The effect of post-annealing on surface acoustic wave devices based on ZnO thin films prepared by magnetron sputtering

Zinc oxide (ZnO) thin films were deposited on unheated silicon substrates via radio frequency (RF) magnetron sputtering, and the post-deposition annealing of the ZnO thin films was performed at 400 °C, 600 °C, 800 °C, and 1000 °C. The characteristics of the thin films were investigated by X-ray diffractometry (XRD), scanning electron microscopy (SEM), and atomic force microscopy (AFM). The films were then used to fabricate surface acoustic wave (SAW) resonators. The effects of post-annealing on the SAW devices are discussed in this work. Resulting in the 600 °C is determined as optimal annealing temperature for SAW devices. At 400 °C, the microvoids exit between the grains yield large root mean square (RMS) surface roughness and higher insertion losses in SAW devices. The highest RMS surface roughness, crack and residual stress cause a reduction of surface velocity (about 40 m/s) and increase dramatically insertion loss at 1000 °C. The SAW devices response becomes very weak at this temperature, the electromechanical coupling coefficient (k²) of ZnO film decrease from 3.8% at 600 °C to 1.49% at 1000 °C.     

Potential of a piezoelectric energy harvester from sea waves

A sea wave energy harvester from the longitudinal wave motion of water particles is developed. The harvester consisting of a cantilever substrate attached by piezoelectric patches and a proof mass is used to collect electrical energy owing to the electromechanical coupling effect of the piezoelectric patches from the longitudinal wave motion. To describe the energy harvesting process, a mathematical model is developed to calculate the output charge and voltage from the piezoelectric patches according to the Airy linear wave theory and classical elastic beam model. Results show that the mean value of the generated power increases with the increase in the ratio of the width to the thickness of the cantilever, the wave height, the sea depth (which equals to the cantilever height in this study), the ratio of the proof mass to the cantilever mass, and the ratio of the sea depth to the wave length. A value of the power up to 55 W can be realized for a practical sea wave with the values of the sea depth, wave height and wave length to be 3 m, 2 m, and 15 m, respectively. The collected power harvesting with respect to different categories of the sea waves are provided. Our simulations also show the generated electric power can be further increased by an increase in dimensions of the harvester considering the scale effect. This research develops a new technique for energy harvesting from sea waves by piezoelectric energy harvesters.     

Myocardial effects of local shock wave therapy in a Langendorff model

Objective

Applying shock waves to the heart has been reported to stimulate the heart and alter cardiac function. We hypothesized that shock waves could be used to diagnose regional viability.

Method

We used a Langendorff model to investigate the acute effects of shock waves at different energy levels and times related to systole, cycle duration and myocardial function.

Results

We found only a small time window to use shock waves. Myocardial fibrillation or extrasystolic beats will occur if the shock wave is placed more than 15 ms before or 30 ms after the onset of systole. Increased contractility and augmented relaxation were observed after the second beat, and these effects decreased after prolonging the shock wave delay from 15 ms before to 30 ms after the onset of systole. An energy dependency could be found only after short delays (−15 ms). The involved processes might include post-extrasystolic potentiation and simultaneous pacing.

Conclusion

In summary, we found that low-energy shock waves can be a useful tool to stimulate the myocardium at a distance and influence function.     

A multi-channel full-duplex 60-GHz-band radio-over-fiber system

We propose and simulate a novel full-duplex radio-over-fiber system using a single light source at central station (CS). The scheme is employed to generate 60-GHz optical millimeter wave at CS for down-link transmission while the same optical carrier is reused at base station for up-link connection. There is no additional laser source for the upstream data generation in the base station. The bidirectional full-duplex 2.5 Gb/s data are successfully transmitted over 40 km standard single-mode fiber (SMF). The power penalty for the down-link data after transmission over 40 km SMF is less than 0.6 dB, while for the up-link data, the power penalty after transmission over 40 km SMF is neglected. This system shows good performance over long-distance delivery and has important applicable value in high radio frequency (RF) sector and multi-channel full-duplex system.     

