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JPC – Journal of Planar Chromatography – Modern TLC - A new, simple, accurate, and precise high-performance thin-layer chromatographic (HPTLC) method has been developed for the...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - High-performance thin-layer chromatography (HPTLC) on silica gel 60 F254 TLC plates, with ethyl acetate-methanol-acetone-acetic...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - This paper describes a validated high-performance thin-layer chromatography (HPTLC) method for the simultaneous determination of...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - This study is a first attempt to present a report about a high-performance thin-layer chromatography (HPTLC)—densitometric...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - Simple, accurate, precise, sensitive, and validated high-performance liquid chromatography (HPLC) and thin-layer chromatography...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - A high-performance thin-layer chromatography (HPTLC) method for the quantification of propranolol in human serum is developed and...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - High-performance thin-layer chromatography (HPTLC) has been used for separation and quantitation of components of high explosives...  相似文献   

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Electronic absorption spectra and the chromatographic retention of six alkaloids from the roquefortine group under conditions of thin-layer chromatography and high-performance liquid chromatography were examined. The applicability of these techniques to the identification of diketopiperazine alkaloids in culture liquid extracts was demonstrated using the fungusPenicillium chrysogenumVKM F-1987 as an example.  相似文献   

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薄层色谱法同时测定邻苯二酚、间苯二酚和对苯二酚异构体   总被引:11,自引:0,他引:11  
黄少鹏  徐金瑞  王琼 《分析化学》1999,27(3):331-333
研究了在自制硅胶薄板上邻苯二酚,间苯二酚异构体的薄层色谱特性。展开剂为本:乙醚:冰醋酸=7:2:1(V/V/V),Rf值分别为0.59,0.53,0.48。检测限分别为1.07×10^-4,1.64×10^-4,1.90×10^4mol/L。其他常见酚不干扰测定。可应用于实际样品的测定,回收率为96%-104%。  相似文献   

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Abstract

Ten amines found in marine foods, dimethylamine, trimethylamine, trimethylamine oxide, ammonia, urea, histamine, cadaverine, putrescine, spermine and spermidine were separated by HPLC using an ion-moderated partition column. Optimum resolution and sensitivity were obtained using 0.003N sodium hydroxide as the mobile phase and UV detection at 208 nm.  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - Quantification of carbohydrates and metabolites in fermentation processes can be considered as key factor in determining yield and...  相似文献   

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A rapid and accurate HPLC method has been developed for simultaneous determination of pioglitazone and glimepiride. Chromatographic separation of the two pharmaceuticals was performed on a Cosmosil C18 column (150 mm × 4.6 mm, 5 m) with a 45:35:20 (v/v) mixture of 0.01 m triammonium citrate (pH adjusted to 6.95 with orthophosphoric acid), acetonitrile, and methanol as mobile phase, at a flow rate of 1.0 mL min–1, and detection at 228 nm. Separation was complete in less than 10 min. The method was validated for linearity, accuracy, precision, limit of quantitation, and robustness [1, 2]. Linearity, accuracy, and precision were found to be acceptable over the ranges 2.50–30.00 g mL–1 for pioglitazone and 0.10–10.00 g mL–1 for glimepiride.  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - A simple, sensitive, and precise high-performance thin-layer chromatographic method has been developed for the estimation of...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - A normal-phase TLC method has been established for the estimation of rosuvastatin calcium in its bulk drug and pharmaceutical...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - A sensitive and accurate high-performance thin-layer chromatographic method has been developed, validated, and used for...  相似文献   

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JPC – Journal of Planar Chromatography – Modern TLC - An HPTLC method with densitometric detection at 280 nm has been established for quantification of lamotrigine in human serum....  相似文献   

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《Analytical letters》2012,45(12):2491-2500
ABSTRACT

A method for the simultaneous determination of valsartan and hydrochlorothiazide in tablets is described. The procedure, based on the use of reversed-phase high-performance liquid chromatography, is linear in the concentration range 5.0-10.0 μg ml?1 for valsartan and 0.5-2.0 μg ml?1 for hydrochlorothiazide, is simple and rapid and allows accurate and precise results. The limit of detection was 1.0 μg ml?1 for valsartan and 0.05 μg ml?1 for hydrochlorothiazide.  相似文献   

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