A melt depth prediction model for quality control of laser surface glazing of inhomogeneous materials

This paper reports on an investigation into the development of an analytical model for the quality control of laser marking/engraving of clay tiles using a high-power diode laser (HPDL). An analytical model for the laser melting of inhomogeneous workpieces with parabolic melt pool geometry being assumed was developed. The theoretical results were compared with the experimental data. The predicted melt pool depth and the experimental values were in close correlation with the parameter for values less than 15 Wmm⁻¹ s^−1/2, in spite of simplifications introduced in the model. At the relatively large values of parameter the assumption of parabolic melt pool shape and one-dimensional heat transfer no longer holds true.     

Study of a line width estimation model for laser micro material processing using a photodiode

Estimation of the line width for a laser marking on the silicon wafer is very important to improve the productivity of the final product which use nonpackaged chip. Until now, only theoretical and numerical estimation models have been studied. However, it is not easy for these models to apply to real systems. In this study, a process monitoring system was used to develop an estimation model for the laser marking width. The plasma produced by interaction between the laser and the wafer was measured using an optical sensor. For each laser power setting, the correlation between the signal acquired from the optical sensor and the resulting line width was analyzed. Estimation models were developed for laser marking width through statistical regression analysis and an artificial neural network algorithm.     

Effects of process variables on laser direct formation of thin wall

In this paper, effects of process variables on wall thickness, powder primary efficiency and speed of forming a thin metallic wall in single-pass coaxial laser cladding are investigated, and some resolution models are established and testified experimentally. With some assumptions, each of wall thickness, powder primary efficiency and formation speed can be defined as a function of the process variables. Wall thickness is equal to width of the molten pool created in single-pass laser cladding and determined by laser absorptivity, laser power, initial temperature, scanning speed and thermo-physical properties of clad material. Powder primary efficiency and formation speed are both dependent on an exponential function involving the ratio of melt pool width, which is decided by the process variables, to powder flow diameter. In addition, formation speed is influenced by powder feed rate. In present experiment, a 500 W continual-wave (CW) CO₂ laser is used to produce thin-wall samples by single-pass coaxial laser cladding. The experimental results agree well with the calculation values despite some errors.     

Laser marking using organo-metallic films

In this work, the technical aspects of laser marking using organo-metallic films of different compositions are reported. Orasols of different types and palladium (II) acetate are used, for the first time, to produce permanent markings of various colors on different substrates. Ceramic and plastic substrates were used. The deposition process is a photothermal process and the markings were carried out using an argon ion laser operating at λ = 514 nm. Two laser marking techniques are used with the orasol dyes and palladium (II) acetate. The first of these two techniques is mask marking, where laser light is projected onto a workpiece through a mask replicating the information to be marked. The second technique applied is real-time motion marking. The workpiece was translated under the stationary laser beam using a programmable stage translator. For both techniques, optimum marking parameters (scanning speed/exposure time, power, and deposited line width) are reported along with typical examples.     

Heat transfer modelling and stability analysis of selective laser melting

The process of direct manufacturing by selective laser melting basically consists of laser beam scanning over a thin powder layer deposited on a dense substrate. Complete remelting of the powder in the scanned zone and its good adhesion to the substrate ensure obtaining functional parts with improved mechanical properties. Experiments with single-line scanning indicate, that an interval of scanning velocities exists where the remelted tracks are uniform. The tracks become broken if the scanning velocity is outside this interval. This is extremely undesirable and referred to as the “balling” effect. A numerical model of coupled radiation and heat transfer is proposed to analyse the observed instability. The “balling” effect at high scanning velocities (above ∼20 cm/s for the present conditions) can be explained by the Plateau-Rayleigh capillary instability of the melt pool. Two factors stabilize the process with decreasing the scanning velocity: reducing the length-to-width ratio of the melt pool and increasing the width of its contact with the substrate.     

Process monitoring of powder pre-paste laser surface alloying

Instead of the continuous powder delivery method using a powder feeder for thick layer laser cladding, pre-pasting of the alloying powder on the substrate is a widely used method to supply the coating powders into the melt pool for LSA. A method to monitor the process of laser surface alloying based on the infrared emission from the melt pool using infrared photodiodes was developed. The technique is solely aimed at the process of laser surface alloying using pre-paste metal powder on the substrate surface prior to laser melting. This monitoring technique is able to distinguish the existence or the absence of the pre-paste powder and the consistency of the laser surface alloying process. The technique is of low cost and is simple to implement into the process.     