Design and analysis of a metallic waveguide with a DAST cap for continuously phase-matched terahertz difference frequency generation

We present a novel source for continuous terahertz (THz) wave generation using an organic ionic salt, 4-dimethylamino-N-methyl-4-stilbazolium-tosylate (DAST). THz waves are generated based on difference frequency generation (DFG) in the device. Phase matching condition and THz generation between 1.3 THz and 2.7 THz, for optical pump around 1.6 μm, are investigated. Our calculations predict that the device produces a relatively high THz output power of 11.07 μW from a 4 cm long waveguide at 2 THz.     

Wave front reversal of surface magnetostatic waves

The wave front reversal (WFR) of non-reciprocal waves has been investigated. The experiment was performed using surface magnetostatic waves (SMSW) excited by a pulsed microwave signal of the carrier frequency ∼4.7 GHz in an epitaxial yttrium–iron garnet (YIG) film. The WFR was realized by pulsed parametric pumping of a double frequency. It was shown that WFR with high efficiency can be achieved for SMSW having relatively small wavenumbers k∼10² rad/cm.     

Axisymmetric fluid-dominated wave in fluid-filled plastic pipes: Loading effects of surrounding elastic medium

Axisymmetric (n = 0) waves that propagate at low frequencies are of practical interest in the application of acoustic techniques for the detection of leaks in fluid-filled pipelines. A general expression for the fluid-dominated (s = 1) wavenumber is presented in a thin-walled fluid-filled pipe surrounded by an elastic medium. In this paper the analysis is extended to investigate the loading effects of surrounding medium on the low-frequency propagation characteristics of the s = 1 wave. The analytical model is subsequently applied to MDPE water pipes surrounding by three media, namely an air, water and soil. It is used to demonstrate explicitly the loading effects of surrounding medium, acting as a combination of mass, stiffness and radiation damping on the s = 1 wavenumber. Good agreement is achieved between the measurements and predictions. The theory with experimental validations provides the basis for improving acoustic leak detection methods in fluid-filled pipe systems.     

Noncascading THz-wave parametric oscillator synchronously pumped by mode-locked picosecond Ti:sapphire laser in doubly-resonant external cavity

A noncascading terahertz (THz) wave parametric oscillator synchronously pumped by a mode-locked picosecond Ti:sapphire laser whose average power was less than 1 W was demonstrated with a noncollinear phase-matching MgO:LiNbO₃ crystal in an external enhancement cavity doubly resonant for both pump (780 nm) and signal (781-784 nm) waves. In the external cavity, in which the pump wave enhanced so as to reduce the pumping threshold of parametric processes, the signal wave could also resonate and thus be enhanced simultaneously, resulting in a THz wave output at approximately 0.9 THz as the idler wave. The novel dual enhancement of pump and signal waves reduced the threshold pumping intensity to approximately 50 MW/cm², which was much lower than that of a conventional externally pumped THz wave parametric oscillator with a crystal.     

Electronic and optical properties of high pressure stable phases of ZnS: Comparison of FPLAPW and PW-PP results

A theoretical study of the structural phase transformation of ZnS under high pressure has been performed using first principle plane wave pseudopotential (PW-PP) and full potential linear augmented plane wave method (FPLAPW) calculation in which Zn-3d states are treated as valence states. In both methods, we have used a generalized gradiant approximation for the study of phase transformation and structural parameters. The calculated difference in lattice constants (Δα₀) by PW-PP and FPLAPW methods for zinc-blende, cinnabar and rocksalt structures is equal to 0.003, 0.01 and 0.001 Å respectively. There is a very good agreement between the results of PW-PP and FPLAPW calculations that shows soundness of our choice of pseudopotential. The calculated transition pressure for zinc-blende → rocksalt is in agreement with available measured data. We present calculations of the optical properties for three phases of ZnS. The band gap of different phases of ZnS decreases in order of zinc-blende → cinnabar → rocksalt mainly due to red shift of Zn-s states in the lowest conduction band. Besides, the optical band gap decreases from 2.84 eV (direct) to 0.188 eV (indirect). The shift of calculated complex dielectric function ε₂(ω) for zinc-blende → cinnabar → rocksalt is also discussed in details of optical transition that occurred in different phases.     

