热稳定法拉第旋转TbYbBiIG磁光单晶及性能

采用高温溶液法，以Ｂｉ２Ｏ３／Ｂ２Ｏ３为助熔剂成功地生长出掺铋复合稀土铁石榴石（ＴｂＹｂＢｉ）３Ｆｅ５Ｏ１２（简称ＴｂＹｂＢｉＩＧ）晶体。晶体外形规则，最大尺寸为７×６×４ｍｍ３，Ｘ射线衍射分析证实，生长的晶体为ＴｂＹｂＢｉＩＧ单相单晶体，扫描电镜能谱分析其组成为Ｔｂ２．０６Ｙｂ０．４６Ｂｉ０．４８Ｆｅ５Ｏ１２。在１．０μｍ～１．７μｍ波段测量出晶体法拉第旋转谱和光吸收谱。当λ＝１．５５μｍ时，在１０°Ｃ～８０°Ｃ温度范围内测得法拉第旋转θＦ的温度系数为ｄθＦ／ｄＴ＝－２．３×１０－２ｄｅｇ·ｍｍ－１Ｋ－１。研究结果表明，ＴｂＹｂＢｉＩＧ单晶体在近红外波段θＦ约为ＹＩＧ单晶的３倍，温度系数小，是制作高性能光隔离器的一种好材料     

Pb、La掺杂Bi2201相高质量单晶的生长和表征

自助熔法从富Ｂｉ２Ｏ３ 的Ｂｉ１ ．８ ＋ ｘＰｂ０ ．２Ｓｒ１ ．６５Ｌａ０ ．３５ＣｕＯｙ（ｘ＝ ０ ．１ ,０ ．２,０ ．３ ,０．４ ,０ ．５） 熔体中生长出了高质量的Ｐｂ、Ｌａ 掺杂的Ｂｉ２２０１ 相大单晶,最大尺寸达８ ×４ ×０ ．０５ｍｍ３ ．在生长单晶时不同程度过量的Ｂｉ２Ｏ３ 用作助熔剂,最佳助熔剂含量以及最佳温度控制过程被确定．通过单晶的（００ｌ） ＸＲａｙ 衍射和摇摆曲线以及电子衍射对一块尺寸为４ ×１ ．６ ×０ ．０３ｍｍ３ 的高质量单晶做了结构表征．由试验发现从富Ｂｉ２Ｏ３ 的熔体中生长高质量Ｂｉ２２０１ 相大单晶的关键是合适的助熔剂含量和温度控制过程     

单畴YBCO块材的晶粒取向对磁悬浮力的影响

熔化生产工艺是制备高性能ＹＢＣＯ块材的重要方法。用该方法制备的直径为Х３０ｍｍ的单畴ＹＢＣＯ块材在７７．３Ｋ下磁悬浮力达７０Ｎ。将该样品按晶体的取向不同切割成尺寸为３．５×３．５×５ｍｍ＾３的一组样品,分别对其磁悬浮力进行测量。结果发现,取向不机样品的磁悬浮力随着ｃ轴与磁场方向夹角θ（０≤θ≤９０°）的增加而单调减小。在此基础上,提出了一个简单的物理模型,通过计算对实验结果作了满意的解释。     

Li2B4O7晶体生长及其二次谐波系数

用恰克拉斯基（Ｃｚｏｃｈｒａｌｓｋｉ）法特殊工艺生长出尺寸为Φ３０×３０ｍｍ的优质Ｌｉ２Ｂ４Ｏ７单晶，讨论了工艺参数对晶体宏观缺陷的影响。用Ｍａｋｅｒ条纹测量了晶体的二次谐波系数ｄ３１和ｄ３３，结果表明，Ｌｉ２Ｂ４Ｏ７的ｄ３３是石英晶体ｄ１１的三倍。     

NdvGdCOB晶体1331.0nm基频光运转和自倍频红光的观察

ＮｄｖＣａ４ＧｄＯ（ＢＯ３）３（简称ＮｄｖＧｄＣＯＢ）是一种新型自倍频晶体［１］。利用该晶体实现１０６０．０ｎｍ的自倍频绿光输出,因内外均已有报道［２］。我们利用Ｄａｔａｃｈｒｏｍ５０００型染料激光器泵浦该晶体成功地实现了１３３１．０ｎｍ基频光和６６５．５ｎｍ自倍频红光的输出。ＮｄｖＧｄＣＯＢ属单斜双轴晶体,具有明显的偏振吸收特性。生长该晶体所用原料为Ｃａ４Ｎｄ０．０８Ｇｄ０．９２Ｏ（ＢＯ３）３。晶体样品尺寸为３ｍｍ×３ｍｍ×８ｍｍ,通光方向为ｘ（ｘ轴与晶体的ｃ轴的夹角为１２°,ｚ轴与ａ轴的夹…     

