γ-α相变中不同晶界特征下铁素体生长形貌的相场模拟

利用多相场模型模拟了奥氏体(γ)-铁素体(α)相变过程中不同晶界特征下铁素体晶粒的形貌与生长动力学.模型中通过能量梯度系数和耦合项系数的协同变化定量表达晶界能与晶界迁移率的各向异性,同时固定相场界面宽度来保证计算精度.模拟结果显示:随着原奥氏体晶界能与铁素体-奥氏体晶界能比值σ_(γ,γ)/σ_(α,γ)的增加,三叉相界面处的平衡角β减小,铁素体晶粒沿原奥氏体晶界与垂直于奥氏体晶界方向的生长速率差变大.铁素体与奥氏体晶粒间的晶粒取向越接近,铁素体生长越缓慢.模拟结果可描述铁素体晶粒生长形貌的多样性,与实验结果符合.     

奥氏体不锈钢焊缝中的声学仿真模型与全聚焦成像检测

声波在奥氏体不锈钢焊缝中传播时声束弯曲,为超声成像带来了困难。基于Ogilvy焊缝模型,建立了奥氏体不锈钢焊缝非均匀各向异性声场仿真模型,采用Dijkstra路径搜索算法对各向异性条件下的声传播路径和声传播时间进行了数值模拟和分析。在此基础上,采用Verasonics超声相控阵成像系统,进行了奥氏体不锈钢焊缝的全聚焦成像实验,采集全矩阵回波数据,并结合理论模型计算的声传播路径和相应的传播时间,进行了成像结果修正。结果表明,与均匀介质模型的全聚焦成像结果相比,基于该文模型的焊缝全聚焦成像检测结果具有更高的缺陷定位精度和分辨率,验证了该方法的可行性,为奥氏体不锈钢焊缝成像检测提供了新的思路。     

考虑晶粒分布的多晶体材料超声散射统一理论

现有超声散射统一理论可通过多晶体材料的微观结构和力学特性,实现全频域范围内衰减和相速度的正演建模,但其忽略晶粒尺寸分布的影响,进而降低了正演模型的计算精度.本文对不均匀介质的波动方程进行二阶Keller近似,用全频域格林函数推导介质中的平均波;以截断对数正态分布描述晶粒分布,构建加权的空间相关函数;结合材料的弹性模量协方差,建立含晶粒分布的超声散射统一理论,揭示晶粒分布对超声散射的影响规律;制备304不锈钢试块并开展超声散射实验.结果表明考虑晶粒分布特性后,纵波衰减谱和相速度谱相对于实验结果的相异性降低约49%和64%,横波衰减谱和相速度谱相对于实验结果的相异性降低约12%和4%.可见,本文的统一理论模型能有效修正晶粒分布导致的衰减谱和相速度谱偏差,为晶粒分布反演评价提供理论基础.     

多层奥氏体钢中超声相控阵辐射声场分析

针对一维线性超声相控阵透过楔块,在多层不同晶轴取向的奥氏体钢中的声场辐射问题,结合高斯声束等效点源模型以及基于时间最小原理的射线追踪法,给出了各层介质中透射声场的计算方法。将奥氏体钢近似为横向各向同性介质,计算了相控阵透过楔块,在晶轴取向为0°的奥氏体钢中的无延时纵波声场,计算结果与COMSOL仿真结果相吻合,从而验证了所用方法的正确性。通过加入不同的延迟法则,仿真计算了三层含有不同晶轴取向(0°,30°,100°)的奥氏体钢中的纵波声场,实现了相控阵声场的偏转与聚焦,分析了偏转声场与聚焦声场的传播特性。仿真结果表明,不同的晶轴取向将导致不同的声束偏转以及聚焦效果。通过延迟激励各阵元,虽然可以控制声束偏转或聚焦到预定位置,但是晶轴取向仍会对声束宽度以及幅值产生一定的影响。      

