NaI（TI）对6．13MeV-γ射线的长管体源的探测效率的测量

导出了核动力反应堆一回路^16N的泄漏率与γ射线探测器的计数率、高压蒸气流速、^16N的衰变常量及其发射γ射线的概率和效率的关系式，并得出效率与高压蒸气流速和^16N的衰变常量等无关的结论．用发射6．13MeV-γ射线的PuC点源测量了NaI(TI)探测器对长管体源的相对效率的空间分布和参考点的绝对效率，据此计算出长管体源的效率，效率的测量值与MC法的计算值在7％之内符合．分析了6．13和7．12MeV-γ射线的效率差异对^16N泄漏率和Compton小角散射的次级γ射线对收敛长度的影响．     

不同射线能量及线衰减系数条件下体源探测效率的函数模型

基于放射性废物桶内所含介质材料和放射性核素分段均匀分布的假设, 采用蒙特卡罗程序模拟计算多种射线能量、多种样品密度条件下的线衰减系数和体源探测效率, 通过多元非线性拟合得到以线衰减系数和能量为自变量的体源探测效率函数。基于壳源法, 通过多个点源组合测试近似替代均匀体源的实验测量, 对3种能量射线和3种密度的样品进行验证实验, 利用蒙卡模拟与数值拟合结合方法和实验测量两种方式获得各自的体源探测效率, 完成活度估算。两种方式活度估算结果相对误差均小于23%。通过蒙卡模拟与数值拟合结合方法所得结果与实验结果基本吻合, 证明了该方法的有效性。     

闪烁探测器Nal(TI)对γ射线的光峰效率刻度

在辐射的探测与测量中,精确的效率刻度是绝对强度测量必不可少的步骤。本工作是为研究磁约束聚变装置(托卡马克)在放电过程中的逃逸电子成分及硬X射线绝对辐射强度而作的实验准备工作。     

Measurement of the total reaction cross section for the mirror nuclei ~(12)N and ~(12)B

The mirror nuclei ~(12)N and ~(12)B are separated by the Radioactive Ion Beam Line in Lanzhou (RIBLL)at HIRFL from the breakup of 78.6 MeV/u ~(14)N on a Be target. The total reaction cross-sections of ~(12)N at 34.9 MeV/u and ~(12)B at 54.4 MeV/u on a Si target have been measured by using the transmission method.Assuming ~(12)N consists of a ~(11)C core plus one halo proton, the excitation function of ~(12)N and ~(12)B on a Si target and a C target were calculated with the Glauber model. It can fit the experimental data very well. The characteristic halo structure for ~(12)N was found with a large diffusion of the protons density distribution.     

氮－14远程核四极共振谱仪

为了满足检测与探头有一定距离的含氮化合物的核四极共振信号，本文研制了一台结构简单，造价低廉的核四极共振操测仪．它利用了脉冲付里叶变换技术，可将获得的核自由感应衰减信号或者回波信号进行相干累加．整个系统分硬件和软件两大部分．前者由射频脉冲放大器（约５００Ｗ脉冲输出功率），探头，接收机，ＭＣＳ－９６型单片机和ＰＣ机构成．后者由单片机上的脉冲序列程序与ＰＣ机上的数值信号处理程序组成．利用这台谱仪，可以在几十秒时间内得到距离探头线圈１０ｃｍ内的典型￣（１４）Ｎ样品的核四极共振谱．     

FX-100核磁共振谱仪上的MLEV-16宽带去偶实验

本文叙述了在FX-100核磁共振谱仪上进行的MLEV-16宽带去偶实验。实验表明:其去偶范围大大增加,效率明显提高,对常规质子去偶的¹³C谱实验所需要的去偶场B₂比谱仪原有的噪声去偶系统的去偶场B₂降低约一个数量级。并且,用谱仪原有的去偶功率实现了¹³C{¹⁹F}氟宽带去偶的¹³C谱的观测,去偶范围达14KHz,可以满足大部分氟化物的¹³C核磁共振研究的要求。     

