Low-carbon steel samples deformed by cold rolling—analysis by the magnetic adaptive testing

Three series of samples of low-carbon steel were investigated by the method of magnetic adaptive testing (MAT). The samples were plastically deformed by cold rolling to five consecutive stages of deformation. Samples in one series were magnetically closed, those in the other two series were magnetically open. The presented results of MAT - typical by its low required magnetization of the samples - show highly sensitive and reliable correlation with plastic deformation and as a consequence also with mechanical embrittlement of the investigated material, regardless of the sample shape.     

Nondestructive indication of plastic deformation of cold-rolled stainless steel by magnetic minor hysteresis loops measurement

Cold-rolled austenitics stainless steel samples were non-destructively characterized by means of sets of magnetic minor hysteresis loops. The flat samples were magnetized by an attached yoke, and reliable parameters were obtained from the series of minor loops, without magnetic saturation of the samples. It was found, that some magnetic quantities, well known to be closely connected to the samples’ structure variation, especially relative coercivity and remanent induction, could be distinguished even more sensitively from minor loops, than from the major one.     

Evaluation by means of magneto-acoustic emission and Barkhausen effect of time and space distribution of magnetic flux density in ferromagnetic plate magnetized by a C-core

Experimental results are shown of magneto-acoustic emission (MAE) and Barkhausen effect (BE) for two ferritic steel plates of different dimensions. The paper presents preliminary results of modelling the MAE, based on the finite element method (FEM), taking into account the key role of the eddy currents. Explanations are suggested as to the effects of MAE peak maximum growth, shift, as well as the characteristic BE profiles at the bottom of the large plates.     

Investigation of applicability of extrapolation method for sample field determination in single-yoke measuring setup

In this work the single-yoke measuring technique is proposed to be optimized by extrapolation of a magnetic field profile to the sample surface for determination of the “real” field inside the sample. It has been shown that this approach gives reasonable values of magnetic parameters and allows to solve the well-known problem of considerable fluctuations of the measurement results due to imperfections of the yoke–sample contact. The magnetization process with the single-yoke setup is considered on basis of the surface field measurements around the sample and their extrapolation to the sample surfaces. Advantages as well as drawbacks of the measuring procedure and of the suggested optimization method are discussed.     

Governing conditions of repeatable Barkhausen noise response

The paper is devoted to the establishment of experimental conditions, which ensure the repeatability of magnetic Barkhausen noise testing in practice. For this task, the measurements were performed on open flat samples using different experimental configurations, including: different magnetization frequencies, sampling rates, and filter cut-off frequencies; using a sample-wrapped coil and using attached pick-up coils of various dimensions, with different lift-offs of a single yoke magnet and of the attached coil. The sample magnetization was controlled by a vertical array of three Hall sensors; their readings were extrapolated to the sample surface to precisely define its field. After analysis of the results, a scheme for an optimized sensor with a controlled field waveform was suggested to improve the measurement repeatability. The important issues of signal processing and parameter applicability were also discussed in detail.     

Influence of rate of change of magnetization processes on sensitivity of magnetic adaptive testing

The rate of change of magnetizing field (field-slope), applied for the nondestructive method of magnetic adaptive testing, influences both signal-to-noise ratio and sensitivity of the chosen magnetic parameters with respect to the investigated degradation of the ferromagnetic material (degradation functions). Dependence of the degradation functions sensitivity on the field-slope is analyzed in this paper. It is shown that whereas sensitivity of the top-responsive degradation functions from around the top permeability of the nondegraded (reference) material drops down with increasing field-slope, sensitivity of the mild-responsive degradation functions from regions with lower permeability of the reference material is frequently field-slope-independent. The most favorable choice of the best degradation functions and of the proper magnetizing field-slope remains to be a question of optimum adaptation of the tests both to the investigated material and to the applied measuring technique.     

The influence of plastic deformation on the magnetoelastic properties of the CSN12021 grade steel

Magnetoelastic properties of materials are strongly influenced by changes of the dislocation structure that take place during the process of plastic deformation. Such changes can be used as a basis for a method of nondestructive evaluation (NDE) of the deformation level. So far, various methods, based on magnetic hysteresis loop properties as well as on the Barkhausen effect (BE), have been proposed. In the paper, the results obtained with the help of the abovementioned methods are compared with the results of the magnetoacoustic emission (MAE) signal measurements. The MAE signal is relatively easy to implement as a nondestructive method and unlike the BE effect signal gives information about the whole magnetized volume.     

Magnetic characterization of HSLA steel by power-law decay exponents of Barkhausen emission signal

The general trend of magnetic behaviour of materials is that the mechanically hard materials are also magnetically hard. However for the high strength low alloy (HSLA) steel tempered at various aging temperatures, the correlation was reported as negative. The anomaly could not be explained by the magnetic parameters like RMS voltage calculated from the Barkhausen emission signal and the coercivity from the magnetic hysteresis loop. This paper reports another magnetic parameter known as power-law decay exponent which shows excellent correlation with the mechanical properties and thus explains the progressive evolution of the microstructural constituents in HSLA steel.     

