A New Technique for Characterization of Low Impedance Materials at Acoustic Frequencies

Measuring the mechanical properties of low impedance rubbery polymers at acoustic frequencies is a challenging problem due to the small signal amplitudes, relatively high loss, and the long wavelength of stress waves. One such material is solid polyurea (PU), an elastomeric copolymer, which has excellent chemical, thermal, and mechanical properties and is widely used as a coating (e.g. in truck bed lining) or blast protection (advanced helmet designs and concrete structures) material. Moreover, due to its heterogeneous structure, PU has a wide transition of thermo-mechanical behavior from rubber-like to glassy compared to most engineering polymers, which translates to a broader loss spectrum in frequency domain. In this study, we have developed a new test technique by modifying the split Hopkinson pressure bar and using ball impact to measure Young’s storage and loss moduli of polyurea at kHz frequencies. This will therefore fill the frequency gap between the dynamic mechanical analysis (DMA) and ultrasonic (US) wave measurement. The measured Young’s storage and loss moduli from this technique are compared with the master curves of the moduli developed using experimental data of dynamic mechanical analysis and ultrasonic wave measurements. This technique is a direct measurement which provides more reliable data in the kHz frequency range and can be used to evaluate the reliability of other indirect estimations including master curves. The utility of this technique is not limited to polyurea and it can be used to characterize other low impedance materials at kHz frequencies.     

Measurement of instantaneous velocity and surface topography in the wake of a cylinder at low Reynolds number

A technique capable of simultaneous measurement of free-surface topography and velocity vector field data is presented. This technique offers substantial benefits of both reduced complexity and enhanced accuracy over all other techniques known to offer the same measurements. The flow behind a circular cylinder at low Reynolds numbers is measured using this technique. The velocity and vorticity fields as well as Strouhal number closely match the expected results. The free-surface topography, which can be related to the pressure field, exhibits an intimate relationship to the vorticity field.     

Reconstruction of velocity fields from wall pressure measurements in a shock wave/turbulent boundary layer interaction

We present here experimental results in a shock wave/turbulent boundary layer interaction at Mach number of 2.3 impinged by an oblique shock wave, with a deflection angle of 9.5°, as installed in the supersonic wind tunnel of the IUSTI laboratory, France. For such a shock intensity, strong unsteadiness are developing inside the separated zone involving very low frequencies associated with reflected shock motions.The present work consists in simultaneous PIV velocity fields and unsteady wall pressure measurements. The wall pressure and PIV measurements were used to characterize the pressure distribution at the wall in an axial direction, and the flow field associated. These results give access for the first time to the spatial-time correlation between wall pressure and velocity in a shock wave turbulent boundary layer interaction and show the feasibility of such coupling techniques in compressible flows. Linear Stochastic Estimation (LSE) coupled with Proper Orthogonal Decomposition (POD) has been applied to these measurements, and first results are presented here, showing the ability of these techniques to reproduce both the unsteady breathing of the recirculating bubble at low frequency and the Kelvin–Helmholtz instabilities developing at moderate frequency.     

Limitations of temperature measurements with holographic interferometry in the presence of pressure variations

In recent years oscillatory flows have shown to be a promising strategy to enhance heat transfer. However, the mechanisms underlying oscillatory heat transfer enhancement are not yet completely understood. One problem, when investigating heat transfer in oscillatory flows experimentally, is to resolve the temperature distribution as a function of time. This is one reason that most studies reported in the literature so far were restricted to frequencies of a few hertz. As shown in this paper, an appropriate tool to investigate oscillatory heat transfer phenomena at higher frequencies (1000 Hz) is real time holographic interferometry (HI) combined with high-speed cinematography. In the present paper HI was applied to study acoustically driven flow. To apply HI to such a physical situation it was necessary to expand its applicability to cases where changes in the refractive index are caused not only by temperature changes but also by pressure variations. For this purpose a new evaluation formula that accounts for pressure variations was derived. On the example of the acoustic field, we discuss the impact of the pressure variations on temperature measurements. Additionally, an image processing algorithm was developed that allows the measurement of time dependent temperature distributions. The uncertainties of the temperature measurements introduced by the image processing algorithm were found to be in the range of thermocouple measurements.     

