电流退火铁基薄带巨磁阻抗效应的影响

研究了电流退火工艺对铁基非晶合金Fe₈₄Zr₈Nb_3.5B_3.5Cu_{1〈/sub>薄带巨磁阻抗效应的影响.实验结果表明,该铁基合金的巨磁阻抗ΔZ/Z随退火电流的增加而增强,当电流为820mA时,ΔZ/Z达到最大值62％,阻抗变化灵敏度可达约0.23％（A/m)^-1.结合此合金在电流退火燧后电性能和软磁性能的演变,讨论了材料的巨磁阻抗效应借助趋肤效应与交流频率和外加纵向磁场的关系. 关键词：}     

The influence of a demagnetizing field on hysteresis losses in a dense assembly of superparamagnetic nanoparticles

The electrodynamic method is used to measure the hysteresis losses of a dense assembly of magnetite nanoparticles with an average diameter D=25 nm in the frequency range f=10–150 kHz and for magnetic field amplitudes H₀=100–300 Oe. It is found that the specific loss power is determined by a demagnetizing factor of a whole sample. It diminishes approximately 4.5 times when the sample aspect ratio decreases from L/d=11.4 to L/d≈1, where L and d are the sample length and diameter, respectively. For H₀≤300 Oe the maximal specific loss power 120 W/g is obtained for the sample with L/d=11.4 at f=120 kHz. For comparison, the assembly specific absorption rate has been determined also by means of direct measurement of the temperature difference between the inner and outer surfaces of a flat cuvette containing magnetic nanoparticles. For both methods of measurement close values for the specific absorption rate are obtained for samples with similar demagnetizing factors.     

Giant magnetoimpedance effect and voltage response in meander shape Co-based ribbon

Field-annealed Co-based amorphous ribbon (Metglas^® 2705M) with a meander structure is fabricated by MEMS technology and the giant magnetoimpedance (GMI) effects are studied at different magnetic fields and frequencies. The maximum longitudinal GMI ratio of the ribbon is 193.7% and the magnetic field sensitivity is 17.4%/Oe. The maximum GMI ratio of the meander ribbon is much larger than the single strip ribbon mainly due to the larger change ratio of inductance L. The sensitivity of an output U reach up to 10 V/A and U thermal fluctuation is less than 15 mV in the temperature range of ?20 to 40°C. This meander shape ribbon can be considered as a good candidate for the GMI-based sensor fabrication.     

Transverse anisotropy field and lattice plane anisotropy of stress annealed Fe–Cu–Nb–Si–B ribbons

The transverse magnetic anisotropy and lattice plane anisotropy of stress-annealed Fe–Cu–Nb–Si–B amorphous ribbons have been studied. The GMI effect or impedance ratio decreased gradually with increasing applied tensile stress. The transverse anisotropy field (H_k) corresponded to the full width at half maximum (FWHM) of the GMI curves. A linear response was found between the applied tensile stress (σ) and the transverse anisotropy field (H_k), and it was seen from the linear expression that annealing without stress resulted in a very small H_k of ～200 A/m. We also calculated the strains from the elongations obtained during the stress annealing process, the results showed that the strain and applied stress were linearly related and for a zero-tensile stress, the elastic strain was negative (?0.0219) showing that contraction dominates during annealing without tensile stresses. The lattice plane anisotropy (Δd) calculated from XRD peaks was also linearly related to the applied tensile stress. The lattice spacing in the direction parallel to the tensile stress was elongated while the lattice spacing in the direction perpendicular to the tensile stress was compressed.     

FeCuNbSiB单层膜和三明治膜的磁特性与巨磁阻抗效应

用射频溅射法制备了Fe_73.5Cu₁Nb₃Si_13.5B₉单层膜和 Cu或Ag作为中间层的三明治膜.溅态膜为非晶态结构.磁畴观察结果表明,单层膜在380℃退火后,呈现均匀磁化的纳米晶结构,该样品软磁特性最佳,其巨磁阻抗效应最大,在13MHz,最大磁阻抗比纵向为18％,横向为14％.溅态三明治膜具有较大的巨磁阻抗效应,在13MHz,Cu夹层三明治膜的最大磁阻抗比纵向为32％,横向为11％,Ag夹层三明治膜的最大磁阻抗比纵向为47％,横向为57％.Cu夹层三明治膜经250℃退火后,在低频下表现为巨磁电感效应,在100kHz,最大磁电感比为1733％. 关键词：     

On the natural width of the hypersatellite lines

The natural width of a hypersatellite line (K ^?2→K ^?1 L ^?1 transition) has been measured for the first time. In the case of Cu (Z=29) this width has been found equal toΓ = 5 eV, i.e. much larger than that of the diagram (K ^?1→L ^?1) line. This result follows a proposed empirical law assuming this width to be equal to 3Γ _K+Γ_L.     