Multipole surface plasmon resonance of an aluminium surface

The surface photoelectric effect and the surface plasmon resonances appear when a p/transverse magnetic polarized laser hits a gas-solid interface. We model this effect in the long wave length (LWL) domain (λ_vac > 10 nm, ?ω < 124 eV) by combining the Ampère-Maxwell equation, written in classical approximation, with the material equation for the susceptibility. The resulting model, called the vector potential from the electron density (VPED), calculates the susceptibility as a product of the bulk susceptibility and the electron density of the actual system. The bulk susceptibility is a sum of the bound electron scalar susceptibility taken from the experiment and of the conduction electron non-local isotropic susceptibility tensor in a jellium metal (Lindhard, 1954 [1]). The electron density is the square of the wave function solution of the Schrödinger equation. The analysis of observables, the reflectance R and the photoelectron yield Y as well as the induced charge density permits to identify and characterize the multipole surface plasmon resonance of Al(111) appearing at ω_m ∼ 0.8ω_p or 11-12 eV.     

Realization of p-ZnO thin films by GaP codoping

An attempt has been made to realize p-ZnO by directly doping (codoping) GaP into ZnO thin films. GaP codoped ZnO thin films of different concentrations (1, 2 and 4 mol%) have been grown by RF magnetron sputtering. The grown films on sapphire substrate have been characterized by X-ray diffraction (XRD), Hall measurement, Photoluminescence (PL) and Energy dispersive spectroscopy (EDS) to validate the p-type conduction. XRD result shows that all the films have been preferentially oriented along (0 0 2) orientation. The decrease of full-width at half maximum (FWHM) with increase in GaP doping depicts the decrease in native donor defects. Hall measurement shows that among the three films, 2 and 4 mol% GaP doped ZnO shows p-conductivity due to the sufficient amount of phosphorous incorporation. It has been found that low resistivity (2.17 Ωcm) and high hole concentration (1.8×10¹⁸ cm⁻³) for 2% GaP codoped ZnO films due to best codoping. The red shift in near-band-edge (NBE) emission and donar-acceptor-pair (DAP) and neutral acceptor bound recombination (A°X) observed by room temperature and low temperature (10 K) PL, respectively, well acknowledged the formation of p-ZnO. The incorporated phosphorous in the film has been also confirmed by EDS analysis.     

Parametric harmonic-to-fundamental ratio contrast echocardiography: a novel approach to identification and accurate measurement of left ventricular area under variable levels of ultrasound signal attenuation

Objectives

We introduced a harmonic-to-fundamental ratio (HFR) of the radiofrequency (RF) signals that reduces confounding effects of attenuation. We studied whether HFR analysis of RF signals received from contrast microbubbles allows accurate measurement of the left ventricular (LV) cavity area under varying levels of attenuation.

Background

Attenuation is a fundamental problem in ultrasound imaging and limits the use of clinical echocardiography.

Methods

RF data from short axis systolic and diastolic scans were obtained from 14 open-chest dogs following left-atrial bolus of Optison. Attenuation was induced by interposed silicone pads calibrated to induce 7 dB or 14 dB reductions of the backscattered RF signal. RF images were reconstructed from the RF signals, HFR values calculated for each image pixel for 0 dB, 7 dB and 14 dB attenuation conditions, and LV area obtained by summation of “LV cavity pixels”. A reference LV cavity area was obtained from endocardial border tracings in enhanced scans by experts.