天然丰度的N-磷酰化氨基酸的15N NMR 研究

采用¹⁵N-¹H的2D HSQC、HMBC实验方法,测定了天然丰度的N-磷酰化氨基酸样品在溶液中的¹⁵N化学位移δ_N及偶合常数J_N-P,J_N-H. 实验表明：对于¹⁵N天然丰度样品,这是一种快速有效的实验方法. 研究发现：N-酰化后的氨基酸,其δ_N以及与氮原子直接相连的质子¹H的化学位移均发生十分明显的高场位移,而偶合常数¹J_N-P,¹J_N-H的变化与化合物构型相关联 .     

脂肪胺类化合物氨基15N NMR化学位移规律的研究

提出了计算脂肪胺类化合物的¹⁵N NMR化学位移的经验公式：δ_cal（¹⁵N）=-380.2+ΣΔα+ΣΔβ+ΣΔγ+ΣΔδ+ΣC,结合最小二乘法通过线性回归得到了11种取代基参数,计算结果以133种化合物的133个¹⁵N NMR化学位移数据为样本点进行回归检验,置信度为99.5 %,约有94.7 %的¹⁵N NMR化学位移计算值的计算误差小于5.0（相对误差小于0.5 %）.     

Symmetry Breaking in Finite Volume-a Study in the O(N) Model

Spontaneous symmetry breaking plays a crucial role in quantum field theories and it occurs only for systems with infinite degrees of freedom. For a system in a large but finite volume, although the symmetry is not broken spontaneously, an adiabatic approximation can be applied to study the would-be broken symmetry. Lattice O(N) model is studied within the Hamiltonian approach. It is shown that the low-lying spectrum of the system can be explained using an adiabatic, or Born-Oppenheimer approximation, which turns out to become 1 an expansion in the inverse power of volume. In the infinite volume limit, the symmetry is broken while in the finite volume the slow rotation of the zero-momentum mode restores the symmetry and gives rise to the rotator spectrum, which has been observed in real Monte Carlo simulations.     

KTP(001)晶体分光性能研究

根据同步辐射光源对软X射线分光晶体的性能要求,分析了软X射线能区常用分光晶体的性能优劣,指出对于晶格常数值大的分光晶体,KTP(KTiOPO₄)(011)是该能区比较理想的分光晶体. 同时提出了一种利用同步辐射光源测量晶体衍射效率的实验方法,指出光源的发散度与晶体的衍射效率密切相关. 测量了KTP(011)晶体的晶格常数,给出了KTP(011)晶体的实测衍射效率.关键词：同步辐射KTP(011)晶体衍射效率光源发散度     

A multi NaI(Tl) detector array for medium energyγ-ray spectroscopy

An array of seven hexagonal NaI(Tl) detectors has been set up for measuringγ-ray spectra in the energy region 5 MeV ≤E _γ ≤ 40 MeV with good accuracy. This is in contrast to earlier set ups which mostly used one large sized (about 10 inchesφ × 15 inches long)NaI(Tl) detector. This set up has been made for the study ofγ decay of GDR based on high spin states and ultra-dipole radiations. The array has been provided with the following features: a) TOF discrimination against neutrons, b) pile up detection and elimination, c) active and passive shielding to cut down background and d) an array of trigger counters for multiplicity dependence measurements. The well known program EGS4 has been used to determine the response of the array forγ-rays in the energy region 5–40 MeV and several test measurements have been carried out to confirm the validity of the calculated response functions. Some typicalγ-ray spectra fromα and¹⁶O induced reactions measured at VECC, Calcutta and Pelletron accelerator at TIFR are also shown.     

N2（A）及N（2D）对IF（X）的传能研究

在微波放电系统中,对NH_3-F-F_2-CF_3I体系进行研究,结果表明,向IF(X)传能的诸多媒介中,N_2(A)及N(~2D)起着主要作用,并且这一结论在经微波激发后的N_2与CF_3I的直接反应中得到了进一步证实。