Simultaneous droplet impingement dynamics and heat transfer on nano-structured surfaces

This study examines the hydrodynamics and temperature characteristics of distilled deionized water droplets impinging on smooth and nano-structured surfaces using high speed (HS) and infrared (IR) imaging at We = 23.6 and Re = 1593, both based on initial drop impingement parameters. Results for a smooth and nano-structured surface for a range of surface temperatures are compared. Droplet impact velocity, transient spreading diameter and dynamic contact angle are measured. The near surface average droplet fluid temperatures are evaluated for conditions of evaporative cooling and boiling. Also included are surface temperature results using a gold layered IR opaque surface on silicon. Four stages of the impingement process are identified: impact, boiling, near constant surface diameter evaporation, and final dry-out. For the boiling conditions there is initial nucleation followed by severe boiling, then near constant diameter evaporation resulting in shrinking of the droplet height. When a critical contact angle is reached during evaporation the droplet rapidly retracts to a smaller diameter reducing the contact area with the surface. This continues as a sequence of retractions until final dry out. The basic trends are the same for all surfaces, but the nano-structured surface has a lower dissipated energy during impact and enhances the heat transfer for evaporative cooling with a 20% shorter time to achieve final dry out.     

Experimental study on turbulent mixing of spray droplets in crossflow

Centrifugal spray injected at various angles in gas crossflow has been studied experimentally using PIV visualization system and image-processing techniques. Experiments were carried out inside a rectangular duct (95 mm × 95 mm in cross-section) at ambient temperature and pressure, with different gas Reynolds numbers (vary from 12,900 to 45,000) and three injection angles (60°, 90° and 120°). The spray angle of the centrifugal nozzle is 80°, with D₃₂ of 80 μm. The instantaneous images of droplets distribution and the values of the line-averaged D₃₂ at different positions on the cross-sections along the flow field for each condition were obtained, and their flow field configurations were achieved. Quantitative assessments of mixing degree between two phases for different injection angles were determined using a spatial unmixedness parameter. It is found that the addition of droplets into the gas crossflow enhanced the turbulence intensity of the gas crossflow and caused different-scale vortices. The flow field structure, to a great extent, is dependent on the injection angle. The entrainment and centrifugal force of large vortex lead to uneven droplet distribution and moreover influence the mixing of droplets and gas crossflow. A better mixing result can be obtained with the injection angle of nozzles of 60°.     

Experiments and analysis on self-motion behaviors of liquid droplets on gradient surfaces

A surface with surface energy gradient was fabricated by using chemical vapor deposition technology with dodecyltrichlorosilane (C₁₂H₂₅Cl₃Si), and its property was characterized by sessile drop method and Atomic Force Microscope scanning. Visualization experiments were carried out to investigate the motion behaviors of water and ethylene glycol droplets on horizontal and inclined gradient surfaces. And system free energy transition was analyzed to understand the mechanics of the droplet self-motion. The results show that the height and density of the silane molecules groups determined surface energy distribution on the surface. The liquid droplets were self-propelled to move horizontally or uphill from hydrophobic zone to hydrophilic zone on horizontal and inclined gradient surface. The motion process of the droplet experienced an accelerating stage and a creeping decelerating stage; the velocity and the displacement as well as the creeping frequency were proportional to the droplet size. The velocity of 2 ml water droplet reached 42 mm/s on the horizontal surface and 18 mm/s on the inclined surface, while that for ethylene glycol droplet reached 7 mm/s on the horizontal surface. The droplet motion was resulted from the energy transition among interfacial energy, kinetic energy, gravitational potential energy, and viscous dissipation energy. The interfacial energy released from deformation of the droplet is the main source for the motion.     