Giant magnetoimpedance in amorphous (Co0.93Fe0.7)63Ni10Si11B16 glass-coated microwire

Giant magnetoimpedance (GMI) effect has been measured in a glass-coated amorphous (Co_0.93Fe_0.7)₆₃Ni₁₀Si₁₁B₁₆ microwire as a function of DC magnetic field and up to the frequency of 11 MHz. The sample shows single peak GMI characteristics within the whole range of frequency. The domain structure of the above sample has been changed by applying tensile stresses up to 603 MPa and current annealing with a DC current of 50 mA for various time durations, and the corresponding effect on GMI has been studied in detail. A maximum change of 8.85% in MI of the as-quenched sample has been observed around a frequency of 5.05 MHz. Application of an external tensile stress reduces the GMI value by increasing the inner core domain, whereas heat treatment of the sample enhances the same. The square-shaped magnetic hysteresis loop of the as-quenched sample helps us understanding the MI results.     

射频溅射功率对FeZrBCu软磁合金薄膜巨磁阻抗效应的影响

用射频溅射法制备了FeZrBCu软磁合金薄膜.研究了不同溅射功率对FeZrBCu薄膜软磁特性和巨磁阻抗效应的影响.用电子探针显微镜测量发现，当溅射功率为240W时，薄膜样品中Fe的原子含量为8732%，Cu的原子含量为29%.这种样品的矫顽力最小，为68A/m，饱和磁化强度约为111×105⁵A/m，软磁性能最佳，巨磁阻抗效应最大，溅态膜在 13MHz最大巨磁阻抗比纵向为17%，横向为11%.重点分析了阻抗的电阻、电感分量及横向有 效磁导率随频率的变化，得到在低频下主要是磁电感 关键词： 铁基合金 薄膜 巨磁阻抗效应     

交流电流对铁基纳米晶丝巨磁阻抗效应形貌的影响

本文研究了交流电流的大小(I ＝0.2—20 mA)和频率(f ＝ 1—1 MHz)对具有横向畴结构的铁基纳米晶丝的巨磁阻抗效应形貌的影响.实验结果表明,样品的巨磁阻抗效应呈双峰特征,随着频率的增大,双峰的位置H=±H_m向高场移动;但随着电流的增大,双峰的位置逐渐向中心(H ＝ 0)收缩,甚至变成单峰位形.理论上一般认为,双峰的位置与横向各向异性场H_k相对应,即H< 关键词： 巨磁阻抗效应 交流电流 铁基纳米晶丝     

Study of the structural and magnetic characteristics of epitaxial Fe3Si/Si(111) films

The results of the structural and magnetic studies of the epitaxial structure prepared during the simultaneous evaporation from two iron and silicon sources on an atomically pure Si(111)7 × 7 surface at a substrate temperature of 150°C have been presented. The epitaxial structure has been identified as a single-crystal Fe₃Si silicide film with the orientation Si[111]‖Fe₃Si[111] using methods of the X-ray structural analysis, transmission electron microscopy, and reflection high-energy electron diffraction. It has been established that the epitaxial Fe₃Si film at room temperature has magnetic uniaxial anisotropy (H _a = 26 Oe) and a relatively narrow uniform ferromagnetic resonance line (ΔH = 11.57 Oe) measured at a pump frequency of 2.274 GHz.     

Tuning giant magnetoimpedance response of Fe75.5Si13.5B7Nb3Cu1 amorphous ribbon by laser ablation

An easy method of tuning the response of maximum magnetoimpedance (MI) ratio in Fe_75.5Si_13.5B₇Nb₃Cu₁ amorphous ribbons was investigated by laser ablation. In order to obtain different GMI peak positions, the stripes were ablated by laser with different separations on the surface layer of the ribbon. When the stripes were parallel (or perpendicular) to the applied magnetic field, the peak location of maximum MI ratio would drift to larger (or smaller) external field. And the shift was correlated with the spaces between stripes. The applied fields corresponding to the minimum and maximum values of peak location are 13 Oe and 49 Oe at the frequency of 15 MHz, respectively. The phenomenon can be explained by the anisotropy field induced by demagnetizing field after the laser ablation.     