Spectroscopic characterization of low-nickel copper welding with pulsed Nd:YAG laser

Effects of various operating parameters of 400 W pulsed Nd:YAG laser on welding of nickel-alloyed copper have been investigated. The induced plume spectra in case of using different assist gases and preheat temperatures have been analyzed and the effects of these key factors on melt features such as penetration depth, porosity and spattering have been attributed to the spectroscopic behavior of the plume. Moreover, the CuI electron temperature and its standard deviation as the spectroscopic responses of the plasma plume to various laser process parameters have been quantitatively evaluated at different average and peak powers and pulse energies. Also, the mentioned responses were utilized to justify the weld bead profile features, involving weld depth, width and their stabilities, at similar process parameters. The operating conditions of welding were optimized, regarding the results of spectroscopic observations and attributing them to the qualitative aspects of the melt pool.     

3-D finite element modeling of laser cladding by powder injection: effects of laser pulse shaping on the process

This paper introduces a 3-D transient finite element model of laser cladding by powder injection to investigate the effects of laser pulse shaping on the process. The proposed model can predict the clad geometry as a function of time and process parameters including laser pulse shaping, travel velocity, laser pulse energy, powder jet geometry, and material properties. In the proposed strategy, the interaction between powder and melt pool is assumed to be decoupled and as a result, the melt pool boundary is first obtained in the absence of powder spray. Once the melt pool boundary is obtained, it is assumed that a layer of coating material is deposited on the intersection of the melt pool and powder stream in the absence of the laser beam in which its thickness is calculated based on the powder feedrate and elapsed time. The new melt pool boundary is then calculated by thermal analysis of the deposited powder layer, substrate and laser heat flux. The process is simulated for different laser pulse frequencies and energies. The results are presented and compared with experimental data. The quality of clad bead for different parameter sets is experimentally evaluated and shown as a function of effective powder deposition density and effective energy density. The comparisons show excellent agreement between the modeling and experimental results for cases in which a high quality clad bead is expected.     

Determination of geometrical factors in Layerwise Laser Melting using optical process monitoring

Layerwise Laser Melting (LLM) is a layerwise production technique enabling the production of complex metallic parts. In the process a thin layer of powder is first deposited on a base plate. With the energy of a scanning laser beam this layer is melted at selected places, according to a predefined scanning pattern. After scanning, a new layer of powder is deposited on top of the previous layer and selectively melted. This sequence of depositing and scanning is repeated until the complete part is built. The local geometry surrounding the melt pool has a large influence on the processing behavior. For process control issues, this influence must be known and quantified, in order to determine a priori optimal processing conditions and to interpret measured melt pool radiation. In order to study the melt pool behavior, optical process monitoring of LLM has been applied using a high speed near-infrared CMOS camera and a large area silicon photodiode sensor. Data processing rates up to 10 kHz and real-time process monitoring are achieved using image and signal processing on a Field Programmable Gate Array (FPGA). Several case studies will be presented showing that the geometric influencing factors can be studied and quantified by analyzing the melt pool sensor output.     

Optimization of hybrid laser – TIG welding of 316LN steel using response surface methodology (RSM)

In the present study, the hybrid laser – TIG welding parameters for welding of 316LN austenitic stainless steel have been investigated by combining a pulsed laser beam with a TIG welding heat source at the weld pool. Laser power, pulse frequency, pulse duration, TIG current were presumed as the welding process parameters whereas weld bead width, weld cross-sectional area and depth of penetration (DOP) were considered as the process responses. Central composite design was used to complete the design matrix and welding experiments were conducted based on the design matrix. Weld bead measurements were then carried out to generate the dataset. Multiple regression models correlating the process parameters with the responses have been developed. The accuracy of the models were found to be good. Then, the desirability approach optimization technique was employed for determining the optimum process parameters to obtain the desired weld bead profile. Validation experiments were then carried out from the determined optimum process parameters. There was good agreement between the predicted and measured values.     

