent refractive index model, we theoretically anticipate the “blue shift” of the transmission dips of the TCF-based filter when sensor head is bent. Experimentally, we fabricate an 86.9 mm TCF-based filter with a free spectral range of 49 nm and characterize its curvature performance by measuring the wavelength shift. A nonlinear “blue shift” of the wavelength is observed when we increase the curvature. The relationship between wavelength shift and curvature is a second-order polynomial function. In the range from 0 to 9.30 m^?1, the maximum sensitivity is up to ?14.7 nm/m^?1. The measurement range can be further increased by selecting a shorter TCF.     

基于包层模的光纤布拉格光栅折射率传感特性

提出了基于光纤布拉格光栅(FBG)包层模式的折射率传感方案。实验中,利用不同浓度的丙三醇水溶液作为外界折射率传感溶液,采用氢氟酸溶液化学腐蚀的方法来减小光纤包层的直径以增大包层模式对外界折射率的敏感度,研究了腐蚀后光纤布拉格光栅包层模式的耦合波长对外部折射率的变化关系。实验结果表明在1.3300~1.4584的折射率范围内,包层模式耦合波长随外界折射率增大而增大,在接近光纤包层折射率处具有很高的折射率灵敏度,最大达到了172 nm/riu(refractive index unit)。而且,包层模谐振的光谱半峰全宽(约0.07 nm)仅为布拉格纤芯模谐振光谱半峰全宽的1/4,能够获得更好的传感精度。     

High sensitivity refractive index gas sensing enhanced by surface plasmon resonance with nano-cavity antenna array

The surface plasmon resonance gas sensor is presented for refractive index detection using nano-cavity antenna array.The gas sensor monitors the changes of the refractive index by measuring the spectral shift of the resonance dip,for modulating the wavelength of incident light.It is demonstrated that minute changes in the refractive index of a medium close to the surface of a metal film,owing to a shift in the resonance dip of the wavelength,can be detected.The average detection sensitivity is about 3200 nm/RIU(refractive index units),which is more than twice that of a metal grating-based gas sensor.The reflectivity of the surface plasmon resonance dip is only ～ 0.03%,and the full widths at half maximum(FWHMs) of bandwidth of the angle and wavelength are ～ 0.20° and 4.71nm,respectively.     

Trimming of microring resonators by photooxidation of a plasma-polymerized organosilane cladding material

As the complexity of microphotonic devices grows, the ability to precisely trim microring resonators becomes increasingly important. Photo-oxidation trimming uses UV irradiation to oxidize a cladding layer composed of polymerized hexamethyldisilane (6M2S) deposited with plasma-enhanced chemical vapor deposition (PECVD). PECVD 6M2S has optical properties that are compatible with microring devices, and its high cross linking renders it insoluble. Photo-oxidation decreases the refractive index of PECVD 6M2S by nearly 4%, permitting large resonance shifts that are not feasible with thermal trimming techniques. Resonance shifts from single-mode, 100 microm diameter Si3N4 (n =2.2) rings were as large as 12.8 nm for the TE mode and 23.5 nm for the TM mode.     

基于光纤M-Z干涉的高灵敏度液体折射率传感器的实验研究

提出并制备了一种基于Mach-Zehnder干涉效应的高灵敏度光纤液体折射率传感器.分别利用NaCl溶液和甘油溶液,研究了传感器的透射光谱和外界介质折射率的关系.实验结果表明,随着周围介质折射率的增大,传感器干涉谱的极小值点对应的波长向长波方向漂移,在1.333~1.356的折射率变化范围内,极小值点对应的波长的漂移量和折射率的变化具有较好的线性关系,对应的灵敏度约为4 086 nm/refractive-index.该传感器制作简单、结构紧凑,在生物和化学测量中具有较好的应用前景.     

基于光纤M-Z干涉的高灵敏度液体折射率传感器的实验研究

提出并制备了一种基于Mach-Zehnder干涉效应的高灵敏度光纤液体折射率传感器.分别利用NaCl溶液和甘油溶液,研究了传感器的透射光谱和外界介质折射率的关系.实验结果表明,随着周围介质折射率的增大,传感器干涉谱的极小值点对应的波长向长波方向漂移,在1.333～1.356的折射率变化范围内,极小值点对应的波长的漂移量和折射率的变化具有较好的线性关系,对应的灵敏度约为4 086nm/refractive-index.该传感器制作简单、结构紧凑,在生物和化学测量中具有较好的应用前景.     