Application of fast-responding pressure-sensitive paint to a hemispherical dome in unsteady transonic flow

The current work focuses on the development and application of fast-responding polymer/ceramic pressure-sensitive paint (PSP) as an advanced surface pressure measurement technique for unsteady flow fields in large-scale wind tunnels. To demonstrate the unsteady PSP technique, the unsteady surface pressure distribution over a hemispherical dome placed in the United States Air Force Research Laboratory’s Trisonic Gasdynamics Facility (TGF) was studied by phase-locking to the characteristic frequency in the flow caused by an unsteady separated shear layer shed from the dome. The wind tunnel was operated at stagnation pressures of 23.92 and 71.84 kPa, with the test section flow at Mach 0.6. Under the two operating conditions, the predominant shear layer frequency was measured to be 272 and 400 Hz, respectively. The quasi-periodic shear layer frequency enabled a phase-averaged method to be employed for capturing the unsteady shock motion on the hemisphere. Unsteady pressure data resulting from this technique are shown to correlate well with measurements acquired by conventional measurement techniques. Measurement uncertainty in the phase-averaging technique will be discussed. To address measurement uncertainties from temperature sensitivity and model movement, a new implementation of an AC-coupled data representation is offered.     

An innovative extensional viscometer for low-viscosity and low-elasticity liquids

A spinline-type extensional viscometer is described in which an innovative method of tensile stress measurement is employed. A limited amount of liquid flows through a vertical capillary at a constant flow rate under the influence of a constant pressure head. The drainage time decreases when the liquid stream leaving the capillary is stretched by the application of vacuum. These drainage times are measured in a manner similar to that used for intrinsic viscosity measurements. The measured difference in drainage times, with and without stretching, is trivially related to the extensional stress at the capillary exit, and this provides a very simple method of accurately determining fluid stretching forces having a magnitude as low as 10^-4 N; stresses at other axial locations in the stretched liquid jet are obtained by means of a force balance in the usual manner. The validity of the proposed technique is demonstrated by obtaining the expected results for a Newtonian oil having a shear viscosity of 56.2 mPa-s. Also presented are preliminary data on polyethylene oxide-in-water solutions having an even lower shear viscosity.     

A quartz-crystal-embedded split Hopkinson pressure bar for soft materials

A dynamic experimental technique that is three orders of magnitude as sensitive in stress measurement as a conventional split Hopkinson pressure bar (SHPB) has been developed. Experimental results show that this new method is effective and reliable for determining the dynamic compressive stress-strain responses of materials with low mechanical impedance and low compressive strengths, such as elastomeric materials and foams at high strain rates. The technique is based on a conventional SHPB. Instead of a surface strain gage mounted on the transmission bar, a piezoelectric force transducer was embedded in the middle of the transmission bar of a high-strength aluminum alloy to directly measure the weakly transmitted force profile from a soft specimen. In addition, a pulse-shape technique was used for increasing the rise time of the incident pulse to ensure stress equilibrium and homogeneous deformation in the low-impedance and low-strength specimen.     

Erratum to: Vibration Analysis of Perforated Plates Using Time-Average Digital Speckle Pattern Interferometry

Digital Speckle Interferometry is a non invasive full-field coherent optical technique used in mechanical vibration measurement. In this research, it is used for tuning resonant frequencies of vibrating plates in order to investigate the dynamical behavior of perforated plates. The plate was excited to resonant vibration by a sinusoidal acoustic source. Fringe pattern produced during the time-average recording of the vibrating plate, for several resonant frequencies were registered. Results of plates fixed at one edge having internal holes and attached masses are presented. Experimental natural frequencies and modal shapes are compared to those obtained by an analytical approximate solution based on the Rayleigh–Ritz method with the use of orthogonal polynomials as coordinate function. A high degree of correlation between computational analysis and experimental results was observed, proving the potentiality of the optical technique as experimental validation of the numerical simulations.     