Atomization of liquids by disintegrating thin liquid films using gas jets

Liquid atomization is useful in many applications, such as engineering, science, pharmaceutics, medicine, forensics and others. In the present research, an innovative methodology and a new device for atomization of liquids into mists of micron and submicron droplets have been developed. The new liquid-atomization method exploits the physical phenomenon of fragmentation of thin liquid films into fine micron and submicron droplets by gas jets. For several tested prototypes, the direct observations using a high-speed visualization technique have demonstrated that bubbles were generated within a liquid and their shells have been subsequently destroyed by applying a mechanical impulse (pressure of a compressed air) once the bubbles came over the liquid surface. The main characteristics of the generated tap water mists have been experimentally measured by means of the laser diffraction technique under various conditions for each prototype. One of the prototype devices allowed obtaining mists containing 90–99% of droplets smaller than 1 µm, with the minimum arithmetic and Sauter mean droplet diameters of 1.48 µm and 2.66 µm, and the 2.64 ml/min of droplet flow rate for 3.5 bar manometer pressure of atomizing air. The gas to liquid mass ratios (GLR) in the new device are depending on the atomizing tube length and the number of perforated orifices in the tube: more the tube length, hence more the number of perforated orifices, and therefore more liquid droplets will form for the same gas flow rate. The measured GLR values related to 1 m length of the utilized atomizing tube were in the range of 0.65–1.06, and for the specifically utilized atomizing tube of 72 mm length were among 9.07–14.67. The results of this study demonstrate that the developed method of generation of very fine droplet mists has many advantages over the existing techniques and can be perspective for many practical applications.     

The atomization of water–oil emulsions

The paper presents the results of experimental studies on atomization of the emulsions flowing through twin-fluid atomizers obtained by the use of the digital microphotography method. The main elements of the test installation were: nozzle, reservoir, pump and measurement units of liquid flow. The photographs were taken by a digital camera with automatic flash at exposure time of 1/8000 s and subsequently analyzed using Image Pro-Plus. The oils used were mineral oils 20–90, 20–70, 20–50 and 20–30. The studies were performed at flow rates of liquid phase changed from 0.0014 to 0.011 (dm³/s) and gas phase changed from 0.28 to 1.4 (dm³/s), respectively. The analysis of photos shows that the droplets being formed during the liquid atomization have very different sizes. The smallest droplets have diameters of the order of 10 μm. The experimental results showed that the changes in physical properties of a liquid phase lead to the significant changes in the spray characteristics. The analysis of the photos of water and emulsions atomization process showed that the droplet sizes are dependent on gas and liquid flow rates, construction of nozzle and properties of liquid. The differences between characteristics of atomization for water and emulsions have been observed. Analysis of photos on forming the droplets in air–water and air-emulsions systems showed that droplets are bigger in air-emulsion system (at the same value of gas to liquid mass ratio). The values of Sauter mean diameter (SMD) increased with increase of volume fraction of oil in emulsion. The droplet size increased with emulsion viscosity.     

Droplet size and velocity characteristics of water-air impinging jet atomizer

A water-air impinging jets atomizer is investigated in this study, which consists of flow visualization using high speed photography and mean droplet size and velocity distribution measurements of the spray using Phase Doppler Anemometry (PDA). Topological structures and break up details of the generated spray in the far and near fields are presented with and without air jet and for an impinging angle of 90°. Spray angle increases with the water jet velocity, air flow rate and impinging angle. PDA results indicate that droplet size is smallest in the spray center, with minimum value of Sauter mean diameter (SMD) of 50 µm at the air flow rate of Q_m = 13.50 g/min. SMD of droplets increases towards the spray outer region gradually to about 120 µm. The mean droplet velocity component W along the air-jet axis is highest in the spray center and decreases gradually with increasing distance from the spray center. SMD normalized by the air nozzle diameter is found firstly to decrease with gas-to-liquid mass ratio (GLR) and air-to-liquid momentum ratio (ALMR) and then remain almost constant. Its increasing with aerodynamic Weber number indicates an exponential variation. The study sheds light on the performance of water-air impinging jets atomizers providing useful information for future CFD simulation works.     

Flow pattern change in horizontal rectangular laterally ribbed ducts through alteration of the ribs thickness and pitch

Experiments were conducted on two-phase flow in laterally ribbed rectangular ducts. Air–water adiabatic flow at atmospheric pressure and room temperature was driven through a 3.6 m long rectangular ribbed test section with cross-section of 100 × 50 mm. To investigate the effect of rib thickness and pitch on flow pattern diagrams and transition boundaries, nine various rib arrangements were implemented with thicknesses of 2, 4 and 8 mm and pitches of 50, 60, and 80 mm. Unlike non-ribbed rectangular duct, lateral rib arrangement did not allow any stratified flow to occur. However wavy, plug and slug flows were parallel in both flow conditions, rib existence caused explicitly coarser pattern shapes. Increasing the rib thickness, while keeping the pitch constant, results in different flow patterns to occur as well as dramatic changes in boundaries positions and shapes. On the other hand, as pitch shifts up at a constant rib thickness, one can notice the duplication of almost identical flow patterns and their boundaries however, boundary values undergo tangible changes. Consistent attention was paid to conditions under which wavy pattern zone extends while intermittent flow zones were avoided. Studies concerned ribbed duct are of major applicable value to designing and enhancing heat transfer systems.     