Influence of preheating and hematite content of clay brick pavers on the characteristics of lines marked with a Nd:YAG laser

This paper reports the clay brick pavers marking by vitrification with a continuous wave Nd:YAG laser (1064 nm). The influence of a preheating and the chemical composition of the bricks on the morphological, visual and dimensional characteristics was studied. The lines marked at room temperature resulted in a discontinuous green glassy phase due to the presence of defects. A remarkable reduction of the defect amount, resulting in smooth, gleaming and darker lines, was obtained when preheating the bricks at 350 °C. The green tone, width, depth and cross-section area of the lines depend on the bricks’ chemical composition and thermal condition, as well as, on the laser energy density. Thus, decorative patterns of good visual quality can be marked by laser vitrification on clay brick pavers preheated at 350 °C.     

CO2 laser heating of surfaces: Melt pool formation at surface

The melt pool formation during the heating of titanium and steel surfaces by a moving CO₂ laser beam is examined. The repetitive pulses are introduced in the simulations and the Marangoni effect in the melt pool is incorporated in the model study. The influence of laser scanning speed and the laser intensity parameter on the melt pool size is also considered. The enthalpy–porosity method is adopted to account for the phase change in the irradiated spot. It is found that the influence of laser scanning speed on the melt pool size is considerable, which is more pronounced for laser beam parameter β=1. The melt pool size is smaller for stainless steel as compared to that corresponding to titanium.     

Investigation on the direct laser metallic powder deposition process via temperature measurement

The direct laser metallic powder deposition process was investigated with the aid of a radiant thermometer by building thin walls. The measured infrared (IR) temperature signal showed good correlation with the deposition process and the quality of the deposited samples. The influence of the powder particle size and the z-increment on the quality of the deposited samples and the IR-temperature signal was examined. It was found that the particle size of the powders shows no significant influence on the measured IR-temperature signal and the deposition process. However, both the deposition process and the measured temperature signal depended strongly on the z-increment. The variation of the melt pool temperature and cooling rate resulted in an inhomogeneous dimension accuracy, microstructure and hardness of the deposited sample. An abnormal deposition process can be recognized by the IR-temperature signal.     

Combining wire and coaxial powder feeding in laser direct metal deposition for rapid prototyping

Powder and wire deposition have been used separately in many laser-cladding, rapid prototyping and other additive manufacturing applications. In this paper, a new approach is investigated by simultaneously feeding powder from a coaxial nozzle and wire from an off-axis nozzle into the deposition melt pool. Multilayer parts are built from 316L steel using a 1.5 kW diode laser and different configurations of the powder and wire nozzles are compared in terms of surface roughness, deposition rate, porosity and microstructure. The parts are analysed using scanning electron microscopy (SEM), X-ray diffraction (XRD) and optical microscopy techniques. Results show that deposition efficiency increased and surface roughness decreased with the combined process; some porosity was present in samples produced by this method, but it was 20-30% less than in samples produced by powder alone. Wire injection angles into the melt pool in both horizontal and vertical planes were found to be significant for attaining high deposition efficiency and good surface quality. Reasons for the final sample characteristics and differences between the combined process and the separate powder and wire feeding techniques are discussed.     

Laser produced melt pool: Influence of laser intensity parameter on flow field in melt pool

The flow field developed in the laser produced melt pool is investigated and the influence of the Marangoni effect on temperature field is examined. The experiment is carried out to trace the solidified melt pool geometry and the heating is simulated in line with the experimental conditions to predict the melt size in the irradiated region. In the simulations, the control volume approach is used incorporating the Marangoni effect. The enthalpy-porosity method is adopted to account for the phase change in the irradiated region. The study is extended to include the influence of the laser intensity parameter (β) on temperature and the flow field in the melt pool. It is found that the melt pool geometry and the flow field in the melt pool is influenced by the laser intensity parameter. In this case, the number of circulation cell formed in the melt pool is doubled for the intensity parameter 0.4≤β≤0.6. The predictions of the melt pool geometry agree well with the experimental data.     

Porosity formation and gas bubble retention in laser metal deposition

One of the inherent problems associated with laser metal deposition using gas-assisted powder transfer is the formation of porosity, which can be detrimental to the mechanical properties of the bulk material. In this work, a comprehensive investigation of porosity is carried out using gas atomised Inconel 718 powder. In the analysis, a clear distinction is made between two types of porosity; namely lack of fusion and gas porosity. The results show that the two types of porosity are attributed by different factors. The gas porosity, which is more difficult to eliminate than the lack of fusion, can be as high as 0.7%. The study shows that the gas porosity is dependent on the process parameters and the melt pool dynamics. The flotation of entrapped gas bubbles was analysed, showing that in a stationary melt pool the gas would be retained by Marangoni-driven flow. The overall Marangoni-driven flow of the melt pool is in the order of five times higher than the flotation effect, and this is the reason why the melt pool geometry would tend to dominate the flow direction of the gas bubbles. Through optimisation, the gas porosity can be reduced to 0.037%.     