Vibration Analysis of Perforated Plates Using Time-Average Digital Speckle Pattern Interferometry

Digital Speckle Interferometry is a non invasive full-field coherent optical technique used in mechanical vibration measurement. In this research, it is used for tuning resonant frequencies of vibrating plates in order to investigate the dynamical behavior of perforated plates. The plate was excited to resonant vibration by a sinusoidal acoustic source. Fringe pattern produced during the time-average recording of the vibrating plate, for several resonant frequencies were registered. Results of plates fixed at one edge having internal holes and attached masses are presented. Experimental natural frequencies and modal shapes are compared to those obtained by an analytical approximate solution based on the Rayleigh–Ritz method with the use of orthogonal polynomials as coordinate function. A high degree of correlation between computational analysis and experimental results was observed, proving the potentiality of the optical technique as experimental validation of the numerical simulations.     

Eine Metallfilmsonde zur Messung von kleinen und schnellen Strömungstemperaturschwankungen

Measurements of the temperature fluctuations in flows are restricted to low fluctuation frequencies, if the temperature probes which have been available and which have a relative high thermal inertia are used. A newly constructed metalfilm probe, which works in principle as a resistance thermometer, overcomes this restriction to a large degree so that temperature fluctuations in the order of 0.01 °C can be measured up to fluctuation frequencies of about 5 kHz. The construction, the procedure of manufacture, and a method of calibration are presented for the newly developed probe, and its applicability for the measurement of temperature fluctuations in flows is demonstrated by some examples (measurements of the natural temperature fluctuations in the wake of a circular rod in air flow at a Reynolds number of about 5 · 10⁴). Some further applications of the probe are mentioned, in which its high sensitivity and its low thermal inertia is especially advantageous (measurement of flow velocities and measurement of fast temperature variations by infra-red detectors).     

Background-oriented schlieren diagnostics for large-scale explosive testing

Experimental measurements of shock wave propagation from explosions of C4 are presented. Each test is recorded with a high-speed digital video camera and the shock wave is visualized using background-oriented schlieren (BOS). Two different processing techniques for BOS analysis are presented: image subtraction and image correlation. The image subtraction technique is found to provide higher resolution for identifying the location of a shock wave propagating into still air. The image correlation technique is more appropriate for identifying shock reflections and multiple shock impacts in a region with complex flow patterns. The optical shock propagation measurements are used to predict the peak overpressure and overpressure duration at different locations and are compared to experimental pressure gage measurements. The overpressure predictions agree well with the pressure gage measurements and the overpressure duration prediction is within an order of magnitude of the experimental measurements. The BOS technique is shown to be an important tool for explosive research which can be simply incorporated into typical large-scale outdoor tests.     

Fluidic control of wake-flow behind a two-dimensional square back bluff body

This experimental study deals with wake-flow fluidic control behind a two-dimensional square back geometry positioned close to the ground. The fluidic control system is made of pulsed jets positioned at the upper edge of the model base. The objective of the fluidic action is to modify the wake-flow development, and as a consequence the static pressure distribution over the model base and hence the pressure drag. The main concern of this study is to determine to what extent the presence of a flow confined between the model and the floor influences the effectiveness of the control. Static pressure measurements at the model base and wake-flow characteristics derived from PIV measurements at a high acquisition frequency indicate global similarities between a case where an underbody flow exists and a case where this underbody flow is absent. For low actuation frequencies, discrepancies in the way the coherent structures due to the control develop in the shear layer appear.     

Computed tomographic X-ray velocimetry for simultaneous 3D measurement of velocity and geometry in opaque vessels

Computed tomographic X-ray velocimetry has been developed for simultaneous three-dimensional measurement of flow and vessel geometry. The technique uses cross-correlation functions calculated from X-ray projection image pairs acquired at multiple viewing angles to tomographically reconstruct the flow through opaque objects with high resolution. The reconstruction is performed using an iterative, least squares approach. The simultaneous measurement of the object’s structure is performed with a limited projection tomography method. An extensive parametric study using Monte Carlo simulation reveals accurate measurements with as few as 3 projection angles, and a minimum required scan angle of only 30°. When using a single/source detector system, the technique is limited to measurement of periodic or steady flow fields; however, with the use of a multiple source/detector system, instantaneous measurement will be possible. Synchrotron experiments are conducted to demonstrate the simultaneous measurement of structure and flow in a complex geometry with strong three-dimensionality. The technique will find applications in biological flow measurement, and also in engineering applications where optical access is limited, such as in mineral processing.     