Magnetic hysteretic characterization of the irradiation-induced embrittlement of Fe,Fe–Cu model alloys,and reactor pressure vessel steel

Neutron irradiation is known to cause embrittlement of iron-based materials; in the nuclear industry, this effect can be detrimental for reactor pressure vessel steels. In this paper, we investigate the variations of the magnetic hysteretic behavior due to neutron irradiation, for four materials, i.e. nominally pure Fe, Fe-0.1 wt% Cu and Fe-0.3 wt%Cu model alloys, and a reactor pressure vessel steel, JRQ A533-B. Two parameters related to the magnetization loop shape, i.e. maximum relative differential permeability and peak intensity of local interaction field distribution, are measured as a function of neutron fluence. For all materials both parameters decrease with increasing fluence, due to the irradiation-induced formation of nano-size defects. This decreasing trend in magnetic parameters during embrittlement is noticeable regardless the origin of the embrittlement, which can be only Cu-precipitation (thermal aging of Fe–Cu), only matrix damage (irradiation of pure Fe), or both mechanisms (irradiation of Fe–Cu or steel). The magnetic parameters relatively change up to 40%, which indicates the potential of magnetic characterization to assess irradiation-induced material hardening and embrittlement.     

Lean non-oriented electrical steel grades

A “Lean Grade Policy” has been adopted involving reduced losses of a given steel composition and supplied grades with typical losses closer to the guarantees. Increased final annealing temperatures and modified hot rolling have resulted in reduced losses and improved permeability. A “lean grade” will have higher heat conductivity and permeability compared to a “standard grade”. The policy could result in less variability and better quality control.     

Quantitative determination of Eu and Eu content in (Eu,Y)-Si-Al-O-N glasses by magnetic measurements

This paper describes a method to determine the oxidation state of europium by means of magnetic measurements. The feasibility of this method is demonstrated using Eu-doped Y-Si-Al-O-N glasses as a model system. Magnetic measurements at (Eu,Y)-Si-Al-O-N glasses show that Eu is completely present as divalent ion for low Eu concentrations (Eu_0.152Y_15.0Si_14.7Al_8.7O_54.1N_7.4). At high Eu concentrations (Eu_15.2Si_14.7Al_8.7O_54.1N_7.4) a maximum of 5 at.% could be present as Eu³⁺.     

Investigations of the first order magnetic phase transition in dysprosium

The first order magnetic phase transition in polycrystalline sample of dysprosium (Dy) has been investigated in detail by dc-resistance vs. temperature (R-T) measurements. Distinct signature of coexistence of two magnetically ordered phases (i.e. ferromagnetic and antiferromagnetic), originating as a result of the metastable behavior associated with the first order phase transition (FOPT) is found near 90 K. By successfully recording the minor hysteresis loops within the hysteretic R-T regime of Dy, a varying degree of phase coexistence in the FOPT is demonstrated.     

Importance of punching and workability in non-oriented electrical steel sheets

In order to reduce energy loss in motors, the use of high-efficiency non-oriented electrical steel sheets and an optimal motor core design are important. It is also crucial to minimize the deterioration of magnetic properties during the motor core manufacturing process. Accordingly, this report evaluates the effects of cutting and clamping methods on the deterioration factors of motor cores. Magnetic properties are largely influenced by both cutting and clamping methods. While it is difficult to avoid cutting and clamping altogether, it is necessary to adopt suitable production conditions and minimize the deterioration involved.     

Effects of the degree of grain alignment on the hard magnetic properties of sintered NdFeB magnets

r increases monotonously with an enhancement in the degree of grain alignment (i.e. decrease in the orientation coefficient σ), whereas the intrinsic coercivity _jH_c decreases monotonously. This dependence leads to a non-monotonic behaviour of the magnetic-inductive coercivity _bH_c and a saturation of the maximum energy product (BH)_max. Received: 28 August 1997/Accepted: 12 January 1998     

Giant magnetic moments in dilute magnetic semiconductors

The concentration dependence of the specific magnetic moment value at room temperature in dilute semiconductor titanium oxides doped with either Co or Fe has been investigated. This value was found to increase sharply at small concentrations of magnetic impurity. The magnetic moment of 22.9 μ_B per impurity atom has been revealed for TiO₂ doped with 0.15 at% Co, not yet reported in any semiconductor oxide systems. We conclude the observed giant magnetic moments are caused by the crystal lattice polarization at small impurity concentrations. The comparison with published data point to different types of the magnetization concentration dependence for various semiconductor matrixes that is probably related to the dielectric permittivity of the environment.     

Formation mechanism of ferromagnetism in Si1−xMnx diluted magnetic semiconductors

Si_1−xMn_x diluted magnetic semiconductor (DMS) bulks were formed by using an implantation and annealing method. Energy dispersive X-ray fluorescence, transmission electron microscopy (TEM), and double-crystal rocking X-ray diffraction (DCRXD) measurements showed that the grown materials were Si_1−xMn_x crystalline bulks. Hall effect measurements showed that annealed Si_1−xMn_x bulks were p-type semiconductors. The magnetization curve as a function of the magnetic field clearly showed that the ferromagnetism in the annealed Si_1−xMn_x bulks originated from the interaction between interstitial and substitutional Mn⁺ ions, which was confirmed by the DCRXD measurements. The magnetization curve as a function of the temperature showed that the ferromagnetic transition temperature was approximately 75 K. The present results can help to improve understanding of the formation mechanism of ferromagnetism in Si_1−xMn_x DMS bulks.     

Hysteresis of two interacting magnetic pairs with inequivalent perpendicular anisotropy

We consider a model for magnetic memory that consists of strongly coupled dipolar or antiferromagnetic (AF) pairs with inequivalent perpendicular anisotropy _K1$K_1$ and _K2$K_2$. For appropriate parameter values, determined in this work, they have two inequivalent storage states with zero net magnetic moment. Both analytical and numerical calculations are performed, in some cases yielding different results because of relaxation effects (i.e., a dependence on the damping parameter α$\alpha$). Hysteresis loops for a wide variety of parameter values are obtained, both for the AF case and the dipole case. An Appendix gives analytic results for slightly non-collinear spins in an applied field, which were used to test the numerical results.