流体饱和多孔圆柱体的声波散射

依据BiotStoll的流体饱和多孔媒质声传播理论,考虑了流体粘滞和骨架非弹性损耗引起的衰减因素,研究了多孔圆柱体对平面声波的散射特性.计算了在开孔和闭孔状态下多孔圆柱的背向散射形式函数和散射声强的方向分布,以及边界处的力学状况和声传播中的损耗因素对散射特性的影响.利用宽带超声实验系统测量了多孔圆柱的背向散射谱.实验测量结果与理论预计值符合得较好 关键词：     

声发射衰减特性管道泄漏定位方法

声发射技术具有灵敏度高、实时性强、覆盖范围大等优点.泄漏产生的声发射波沿管壁传播会发生衰减,通过研究衰减系数与金属晶粒散射和热流损失的关系,建立准确的声发射能量衰减模型.在此基础上,针对声发射频带宽的特点对传统衰减定位模型进行改进,提出宽频带声发射源定位模型,该方法先通过实验确定泄漏信号频带,再将滤波后的信号经过小波包...     

室温至液氢温区奥氏体不锈钢力学性能分析

奥氏体不锈钢在低温工程中广泛使用,正逐渐成为新兴氢能产业中液氢储运容器、输送管路等的首选材料。本文收集了奥氏体不锈钢从室温到液氢温区的力学数据,综合分析了低温下其力学性能的变化规律,阐述了其低温力学性能变化机理,包括化学成分、晶粒尺寸和应变率等因素对奥氏体不锈钢力学性能的影响规律。研究结果表明：随着温度的降低,奥氏体不锈钢屈服强度和抗拉强度增加,塑性和冲击韧性降低,断裂韧性改善,     

基于蒙特卡罗原理的混合颗粒三相体系声衰减计算模型研究

从单个固体和液滴颗粒的声吸收和散射特性计算入手,基于概率统计的蒙特卡罗方法(MCM),将声波以离散化的声子加以处理,通过追踪其运动历程并进行事件统计,建立一种气体介质中球形混合颗粒的声衰减预测模型.对空气中铝粉颗粒和亚微米级水滴的声衰减分别计算和验证后,将模型推广至含有混合颗粒的三相体系,对铝粉和液滴构成的单、多分散混合颗粒体系进行数值研究.结果表明:两类颗粒的声吸收特性差异明显,其散射声压均随颗粒无因次尺寸kR的增加呈现从后向散射占主要地位逐渐过渡到前向增强的趋势.气液固混合颗粒三相体系中,颗粒类型对于声衰减影响明显、且随浓度的增加不同颗粒的衰减贡献不再遵循随混合比的线性递变关系;对于多分散体系而言,声衰减谱受平均粒径影响较大,对于粒径分布宽度参数则不敏感.模型可进一步结合数学反演形成混合颗粒体系测量的理论基础.     

表面粗糙度对固体内部超声背散射的影响

超声背散射法可通过多晶体金属内部的空间方差信号,实现微观结构参数的无损评价,但表面粗糙度对评价模型的精度及实用性存在显著影响.基于高斯声束理论推导垂直入射粗糙界面的纵波声场,以此研究声能的Wigner分布规律;在超声的波长远大于粗糙度的前提下,构造表面粗糙度修正系数,并建立粗糙界面的单次散射响应模型,揭示粗糙度对超声波背向散射的影响规律.用304不锈钢制备轮廓均方根值为0.159μm的光滑试块和25.722μm的粗糙试块开展超声背散射实验,结果表明模型在粗糙度修正前后均可实现光滑试块的晶粒尺寸有效评价,但未经修正的传统模型对粗糙试块的晶粒尺寸评价结果与金相法结果的相对误差高达-21.35%,而本模型的评价结果与金相法结果符合得很好,相对误差仅为1.35%.可见,本模型能有效补偿粗糙度引起的超声背散射信号衰减,从而提高晶粒尺寸无损评价的精度.     