Magneto-Impedance behavior of Co-Fe-Nb-Si-B-based ribbons

The giant magneto-impedance of melt spun Co_xFe_72−xNb₄Si₄B₂₀(x=10, 20, 36, 50) amorphous and nanostructured ribbons have been investigated. Alloys have been optimized at the driving current amplitude, frequency and found that amorphous ribbon of nominal composition of Co₃₆Fe₃₆Nb₄Si₄B₂₀ shown maximum GMI ratio of 13%. The behaviour of the driving current amplitude on the GMI behaviour was studied and the sample was optimized for driving current amplitude, I_ac=10 mA. The frequency dependence of the GMI behaviour was studied for the ribbon sample Co₃₆Fe₃₆Nb₄Si₄B₂₀ at frequency in the range of 100 kHz-1.2 MHz of the optimized driving current amplitude and it was found that the sample showed the maximum GMI behaviour at f=700 kHz. The optimized samples were Joule heated at the current density J=0-35 A/m² for a period of 1 min. The GMI ratio initially increased then progressively deteriorated with J, but after a certain range it shows up to 16% of improvement in the magneto-impedance value due the increase of nanocrystalline volume fraction. The asymmetry in the GMI profile was observed for the sample Joule heated at J=1-5 A/m² for 1 min.     

Dependence of the driving current on the harmonic behavior of giant magneto-impedance voltage of Co-based amorphous wires

The frequency and the amplitude of the driving AC current dependence on the harmonic behavior of the giant magneto-impedance (GMI) voltage of Co-rich amorphous wire have been studied. Single-peak, two-peak and three-peak behavior in the GMI characteristics was studied with the change of amplitude and frequency of the AC current. GMI ratio was calculated from the first harmonic signals which were initially increased and then decreased monotonically with the increase of frequency (f) and the amplitude (I_AC) of the driving current. The response of the GMI voltage was found non-linear with the generation of higher harmonics at higher amplitude of the driving current. The second and third harmonic signals were also evaluated and their dependence on the driving current amplitude and frequency were presented in the paper. The experimental results were analyzed using single domain rotational model. The voltage harmonics were calculated through Fourier transform of the time derivative of the estimated circular magnetization of the sample.     

Faraday effect on the Rb <Emphasis Type="Italic">D</Emphasis> <Subscript>1</Subscript> line in a cell with a thickness of half the wavelength of light

The rotation of the radiation polarization plane in a longitudinal magnetic field (Faraday effect) on the D₁ line in atomic Rb vapor has been studied with the use of a nanocell with the thickness L varying in the range of 100–900 nm. It has been shown that an important parameter is the ratio L/λ, where λ = 795 nm is the wavelength of laser radiation resonant with the D₁ line. The best parameters of the signal of rotation of the radiation polarization plane have been obtained at the thickness L = λ/2 = 397.5 nm. The fabricated nanocell had a large region with such a thickness. The spectral width of the signal reached at the thickness L = 397.5 nm is approximately 30 MHz, which is much smaller than the spectral width (≈ 500 MHz) reached with ordinary cells with a thickness in the range of 1–100 mm. The parameters of the Faraday rotation signal have been studied as functions of the temperature of the nanocell, the laser power, and the magnetic field strength. The signal has been reliably detected at the laser power P_L ≥ 1 μW, magnetic field strength B ≥ 0.5 G, and the temperature of the nanocell T ≥ 100°C. It has been shown that the maximum rotation angle of the polarization plane in the longitudinal magnetic field is reached on the F_g = 3 → F_e = 2 transition of the ⁸⁵Rb atom. The spectral profile of the Faraday rotation signal has a specific shape with a sharp peak, which promotes its applications. In particular, Rb atomic transitions in high magnetic fields about 1000 G are split into a large number of components, which are completely spectrally resolved and allow the study of the behavior of an individual transition.     

Peculiarities of the Giant Magnetoimpedance in Permalloy-Based Film Structures in the Important Temperature Range for Practical Applications

Multilayer structures based on Fe19Ni81 films have been obtained by ion-plasma sputtering and investigated on an impedance spectroscopy apparatus equipped with a temperature unit. An increase in the magnetoimpedance ratios for the total impedance and its real part has been found for the multilayer structure (Cu/FeNi)₅/Cu/(Cu/FeNi)₅ upon heating from 25 to 50°C. The maximum of the giant magnetoimpedance ratio of the total impedance ΔZ/Z = 56% has been observed at a frequency of 80 MHz with a sensitivity of 18%/Oe, while the maximum of the real part ΔR/R = 170% was observed at the frequency of 10 MHz with the sensitivity of 46%/Oe. Magnetization and resistivity at the direct current have been found to depend insignificantly on the temperature and, hence, the relaxation mechanism due to the magnetoelastic anisotropy was proposed as the most probable mechanism of increasing the value and sensitivity of the magnetoimpedance effect.     