Results

Correlation of the HFR-defined and reference areas at systole was R = 0.95, R = 0.94, and R = 0.91 for 0 dB, 7 dB and 14 dB levels of attenuation, respectively, and at diastole was R = 0.95 for 0 dB, 7 dB and 14 dB levels of attenuation. The mean difference from both systolic and diastolic values was <1.45 cm² (i.e. negligible) in all attenuation settings.

Conclusion

Our novel HFR method supports precise measurement of the LV cavity area in contrast images with simulated high attenuation of ultrasound signals.     

Diagnostic value of elastosonography for thyroid microcarcinoma

Objective

To assess the diagnostic value of elastosonography for thyroid microcarcinoma (TMC), particularly with regard to elasticity score (ES) and strain ratio (SR).

Methods

Conventional ultrasound and elastosonography were performed for 487 thyroid micronodules before surgery. We set the histology as the reference standard. The ES and SR values, as well as their diagnostic threshold and efficiency, were compared and analyzed by the receiver-operating characteristic (ROC) curve. Additional comparisons between TMC patients with and without extracapsular extension were also performed.

Results

Statistically significant differences (P < 0.05) in both ES and SR values were detected among the TMC and benign groups. The area under the ROC curve of SR was significantly greater than that of ES (0.956 and 0.844, respectively; P < 0.05). Using ES ? 3 and SR ? 3.65 as diagnostic threshold values, the diagnostic sensitivity, specificity, and accuracy of ES for differentiating benign and malignant nodules were 79.9%, 72.3%, and 80.5%, respectively, whereas those of SR were 86.6%, 85.3%, and 89.4%, respectively. The maximum diameter, microcalcification status, aspect ratio, bilateral cervical lymph node metastasis, and SR values of nodules with extracapsular extension (A1 subgroup) were greater than those of nodules without extracapsular extension (A2 subgroup).

Conclusions

Elasticity imaging technology not only can help differentiate between benign and malignant thyroid micronodules but also allow SR values to provide accurate and objective information on tissue hardness and to predict TMC extracapsular extension or even bilateral cervical lymph node metastasis.     

Stimulated Raman scattering of sub-millimeter waves in bismuth

A high-power sub-millimeter wave propagating through bismuth, a semimetal with non-spherical energy surfaces, parametrically excites a space-charge mode and a back-scattered electromagnetic wave. The free carrier density perturbation associated with the space-charge wave couples with the oscillatory velocity due to the pump to derive the scattered wave. The scattered and pump waves exert a pondermotive force on electrons and holes, driving the space-charge wave. The collisional damping of the decay waves determines the threshold for the parametric instability. The threshold intensity for 20 μm wavelength pump turns out to be ∼2×10¹² W/cm². Above the threshold, the growth rate scales increase with ω_o, attain a maximum around ω_o=6.5ω_p, and, after this, falls off.     

Effect of wood properties on within-tree variation in ultrasonic wave velocity in softwood

The radial variations in the velocity of longitudinal waves propagating through Japanese cedar and Japanese cypress were experimentally investigated. In addition, the tracheid length (TL), microfibril angle (MFA), air-dried density (AD), and moisture content (MC) were measured in order to determine the effect of wood properties on velocity variations within the wood trunk. For both species, the longitudinal wave velocities measured in the longitudinal direction (V_L) exhibited minimum values near the pith. For Japanese cedar, V_L increased from 3600 m/s toward the bark and soon attained a constant value (=4500 m/s). On the other hand, for Japanese cypress, V_L kept increasing from 4000 m/s near the pith to 4800 m/s at the bark. These radial variations in V_L coincided with those in the tracheid length. V_L exhibited strong correlations with TL and MFA with a significant level of (p < 0.01). These findings suggest that the TL and MFA greatly affect the radial variation in the ultrasonic wave velocity in softwood.     