Atomization of glycerin with a twin-fluid swirl nozzle

Atomization of liquids with high viscosity is always a challenge, especially when small diameter droplets and high liquid flow rates are simultaneously required. In the present research, the performance of a Venturi–vortex twin-fluid swirl nozzle is examined, attending to its capabilities to generate droplets with diameters below 20 µm when atomizing pure glycerin at room temperature. In this nozzle, air is injected tangentially in a central convergent section, and discharges suctioning the liquid fed to a coaxial chamber, here using a gear pump. The resulting spray is visualized and analyzed. Droplet size distributions are measured with a laser diffractometer. As expected, droplet diameter increases with liquid flow rate, and quickly diminishes when air flow rate is increased. Sauter mean diameters (SMD) below 15 µm can be obtained even when atomizing pure glycerin. However, these values are obtained for relatively low glycerin flow rates (∼5 l/h), and with rather wide distributions. For 10 l/h and an air-to-liquid mass flow rate ratio (ALR) of 13.7 more than 26% of the glycerin volume is atomized in droplets smaller than 20 µm. Liquid ligaments are observed near the nozzle exit, but they tend to break up while moving downstream.     

Experimental study on local characteristics of oil–water dispersed flow in a vertical pipe

The local flow characteristics of oil–water dispersed flow in a vertical upward pipe were studied experimentally. The inner diameter and length of the test section are 40 mm and 3800 mm, respectively. A double-sensor conductivity probe was used to measure the local interfacial parameters, including interfacial area concentration, oil phase fraction, interfacial velocity, and oil drops Sauter mean diameter. The water flow rates varied from 0.12 m/s to 0.89 m/s, while the oil flow rates ranged from 0.024 m/s to 0.198 m/s. Typical radial profiles of interfacial area concentration, oil phase fraction, interfacial velocity, and oil drops Sauter mean diameter are presented. An interesting phenomenon is that the local and cross-section-averaged interfacial area concentrations display concave change with water flow rate under constant oil flow rate. The physical mechanism of such a variation is discussed in details.     

Coalescence of sessile droplets of varying viscosities for line printing

Coalescence of sessile droplets is studied experimentally with water–glycerin mixtures of different viscosities. Effects of viscosity on the dimensionless spreading length (Ψ) and the center-to-center distance (L) are investigated for two droplets; the first droplet (D_s) is stationary on a substrate and the second droplet (D₀) landing at a center-to-center distance L from the first droplet. For a low viscosity fluid, Ψ is maximum when L approaches zero (or λ → 1, where λ = 1 − L/D_s), which represents a head-on collision. For a high viscosity fluid, Ψ is minimum when λ → 0.6. The effect of λ on line printing for various viscosities is also examined by printing multiple droplets. We found that the larger the viscosity, the less the breakup between droplets; viscosities smaller than 60 wt% glycerin yielded line breakup. The overlap ratio of λ > 0.3 produced not a line, but a bigger droplet or puddle because of coalescence. Data obtained in this work can provide insights for the fabrication of conductive microtracks or microinterconnects in printed-electronics applications where a line breakup between droplets would lead to an electrical circuit short.     

Experimental investigation of a developing two-phase bubbly flow in horizontal pipe

Experimental results for various water and air superficial velocities in developing adiabatic horizontal two-phase pipe flow are presented. Flow pattern maps derived from videos exhibit a new boundary line in intermittent regime. This transition from water dominant to water–gas coordinated regimes corresponds to a new transition criterion C_T = 2, derived from a generalized representation with the dimensionless coordinates of Taitel and Dukler.Velocity, turbulent kinetic energy and dissipation rate, void fraction and bubble size radial profiles measured at 40 pipe diameters for J_L = 4.42 m/s by hot film velocimetry and optical probes confirm this transition: the gas influence is not continuous but strongly increases beyond J_G = 0.06 m/s. The maximum dissipation rate, derived from spectra, is increased in two-phase flow by a factor 5 with respect to the single phase case.The axial evolution of the bubble intercept length histograms also reveal the flow organization in horizontal layers, driven by buoyancy effects. Bubble coalescence is attested by a maximum bubble intercept evolving from 2.5 to 4.5 mm along the pipe. Turbulence generated by the bubbles is also manifest by the 4-fold increase of the maximum turbulent dissipation rate along the pipe.     