新型蓝光衬底材料LiAlO_2晶体的生长和缺陷分析

ＬｉＡｌＯ２和ＧａＮ的晶格失配率只有１．４％，是一种很有希望的ＧａＮ外延生长衬底材料。本文利用温度梯度法生长出了透明的ＬｉＡｌＯ２单晶，并通过化学浸蚀、光学显微镜、透射电子显微镜、同步辐射Ｘ射线貌相术对晶体中的缺陷进行了检测。结果表明：ＬｉＡｌＯ２在钼坩埚中无籽晶自由凝固结晶时，是沿（１００）方向生长。用温度梯度法生长的ＬｉＡｌＯ２晶体质量良好，晶体中无气泡和包裹物。在ＬｉＡｌＯ２（１００）晶面上测得的位错密度为（３．８～６．０）×１０４ｃｍ－２，晶体中的主要缺陷为亚晶界或镶嵌结构，可能是由于温场不稳定、生长速率太快造成的。     

铊系超导单昌的低温生长

采用蠕爬型助熔剂ＣａＯ－ＣｕＯ和蒸发型复合助熔剂ＣａＯ－ＣｕＯ－ＮａＣｌ来制备Ｔｌ－Ｂａ－Ｃａ－Ｃｕ－Ｏ超导单晶，生长炉最高温度８９０℃和８５０℃，因而实现了铊系单晶的低温生工。生长出的单晶分别是典型尺寸为２．０×１．５×０．２ｍｍ＾３，Ｔｃ在１００Ｋ与１１９Ｋ之间的Ｔｌ－２２１２相单晶和尺寸为１．２×１．０×０．１ｍｍ＾３。Ｔｃ约为１１５Ｋ的Ｔｌ－２２２３相超导单晶。     

激光沉积法制备（Y1—xHox）Ba2Cu3O7—δ薄膜

本文报道了用激光沉积法在（１００）ＬａＡｌＯ３衬底上制备（Ｙ１－ｘＨｏｘ）Ｂａ２Ｃｕ３Ｏ７－δ（ｘ＝０，０．２，０．４）超导薄膜．结果表明，新超导薄膜表面光滑，具有很强的ｃ轴织构，零电阻温度Ｔｃ０约９１Ｋ，最佳临界电流密度Ｊｃ为４．７×１０６Ａ／ｃｍ２（７７Ｋ）．     

双水相体系中Cu(Ⅱ)的显色反应研究

本文研究了铬黑Ｔ（ＥＢＴ）作萃取剂和显色剂,在聚乙二醇－２０００（ＰＥＧ）－Ｎａ２ＳＯ４－ＥＢＴ双水相体系中Ｃｕ（Ⅱ）的显色反应条件及应用,实验结果表明,在ｐＨ８．５缓冲溶液中,将Ｃｕ（Ⅱ）络合物从水溶液中萃取到ＰＥＧ相,其最大吸收波长位于５６０ｎｍ,摩尔吸光系数为３．０５×１０＾４Ｌ·ｍｏｌ＾－１·ｃｍ＾－１,此法用于铝合金中铜的测定,获得了满意结果。     

铊系超导单晶的低温生长

采用蠕爬型助熔剂ＣａＯ－ＣｕＯ和蒸发型复合助熔剂ＣａＯ－ＣｕＯ－ＮａＣｌ来制备Ｔｌ－Ｂａ－Ｃａ－ＣＵ－Ｏ超导单晶，生长炉最高温度分别为８９０℃和８５０℃，因而实现了铊系单晶的低温生长．生长出的单晶分别是典型尺寸为２．０×１．５×０．２ｍｍ３，Ｔｃ在１００Ｋ与１１９Ｋ之间的Ｔｌ－２２１２相单晶和尺寸为１．２×１．０×０．１ｍｍ３，Ｔｃ约为１１５Ｋ的Ｔｌ－２２２３相超导单晶．采用蠕爬型助熔剂可以降低熔点而不引进其它非组元杂质，但导致熔料蠕爬，对生长大块单晶不利．采用蒸发型复合助熔剂克服了熔料的蠕爬现象，减少了铊的损失，对生长多铜氧层的单晶有利．     

数字剪切散班干涉术中的刚体位移补偿的新方法

给出一个数字剪切散斑干涉术中的刚体位移补偿的新方法。当刚体位移大于一个像素时，加载前后的散斑图将会由于位置的变化导致失相关。重新安排每一个像素将会克服此失相关。散斑平均、条纹重构以及迭代方法用来改善条纹质量，消除散斑噪声，最后得到可取结果。     

A novel method to obtain electronic speckle pattern interferometry fringe patterns with high contrast

Traditional speckle fringe patterns of electronic speckle pattern interferometry （ESPI） are obtained by adding, subtracting, or multiplying the speckle patterns recorded before and after the deformation. However, these speckle fringe patterns are of limited visibility, especially for addition and multiplication fringe patterns. We propose a novel method to obtain speckle fringe patterns of ESPI from undeformed and deformed speckle patterns. The fringe pattern generated by our method is of high contrast and has better quality than subtraction fringe. The new method is simple and does not require more computational effort. The proposed method is tested on the experimentally obtained undeformed and deformed speckle patterns. The experimental results illustrate the performance of this approach.     