Transmission analysis of ultrasonic Lamb mode conversion in a plate with partial-thickness notch

Mode conversions of Lamb waves can occur upon encountering damage or defect such as a notch, leading to newly-converted modes apart from wave reflection and transmission. In this paper, the transmission of the fundamental Lamb modes symmetrical S0 and anti-symmetrical A0 with anti-symmetrical notches were investigated in steel plates within the relatively short propagation distance. The group velocity and modal energy of the converted modes were analyzed using simulations and experiments. Two-dimensional finite difference time domain (2D-FDTD) method was employed to calculate the scattering field and extract numerical trends for simulation study and experimental confirmation. Both simulations and experiments revealed that the apparent group velocities of the converted modes in the transmitted signals subject to the notch positions. To describe the mode conversion degree and evaluate the notch severity, wave packets of the originally-transmitted modes and newly-converted modes were separated and corresponding mode energy percentages were analyzed at different notch severities. Frequency-sweeping measurements illustrated that the modal energy percentages varied monotonically over the notch-depth increase with a statistically consistency (R = 1.00, P < 0.0004).     

Comparison of mechanisms and effects of Nd:YAG and CO2 laser cleaning of titanium alloys

The paper compares laser cleaning trials performed using a Q-switched Nd:YAG laser, λ = 1.064 μm and a continuous wave (CW) CO₂ laser, λ = 10.6 μm, applied to aerospace-grade, contaminated titanium alloys. The mechanisms for cleaning using each laser system are modelled to determine the mode and extent of contaminant removal. The model results are then compared with the surface chemistry and micro-structural results from the cleaning trials performed. The results show the dominant cleaning process for Nd:YAG cleaning to be by evaporation of the contaminant via conduction through surface heating, while for CO₂ laser cleaning the small fraction of the beam coupling directly with the contaminant is sufficient for direct heating and selective evaporation. The results for experimental cleaning, electron beam (EB) welding and diffusion bonding align well with the model, particularly when secondary reactions are taken into account.     

Giant optical activity and circular dichroism in the terahertz region based on bi-layer Y-shaped chiral metamaterial

We present a bi-layer Y-shaped chiral metamaterial (CMM) that can realize a giant optical activity and circular dichroism (CD) effect to the incident linear polarization wave in the terahertz (THz) region. Numerical simulation results exhibit that the pronounced CD effect with a great difference between the transmission coefficients for the circularly polarized waves can be obtained at 5.06 THz, meanwhile the 90°-polarization rotation can be observed at 5.2 THz when a y-polarized wave is incident to this CMM propagating along the −z-axis. The mechanism of the optical activity and giant CD effect is illustrated by simulated surface current distributions. Further, the influences of the structural parameters of the proposed CMM to the optical activity and CD effect have been investigated numerically.     

FEM simulation of Rayleigh waves for CMOS compatible SAW devices based on AlN/SiO2/Si(1 0 0)

A simulation study of Rayleigh wave devices based on a stacked AlN/SiO₂/Si(1 0 0) device was carried out. Dispersion curves with respect to acoustic phase velocity, reflectivity and electromechanical coupling efficiency for tungsten W and aluminium Al electrodes and different layer thicknesses were quantified by 2D FEM COMSOL simulations. Simulated acoustic mode shapes are presented. The impact of these parameters on the observed Rayleigh wave modes was discussed. High coupling factors of 2% and high velocities up to 5000 m/s were obtained by optimizing the AlN/SiO₂ thickness ratio.     

Multilayered metal oxide thin film gas sensors obtained by conventional and RF plasma-assisted laser ablation

Multilayered thin films of In₂O₃ and SnO₂ have been deposited by conventional and RF plasma-assisted reactive pulsed laser ablation, with the aim to evaluate their behaviour as toxic gas sensors. The depositions have been carried out by a frequency doubled Nd-YAG laser (λ = 532 nm, τ = 7 ns) on Si(1 0 0) substrates, in O₂ atmosphere. The thin films have been characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and electrical resistance measurements. A comparison of the electrical response of the simple (indium oxide, tin oxide) and multilayered oxides to toxic gas (nitric oxide, NO) has been performed. The influence on the structural and electrical properties of the deposition parameters, such as substrate temperature and RF power is reported.