Oil emulsion separation with fluidic oscillator generated microbubbles

Surfactants stabilise oil droplets in water, forming a dispersed oil–water emulsion. Treatment of oily effluents is a serious challenge owing to the high stability and colloidal nature of the oil droplets. In many applications, microbubbles are employed for separation purposes due to their buoyancy and increased surface area to volume ratio. This property has been exploited in the water treatment industry for separation in a process known as dissolved air flotation (DAF). Though practically efficient, the process is energy intensive operating at >5 bars and consequently consuming ∼90% of the total energy required in water purification plants. In this study microbubbles were produced by fluidic oscillation via a no-moving part diverter valve to cut down the energy consumption considerably. Microbubbles are applied for the separation of emulsified oil in a process known as microflotation. The mean bubble size generated by fluidic oscillation from the 50 μm pore diffuser was ∼100 μm, otherwise coarse bubbles were produced under steady flow. The effect of surfactant concentration on oil droplet size was investigated. It was found that oil droplet size varied inversely proportional to surfactant concentration. In addition, it was found that the oil removal efficiency also depends on the surfactant concentration. The maximum oil removal efficiency by Microflotation was found to be 91% under lowest surfactant concentration tested (0.3 wt%) whilst at highest surfactant concentration used (10 wt%); lowest recovery efficiency (19.4%) was recorded.     

A laser extinction based sensor for simultaneous droplet size and vapor measurement

Multiphase flows involving liquid droplets in association with gas flow occur in many industrial and scientific applications. Recent work has demonstrated the feasibility of using optical techniques based on laser extinction to simultaneously measure vapor concentration and temperature and droplet size and loading. This work introduces the theoretical background for the optimal design of such laser extinction techniques, termed WMLE (wavelength-multiplexed laser extinction). This paper focuses on the development of WMLE and presents a systematic methodology to guide the selection of suitable wavelengths and optimize the performance of WMLE for specific applications. WMLE utilizing wavelengths from 0.5 to 10 μm is illustrated for droplet size and vapor concentration measurements in an example of water spray, and is found to enable unique and sensitive Sauter mean diameter measurement in the range of ～1–15 μm along with accurate vapor detection. A vapor detection strategy based on differential absorption is developed to extend accurate measurement to a significantly wider range of droplet loading and vapor concentration as compared to strategies based on direct fixed-wavelength absorption. Expected performance of the sensor is modeled for an evaporating spray. This work is expected to lay the groundwork for implementing optical sensors based on WMLE in a variety of research and industrial applications involving multi-phase flows.     

Experimental investigation of turbulence modulation in particle-laden coaxial jets by Phase Doppler Anemometry

The effect of solid particles on the flow characteristics of axisymmetric turbulent coaxial jets for two flow conditions was studied. Simultaneous measurements of size and velocity distributions of continuous and dispersed phases in a two-phase flow are presented using a Phase Doppler Anemometry (PDA) technique. Spherical glass particles with a particle diameter range from 102 to 212 μm were used in this two-phase flow, the experimental results indicate a significant influence of the solid particles and the Re on the flow characteristics. The data show that the gas phase has lower mean velocity in the near-injector region and a higher mean velocity at the developed region. Near the injector at low Reynolds number (Re = 2839) the presence of the particles dampens the gas-phase turbulence, while at higher Reynolds number (Re = 11 893) the gas-phase turbulence and the velocity fluctuation of particle-laden jets are increased. The particle velocity at higher Reynolds number (Re = 11 893) and is lower at lower Reynolds number (Re = 2839). The slip velocity between particles and gas phase existed over the flow domain was examined. More importantly, the present experiment results suggest that, consideration of the gas characteristic length scales is insufficient to predict gas-phase turbulence modulation in gas-particle flows.     