Numerical simulation of wall dynamics in (111)-oriented garnet films in the presence of an in-plane magnetic field

The domain wall motion in the presence of an in-plane magnetic field H_y perpendicular to the wall is simulated using a fall implicit numerical scheme. Calculations are performed for the drive fields 0 Oe<H_z<15 Oe and in-plane fields -210 Oe?H_y?210 Oe. The relation between the average wall velocity $\text{v}$ and the drive field H_z is discussed considering the wall structure. It was found that an in-plane field increases the peak velocity of the wall and extends the range of the drive fields, where the linear mobility relation is valid. A dynamical Bloch line stacking was found for sufficiently large drives. The influence of an in-plane field on the angular span of horizontal Bloch lines is discussed also. In particular the occurrence of 2π-horizontal Bloch lines is described. Numerical results obtained with a full implicit method are compared with the experimental observations of bubble motion and good agreement is found for |H_y|≤100 Oe.     

Effect of magnetic field annealing and size on the giant magnetoimpedance in micro-patterned Co-based ribbon with a meander structure

Micro-patterned Co-based amorphous ribbons (Metglas^® 2714A) with a meander structure are fabricated by MEMS technology and the giant magnetoimpedance (GMI) effects are measured at different magnetic fields and frequencies. The effect of magnetic field annealing and size (line width and line length) on the GMI effect is investigated. It is found that the GMI effect in the transverse magnetic field-annealed state is larger than that in longitudinal magnetic field-annealed state and nonfield-annealed state. The maximum GMI effect increases from 82 % for the sample with 5 mm length to 150 % for the sample with 10 mm length, and the maximum GMI effect decreases with the increase of the line width.     

磁场退火对Co基熔体抽拉丝巨磁阻抗效应的影响

对Co基熔体抽拉非晶丝进行了普通炉内退火和不同磁场强度（500 Oe,1600 Oe,4000 Oe）下的横向和纵向磁场退火,利用HP4192阻抗分析仪和Lakeshore7407VSM分析了退火态样品的巨磁阻抗（GMI）效应和软磁性能.研究结果表明,纵向磁场降低了环向各向异性,纵向磁场退火样品GMI效应降低且GMI曲线为单峰,最大阻抗变化率ΔZ/Z为131%,磁场响应灵敏度为7%/Oe;而横向磁场提高了环向畴体积,增加了环向各向异性场,导致退火样品GMI曲线随频率升高由单峰转 关键词： 非晶丝 巨磁阻抗效应 退火     

The magnetization of PrFeAsO0.60F0.12 superconductor

The magnetization of the PrFeAsO_0.60F_0.12 polycrystalline sample has been measured as functions of temperature and magnetic field (H). The observed total magnetization is the sum of a superconducting irreversible magnetization and a paramagnetic magnetization. Analysis of dc susceptibility χ(T) in the normal state shows that the paramagnetic component of magnetization comes from the Pr³⁺ magnetic moments. The intragrain critical current density (J_L) derived from the magnetization data is large. The J_L(H) curve displays a second peak which shifts towards the high-field region with decreasing temperature. In the low-field region, a plateau up to a field H^* followed by a power law H^?5/8 behavior of J_L(H) is the characteristic of the strong pinning. A vortex phase diagram for the present superconductor has been obtained from the magnetization and resistivity data.     

电沉积复合丝及其巨磁阻抗效应的研究

采用脉冲电沉积工艺在Cu丝上沉积Fe Ni合金镀层 ,成功地制备出巨磁阻抗效应 (GMI)复合丝材料 ,研究了复合丝的磁性能和巨磁阻抗效应 .复合丝外壳磁性镀层软磁性越好 ,巨磁阻抗效应越明显 ,制备的复合丝最高巨磁阻抗效应为 2 7.19% .研究了复合丝阻抗与巨磁阻抗比值GMI随外加磁场的变化 ,其变化曲线的形状受复合丝磁各向异性场的影响 .此外 ,还研究了复合丝巨磁阻抗效应与驱动交变电流频率的关系 ,复合丝Fe17Ni83 样品巨磁阻抗效应的临界频率为 30kHz(GMI为 9.95 % ) ,特征频率为 30 0kHz(GMI为 2 7.19% ) ,截止频率为 10MHz (GMI为 10 .36 % ) .如此低的临界频率和特征频率及较宽的频率段对于实际应用非常有利 .