Dynamic Rheology of Poly(3-hydroxybutyrate-co-4-Hydroxybutyrate) /Clay Biocomposites

Poly(3-hydroxybutyrate-co-4-hydroxybutyrate) [P(3HB-co-4HB)] composites filled with clay were prepared by a melt blending process. Dynamic rheology of the composites was measured by means of a rotational rheometer. The results showed that the interlayer spacing of the clay increased owing to the presence of the P(3HB-co-4HB) melt in the interlayer regions of the clay. The storage and the loss moduli of the composite samples increased with the increasing frequency, and decreased with the increasing temperature. The addition of the clay enhanced the oscillatory thinning behavior of the composite melts, and improved the processability of the P(3HB-co-4HB) melt. The decrease of the viscosity by increasing both frequency and temperature was feasible and effective for the composites with the clay contents of 1 and 2 wt.%.     

Analysis of hybrid Nd:Yag laser-MAG arc welding processes

In the hybrid laser-arc welding process, a laser beam and an electric arc are coupled in order to combine the advantages of both processes: high welding speed, low thermal load and high depth penetration thanks to the laser; less demanding on joint preparation/fit-up, typical of arc welding. Thus the hybrid laser-MIG/MAG (Metal Inert or Active Gas) arc welding has very interesting properties: the improvement of productivity results in higher welding speeds, thicker welded materials, joint fit-up allowance, better stability of molten pool and improvement of joint metallurgical quality. The understanding of the main relevant involved physical processes are therefore necessary if one wants for example elaborate adequate simulations of this process. Also, for an efficient use of this process, it is necessary to precisely understand the complex physical phenomena that govern this welding technique. This paper investigates the analysis of the effect of the main operating parameters for the laser alone, MAG alone and hybrid Laser/MAG welding processes. The use of a high speed video camera allows us to precisely characterize the melt pool 3D geometry such as the measurements of its depression and its length and the phenomena occurring inside the melt pool through keyhole-melt pool-droplet interaction. These experimental results will form a database that is used for the validation of a three-dimensional thermal model of the hybrid welding process for a rather wide range of operating parameters where the 3-D geometry of the melt pool is taken into account.     

Theoretical and experimental investigation into laser melting of steel samples

Among the available laser applications, laser melting has turned out to be a powerful technique for the production of mechanically improved surfaces. To enhance the understanding of the laser melting process investigations into modeling of the heating mechanism initiating the laser melting are necessary. In the present study, a mathematical modeling of the laser melting process is introduced and power require ments for the laser melting are predicted as functions of workpiece properties and velocity. Maximum melt width is predicted analytically and compared with the experimental results. In this regard, an experiment is conducted to melt the mild steel samples with a cw CO₂ laser at different power settings and workpiece velocities. It is found that the melt variables predicted from theory are in agreement with the experimental results.     

The effect of laser peak power and pulse width on the hole geometry repeatability in laser percussion drilling

In this work, the two main factors that influence the repeatability of the laser percussion drilling process are identified. Experimental parametric analysis was carried out to correlate the laser parameters with the repeatability of a laser percussion drilling process. The experiment was conducted using a flash lamp pumped Nd:YAG laser to drill 2 mm thick mild steel sheets. The relationship between the percentage standard deviation (PSD) of entrance hole diameter, hole circularity and the operating parameters is established. Thirty-five holes were drilled and analysed for each set of identical laser parameters. The PSD of entrance hole diameter ranges between 1.47% and 4.78% for an operating window of 3.5–7 kW peak power, and 1–3 ms pulse width. The circularity of the entrance hole (defined as the ratio between the minimum and maximum diameters of the hole) ranges from 0.94 to 0.87, and is found to correlate with repeatability. The work shows that higher peak power, and shorter pulse width gives better hole geometry repeatability. The effect of melt ejection on hole geometry repeatability is also investigated. Melt ejection and spatter formation have been found to contribute to the poor repeatability of the process.