Numerical and experimental study of an axially induced swirling pipe flow

In-line flow segregators based on axial induction of swirling flow have important applications in chemical, process and petroleum production industries. In the later, the segregation of gas bubbles and/or water droplets dispersed into viscous oil by swirling pipe flow may be beneficial by either providing a pre-separation mechanism (bubble and/or drop coalescer) or, in the case of water-in-oil dispersions, by causing a water-lubricated flow pattern to establish in the pipe (friction reduction). Works addressing these applications are rare in the literature. In this paper, the features and capabilities of swirling pipe flow axially induced by a vane-type swirl generator were investigated both numerically and experimentally. The numerical analysis has been carried out using a commercial CFD package for axial Reynolds numbers less than 2000. Pressure drop, tangential and axial velocity components as well as swirl intensity along a 5 cm i.d. size and 3 m long pipe were computed. Single phase flow experiments have been performed using a water–glycerin solution of 54 mPa s viscosity and 1210 kg/m³ density as working fluid. The numerical predictions of the pressure drop were compared with the experimental data and agreement could be observed within the range of experimental conditions. The experiments confirmed that swirl flow leads to much higher friction factors compared with theoretical values for non-swirl (i.e. purely axial) flow. Furthermore, the addition of a conical trailing edge reduces vortex breakdown. Visualization of the two-phase swirling flow pattern was achieved by adding different amounts of air to the water–glycerin solution upstream the swirl generator.     

Void fraction and pressure waves in a transient horizontal slug flow

The void fraction and the pressure waves in an air–water mixture flowing in the slug regime are experimentally investigated in a horizontal line. The test section is made of a transparent Plexiglas pipe with 26 mm ID and 26.24 m long, operating at ambient temperature and pressure. The flow induced transients are made by quickly changing the air or the water inlet velocity. The test grid has four operational points. This choice allows one to create expansion and compression waves due to the changes to the gas or to the liquid. Each experimental run is repeated 100 times to extract an ensemble average capable of filtering out the intrinsic flow intermittence and disclosing the void fraction and pressure waves’ features. The slug flow properties such as the bubble nose translational velocity, the lengths of liquid film underneath the bubble and the liquid slug are also measured. The objective of the work is two-fold: access the main characteristics of the void fraction and pressure waves and disclose the mechanics of the transient slug flow as described through the changes of the slug flow properties.     

Study of material agglomeration during nozzle injection of multiviscosity liquid into a fluidized bed reactor by the electric conductance method

Fluidized bed agglomeration is an important and challenging problem for thermal cracking in fluid cokers. A low coker temperature can be problematic because the bitumen is injected into the fluidized bed with a different viscosity, resulting in formation of agglomerates of varying sizes, which slows the cracking reactions. In the present study, the bed material agglomeration process during nozzle injection of multiviscosity liquid was investigated in a fluidized bed operated at different mass ratios of the atomization gas to the liquid jets (GLR = 1%–3.5%) and gas velocities (3.9U_mf and 5.9U_mf) based on a conductance method using a water–sand system to simulate the hot bitumen–coke system at room temperature. During the tests of liquid-jet dispersion throughout the bed, different agglomeration stages are observed at both gas velocities. The critical amount of tert-butanol in the liquid jets that could lead to severe agglomeration of the bed materials (poor fluidization) at GLR = 1% is about 10 wt% at the low fluidizing gas velocity (3.9U_mf) and 18 wt% at the high gas velocity (5.9U_mf). This study provides a new approach for on-line monitoring of bed agglomeration during liquid injection to guarantee perfect contact between the atomized liquid and the bed particles.     

Two-phase flow behavior inside a header connected to multiple parallel channels

The main objective of this work is to examine the flow distribution of two-phase mixture to parallel channels and to investigate the flow behavior at header-channel junctions simulating the corresponding parts of compact heat exchangers. The cross-section of the header and the channels were fixed to 14 mm × 14 mm and 12 mm × 1.6 mm, respectively. The mass flux and the mass quality ranges were 70–165 kg/m² s and 0.3–0.7, respectively. Air and water were used as the test fluids. The flow distribution at the fore part of the header (region A) is affected only by the upstream flow configuration and the rate of liquid flow separation decreased a flowing downwards. On the other hand, in the rear part, the downstream effect predominates over the upstream effect due to strong flow recirculation near the end plate. In this part, the liquid separation increased (region B) and then decreased (region C) as the mixture proceeds downwards. The validity of the existing models for branching flows at parallel T-junction was tested, and turned out to be appropriate for region A. However, the models were not applicable to the rear part due to a strong flow recirculation. Moreover, the effect of the membranes in channels was investigated, but that was minor.