Zygo interferometer for measuring refractive index of photorefractive bismuth silicon oxide (Bi12SiO20) crystal

An application of the Zygo system for measuring the refractive index of optical materials such as bismuth silicon oxide (BSO) having a higher value of the refractive index than that of glass is presented. The setting accuracy is found to be of the order of 1 μm in the Zygo phase measuring interferometer. The mean value of refractive index of BSO crystal measured by the interferometer for several samples of thickness in the range of 3–9 mm is 2.542 at a wavelength of 632.8 nm. The accuracy of measurement is ±0.002. It is possible to achieve an accuracy of ±0.0003 for a sample of thickness of 30 mm in the measurement of refractive index due to high setting accuracy of the Zygo system.     

有限包层半径光纤Bragg光栅的理论研究

采用光纤波导三层模型,对有限包层半径光纤Bragg光栅导模有效折射率的改变进行了理论分析,结果表明:当包层直径小于16μm时,单模光纤Bragg光栅(纤芯直径为8.3μm)的导模有效折射率才开始发生明显变化.在包层外添加外包层,通过改变外包层的折射率可以实现对光栅Bragg反射波长的调谐,同时对不同芯子直径的光栅Bragg波长移动进行了数值计算.在保证光纤归一化频率不变的前提下,芯径越小Bragg波长调谐范围越大,当包层厚度为1μm时,芯径为a＝2.2μm的光栅Bragg波长调谐范围约为3.9μm.     

Performance Investigation of Photonic Crystal-Based Microring Resonator for Optical Signal Processing

Abstract

A detailed theoretical analysis is presented to characterize wave propagation at 1,550 nm inside a glass (SiO₂) microring resonator implemented using photonic crystal technology. A photonic crystal reflection is used at each microring resonator corner to enhance the bending efficiency. The characteristics of both photonic crystal beam splitter and microring resonator bending losses are analyzed and investigated using both effective refractive index and finite difference time domain methods. Analytical expressions are also derived to describe the field enhancement inside the microring resonator, the transfer function of the microring resonator, and the main parameters characterizing the resonator such as resonator band width and quality factor. The analysis is also extended to characterize a drop filter implemented using photonic crystal-based microring resonator. The results indicate clearly that the effective refractive index method can give accurate results if one starts the calculations with finite difference time domain-estimated beam splitter parameters. Further, bending efficiency as high as 99% can be obtained using a ten-post layer photonic crystal mirror at each microring resonator corner.     

微米光纤耦合型环境折射率传感器

本文展示一种由两根微米光纤构成的耦合型环境折射率传感器。微米光纤表面存在倏逝波,芯外介质折射率微小的改变将引起倏逝场分布变化,从而导致能量在耦合器两臂中的重新分配。本文通过测量耦合器两端出射光功率的比值来对葡萄糖溶液的浓度进行传感,实验结果表明该微米光纤耦合型传感器的浓度传感灵敏度可达1.58 mol·L~(-1)。本文用耦合模理论详细分析了两根相邻微米光纤的耦合效率与芯外介质折射率之间的关系,发现减小耦合区的光纤的直径,增大入射光波长或增大耦合长度,都可以进一步提高这种传感器的灵敏度。     

Optimal design of temperature-insensitive long period fiber gratings for athermal refractive-index sensor

Based on coupled-mode theory of long-period fiber grating (LPFG), a theoretical analysis and simulations for the optimal design of a temperature-insensitive LPFG is presented in order to achieve an athermal condition for sensing the refractive index of the external medium. Effects of the variation of the cladding radius and grating period on the temperature sensitivity of the LPFG are discussed. Both of these parameters are found to be important to control the temperature sensitivity when the thermo-optic coefficients of core and cladding materials are of the same order. Other grating parameters are also optimized in order to achieve a good contrast of the grating period with resonance wavelength in the 1.5 μm region and to sense the external medium refractive index over a wide range. Variation of external medium refractive index from 1.0 to 1.45 results a red-shift in the LPFG resonance wavelength by 86 nm with its temperature sensitivity as low as 0.008 nm/°C over a temperature range of 0–80 °C for this optimally designed LPFG.