Rough terrain profiling using digital image correlation

Road profiling is an important aspect of vehicle dynamics simulations especially over rough terrains. The accurate measurement of rough terrains allows for more accurate multi body simulations. Three dimensional road profiles are usually performed by utilising a line scan sensor which measures several points lateral to the road. The sensors range from simple road following wheels to LiDAR sensors. The obtained line scans are longitudinally stitched together using the orientation and position of the sensor to obtain a full three dimensional road profile. The sensor’s position and orientation therefore needs to be accurately determined in order to combine the line scans to create an accurate representation of the terrain. The sensor’s position and orientation is normally measured using an expensive inertial measurement unit or Inertial Navigation System (INS) with high sensitivity, low noise and low drift. This paper proposes a road profiling technique which utilises stereography, based on two inexpensive digital cameras, to obtain three-dimensional measurements of the road. The system negates the use of an expensive INS system to determine orientation and position. The data sets also require subsampling which can be computationally expensive. A simple subsampling routine is presented which takes advantage of the structure of the data sets to significantly speed up the process.     

Manifestation of phase separation processes in oscillatory shear: droplet-matrix systems versus co-continuous morphologies

Phase separation processes in mixtures of poly-α-methylstyrene-co-acrylonitrile (PαMSAN) and poly-methylmethacrylate (PMMA) with lower critical solution temperature (LCST) behavior have been studied, focusing on the manifestation of the interface in oscillatory shear measurements. By using blends of different composition, systems with a droplet-matrix morphology or a co-continuous structure are generated during the phase separation process. The feasibility of probing this morphology development by rheological measurements has been investigated. The development of a disperse droplet phase leads to an increase in the elasticity of the blend at low frequency, showing up as a shoulder in the plot of storage modulus versus frequency. Here, the droplet growth is unaffected by the shear amplitude up to strains of 0.2; therefore the resulting dynamic data are suitable for quantitative analysis. In contrast, for blends in which phase separation leads to a co-continuous structure, the storage modulus shows a power law behavior at low frequency and its value decreases as time proceeds. For the latter systems, effects of the dynamic measurement on the morphology development have been observed, even for strain amplitudes as low as 0.01. To probe the kinetics of morphology evolution in droplet-matrix systems, measurements of the time dependence of the dynamic moduli at fixed frequency should be performed (for a whole series of frequencies). Only from such measurements, curves of the frequency dependence of the moduli at a well defined residence time can be constructed. From fitting these curves to the emulsion model of Palierne, the droplet diameter distribution at that particular stage in the phase separation and growth process can be obtained. It is not appropriate to use a simplified version of the Palierne model containing only the average droplet size, because a morphology with too broad a size distribution is generated. Received: 15 February 1999 Accepted: 20 May 1999     

Application of pressure-sensitive paint for determination of the pressure field and calculation of the forces and moments of models in a wind tunnel

The visualization and measurements of aerodynamic effects on a 3D aircraft model were conducted using an optical pressure measurement system, based on the pressure-sensitive paint (PSP) technique. PSP technology provides a good understanding of the flow around the wind tunnel model. The PSP technique can be used to carry out absolute pressure measurements on a surface of the model and to determine additional aerodynamic data using scientific-grade cameras and image processing techniques. Surface pressures from the top, bottom, left, and right viewing directions were obtained using the DLR-PSP system on the entire surface, which can be observed by eight CCD cameras. Finally, the measured pressures can be integrated to calculate the forces and moments of the complete model, or parts thereof.     