各向异性焊缝中超声相控阵瞬态声场仿真及缺陷定位方法

针对多层各向异性奥氏体不锈钢焊缝中超声相控阵瞬态声场的仿真问题,提出应用高斯声束等效点源模型计算宽带离散化的多个单频稳态声场,通过傅里叶变换将其拓展为瞬态声场,并分析了声场转换过程的主要影响参数.该方法可快速计算焊缝内部超声相控阵聚焦声场的瞬态能量分布和任意一点的时域波形信号.在此基础上针对多层奥氏体不锈钢焊缝内部缺陷...     

Multi-phase field simulation of grain growth in multiple phase transformations of a binary alloy

This work establishes a temperature-controlled sequence function, and a new multi-phase-field model, for liquid–solid–solid multi-phase transformation by coupling the liquid–solid phase transformation model with the solid–solid phase transformation model. Taking an Fe–C alloy as an example, the continuous evolution of a multi-phase transformation is simulated by using this new model. In addition, the growth of grains affected by the grain orientation of the parent phase(generated in liquid–solid phase transformation) in the solid–solid phase transformation is studied. The results show that the morphology of ferrite grains which nucleate at the boundaries of the austenite grains is influenced by the orientation of the parent austenite grains. The growth rate of ferrite grains which nucleate at small-angle austenite grain boundaries is faster than those that nucleate at large-angle austenite grain boundaries. The difference of the growth rate of ferrites grains in different parent phase that nucleate at large-angle austenite grain boundaries, on both sides of the boundaries, is greater than that of ferrites nucleating at small-angle austenite grain boundaries.     

Anisotropy of ultrasonic backscatter and attenuation from human calcaneus: implications for relative roles of absorption and scattering in determining attenuation

Although bone sonometry has been demonstrated to be useful in the diagnosis of osteoporosis, much remains to be learned about the processes governing the interactions between ultrasound and bone. In order to investigate these processes, ultrasonic attenuation and backscatter in two orientations were measured in 43 human calcaneal specimens in vitro at 500 kHz. In the mediolateral (ML) orientation, the ultrasound propagation direction is approximately perpendicular to the trabecular axes. In the anteroposterior (AP) orientation, a wide range of angles between the ultrasound propagation direction and trabecular axes is encountered. Average attenuation slope was 18% greater while average backscatter coefficient was 50% lower in the AP orientation compared with the ML orientation. Backscatter coefficient in both orientations approximately conformed to a cubic dependence on frequency, consistent with a previously reported model. These results support the idea that absorption is a greater component of attenuation than scattering in human calcaneal trabecular bone.     

On the nucleation of cementite on bainitic ferrite–austenite interphase boundaries

Among all possible variants of the Isaichev orientation relationship between cementite and ferrite, a single major cementite variant has been observed to appear in bainite. Interphase boundary nucleation of cementite on ferrite–austenite semi-coherent interfaces is considered a plausible reason for this observation. With the aid of known crystallographic relations and habit planes of the ferrite–cementite, ferrite–austenite and austenite–cementite phases, a model for cementite nucleation has been proposed. The interphase-boundary nucleus is assumed to form on a semi-coherent ferrite–austenite interface and to possess ferrite–cementite and austenite–cementite habits as two main facets of the nucleus. It is shown that interphase cementite nucleation will be viable if the energies of all facets of the nucleus are in the semi-coherent range.     

Researches on the ultrasonic scattering attenuation of carbon fibre reinforced plastics with 2D real morphology void model

In order to investigate the ultrasonic propagation in carbon fibre reinforced plastics with complex void morphology, the effective mathematical model needs to be established. The current models are oversimplified on void morphology, leading to the significant inconsistency of theoretical calculation with experimental results. In view of the problem, a real morphology void model (RMVM) was established with the idea of image-based modeling. The void morphology was extracted by digital image processing technology, and the material properties were assigned subsequently. As a result of the complex and random void morphology in RMVMs, a non-unique corresponding relationship was verified between porosity P and ultrasonic attenuation coefficient α. In the scatterplot of simulation, about 66 percent of points were plotted within the ±10% error band of fitting line, while almost all the data located at the ±20% error zone. The simulation results showed good consistency with experiments, and it proved the validity of RMVM. The investigation provides a novel model to explore the ultrasonic scattering mechanism for the composite materials containing random voids.     