Ultrasonic waves in layered anisotropic media: characterization of multidirectional composites

An efficient and stable recursive compliance/stiffness matrix algorithm is presented to model wave propagation in multidirectional composites. The models are applied to clarify angle beam transmission through a multidirectional composite and to process ultrasonic data for determination of the elastic properties of a composite lamina (single ply) from measurements on a multidirectional composite. Ultrasonic characterization of composites using double-through-transmission and time-resolved line focus acoustic microscopy has been addressed. The double-through-transmission measurements and simulations show that the transmission amplitude is highly dependent on ply orientation and angle of incidence. The transmission amplitude decreases rapidly with incident angle deviation from the normal; however, a transmission window is found in the incident angle range 45–60° at frequencies below 2.25 MHz. The time-delay measurements by the double-through-transmission technique have been used to reconstruct lamina properties using the Floquet wave concept. A unidirectional lamina elastic properties measurement using line focus acoustic microscopy of a multidirectional composite sample is also briefly discussed. The effective elastic properties for the composites are determined from the lamina properties by a Floquet wave dynamic homogenization method.     

Ultrasonic waves in layered anisotropic media: characterization of multidirectional composites

An efficient and stable recursive compliance/stiffness matrix algorithm is presented to model wave propagation in multidirectional composites. The models are applied to clarify angle beam transmission through a multidirectional composite and to process ultrasonic data for determination of the elastic properties of a composite lamina (single ply) from measurements on a multidirectional composite. Ultrasonic characterization of composites using double-through-transmission and time-resolved line focus acoustic microscopy has been addressed. The double-through-transmission measurements and simulations show that the transmission amplitude is highly dependent on ply orientation and angle of incidence. The transmission amplitude decreases rapidly with incident angle deviation from the normal; however, a transmission window is found in the incident angle range 45–60° at frequencies below 2.25 MHz. The time-delay measurements by the double-through-transmission technique have been used to reconstruct lamina properties using the Floquet wave concept. A unidirectional lamina elastic properties measurement using line focus acoustic microscopy of a multidirectional composite sample is also briefly discussed. The effective elastic properties for the composites are determined from the lamina properties by a Floquet wave dynamic homogenization method.     

Cross Polarization for Improved Digital Image Correlation

Digital image correlation (DIC) is a surface deformation measurement technique for which accuracy and precision are sensitive to image quality. This work presents cross polarization, the use of orthogonal linear polarizers on light source(s) and camera(s), as an effective method for improving optical DIC measurements. The benefits of cross polarization are characterized through quantitative and statistical comparisons from two experiments: rigid body translation of a flat sample and uniaxial tension of a superelastic shape-memory alloy (SMA). In both experiments, cross polarization eliminated saturated pixels that degrade DIC measurements, and increased image contrast, which enabled higher spatial precision by using smaller subsets. Subset sizes are usually optimized for correlation confidence interval (typically with subsets of 21×21 px or larger), but can be decreased to achieve the highest possible spatial precision at the expense of increased correlation confidence intervals. Smaller subset sizes (such as 9×9 px) require better images to maintain correlation within error thresholds. By comparing DIC results from a uniaxial SMA tension test with unpolarized and cross-polarized images, we show that for 9×9 px subsets, the loss of valid DIC data points was reduced almost ten-fold with cross polarization. The only disadvantage we see to cross polarization is the decrease in specimen illumination due to transmission losses through the polarizers, which can easily be accommodated with sufficiently intense light sources. With the installation of relatively inexpensive linear polarizing filters, an optimum optical DIC setup can provide even better DIC measurements by delivering images without saturated pixels and with higher contrast for increased DIC spatial precision.     

Characterization of pressure dynamics in an axisymmetric separating/reattaching flow using fast-responding pressure-sensitive paint

This collaborative work discusses the results of time-resolved pressure-sensitive paint measurements performed on a model of a generic spacecraft under sub- and transonic test conditions. It is shown that optical pressure measurements using an active layer from platinum?Cporphyrin complexes (PtTFPP) in combination with a polymer-ceramic base layer are able to measure dynamic flow phenomena in the trisonic wind tunnel facility up to sampling rates of 2?kHz. Low amplitude fluctuations in the order of 0.1?kPa were determined by means of this measurement technique. The buffet dynamics, as well as the spatial extent of the recirculation area in the near-wake, compare well with numerical predictions and PIV measurements. Furthermore, characteristic coherent pressure modes on the base were resolved, which were predicted by large-eddy simulations.