The effect of bone structure on ultrasonic attenuation and velocity

The relationship between the structure of bovine cancellous bone, and its ultrasonic propagation parameters is investigated by means of a novel technique involving the application of large static loads, thereby changing the porosity in a controlled manner. The results show that for frequencies in the range 0.4 to 1 MHz, porosity decreases up to 35% are associated with a reduction in attenuation of up to 500%, whereas the velocity increases by roughly 35% for the same changes. The data taken overall suggest that in determining the ultrasonic attenuation coefficient at these frequencies, the amount of material in a given bone section is significantly less important than the distribution of that material.     

Five-parameter crystallographic characteristics of the interfaces formed during ferrite to austenite transformation in a duplex stainless steel

The crystallography of interfaces in a duplex stainless steel having an equiaxed microstructure produced through the ferrite to austenite diffusive phase transformation has been studied. The five-parameter interface character distribution revealed a high anisotropy in habit planes for the austenite–ferrite and austenite–austenite interfaces for different lattice misorientations. The austenite and ferrite habit planes largely terminated on (1 1 1) and (1 1 0) planes, respectively, for the austenite–ferrite interfaces associated with Kurdjumov–Sachs (K–S) and Nishiyama–Wasserman (N–W) orientation relationships. This was mostly attributed to the crystallographic preference associated with the phase transformation. For the austenite–ferrite interfaces with orientation relationships which are neither K–S nor N–W, both austenite and ferrite habit planes had (1 1 1) orientations. Σ3 twin boundaries comprised the majority of austenite–austenite interfaces, mostly showing a pure twist character and terminating on (1 1 1) planes due to the minimum energy configuration. The second highest populated austenite–austenite boundary was Σ9, which tended to have grain boundary planes in the tilt zone due to the geometrical constraints. Furthermore, the intervariant crystallographic plane distribution associated with the K–S orientation relationship displayed a general tendency for the austenite habit planes to terminate with the (1 1 1) orientation, mainly due to the crystallographic preference associated with the phase transformation.     

钢铁材料中形变诱导相变超细化机理研究

通过计算机编程建立奥氏体相中12[1 1 0]刃位错、奥氏体相中非形变区和形变区奥氏体/铁 素体相界模型.用实空间的连分数方法计算了非形变区和形变区奥氏体/铁素体相界界面能， 计算了碳、氮及微合金元素在完整晶体及位错区引起的环境敏感镶嵌能，进而讨论形变过程 中铁素体形核的难易程度，碳、氮及合金元素在位错区的偏聚及析出与铁素体细化的关系. 计算结果表明：α-Fe易于在高密度位错区（形变带、亚晶界、晶界）形核，在奥氏体形变 过程中，就会大大提高α-Fe形核率，细化铁素体晶粒；碳、氮和微合金元素易于单独或共 同 关键词： 奥氏体/铁素体相界 刃位错 形变 晶粒细化     

Modelling the attenuation in the ATHENA finite elements code for the ultrasonic testing of austenitic stainless steel welds

Multipass welds made in austenitic stainless steel, in the primary circuit of nuclear power plants with pressurized water reactors, are characterized by an anisotropic and heterogeneous structure that disturbs the ultrasonic propagation and makes ultrasonic non-destructive testing difficult. The ATHENA 2D finite element simulation code was developed to help understand the various physical phenomena at play. In this paper, we shall describe the attenuation model implemented in this code to give an account of wave scattering phenomenon through polycrystalline materials. This model is in particular based on the optimization of two tensors that characterize this material on the basis of experimental values of ultrasonic velocities attenuation coefficients. Three experimental configurations, two of which are representative of the industrial welds assessment case, are studied in view of validating the model through comparison with the simulation results. We shall thus provide a quantitative proof that taking into account the attenuation in the ATHENA code dramatically improves the results in terms of the amplitude of the echoes. The association of the code and detailed characterization of a weld’s structure constitutes a remarkable breakthrough in the interpretation of the ultrasonic testing on this type of component.