Technique for compensating excessive rigid body motion in nondestructive testing of large structures using shearography

A major limitation of speckle interferometry techniques including shearography is that the occurrence of rigid body motion produces a decorrelation of speckle patterns which destroys the fringe visibility. This paper demonstrates that digital shearography can tolerate much greater rigid body translation than a speckle size as predicted by the conventional speckle decorrelation theory. Excessive rigid body translation in digital shearography can be compensated by either translating the sensor/camera or digitally shifting one of the speckle patterns.     

Holography, speckle, and computers

Surveys are presented on automatic and quantitative deformation measurements using CCDs and computers in holographic interferometry and speckle metrology for diffusely reflecting surfaces. For delivering relationships between object deformation and observed quantities, we discuss formations of fringes and signals observed in these methods in terms of correlation functions of spatially randomly varying complex amplitude of light. Dependencies of the observed patterns on object deformation and optical systems are discussed. Physical meanings of the derived relationships are explained in terms of the dynamic behaviors of speckles resulting from surface deformation. Automatic measurements are described in chronological orders. They include analysis of fringe patterns resulting from photographic recording of specklegrams, video recording and analysis of speckle patterns used in electronic speckle pattern interferometry as well as direct digital correlation techniques, and digital holography that uses both digital recording and reconstruction of holograms.     

基于条纹等值线相关的散斑条纹图处理新方法

在数字散斑干涉术中,通常由物体变形前后得到的两幅原始散斑场用相减方法来得到条纹图,并由相移后的多幅(三幅以上)条纹图来求取相位场。介绍了一种基于条纹等值线相关的条纹图生成新方法,并在此基础上提出了基于单幅干涉条纹图的相位场提取新方法和基于条纹等值线相关的单步相移新方法。实验结果表明,该方法具有良好的结果和发展前景。     

测量物体位移的数字白光散斑照相术

给出了一测量物体刚体位移的数字白光散斑照相术。数字傅里叶变换从双曝光字白光散斑图用来产生杨氏条纹。该杨氏条纹能够用数字傅里叶变换结合条纹重构进行自动分析。此外，给出一种条纹质量增强的方法。     

Contrast of time-averaged image speckle pattern for a vibrating object

In vibration analysis by speckle photography it is qualitatively known that the contrast of speckle patterns averaged in the exposure time varies, depending on the object motion. In this paper, the contrast of time-averaged image speckle patterns is theoretically evaluated and found to be determined by the ratio of the sinusoidally oscillating amplitude of the object motion to the average size of static speckles. An effect of the film response on the contrast of time-averaged speckle patterns is also studied.     

运动界面上反射超声散斑空间运动的研究

在Kirchhoff 衍射理论的基础上，应用随机信号相关原理，推导了作刚体运动的界面上反射超声散斑在空间运动时，保持其复振幅相关的必要条件.由此得到超声散斑的空间运动公式.界面、超声散斑和超声接收探头之间的相对运动，导致界面孔径的改变.分析表明，在保持界面孔径相关的条件下，界面所允许的最大平移量和转角值，与声源位置、接收用聚焦探头的数值孔径、超声入射角以及观察角有关.应用数字相关技术和三维扫描信号采集系统，根据散斑场子集相关系数的单峰性质，对超声散斑空间运动公式进行了实验验证.实验结果表明，理论分析所得的 关键词： 超声散斑 相关原理 空间运动     

散斑干涉相位条纹图的频域滤波处理

为了解决在数字散斑干涉技术测量时,散斑干涉相位条纹图像中大量噪声对相位解包裹结果和精度产生严重影响的问题,介绍了一种条纹正余弦分解和频域低通滤波结合的方法,实现了散斑干涉相位条纹图的高精度滤波。该方法的基本思路是在对相位图像进行滤波处理前,先将相位图通过正余弦函数进行映射转换成两幅图,分别经过频域滤波,然后再合成为相位图。这种分解频域滤波方法可以在滤波的同时,有效保留相位跳变信息。实验结果表明：与传统的图像降噪方法相比,该方法能够在保留图像“尖峰”信息的基础上,较好地滤除图像中的散斑噪声,方法简单有效,有效解决了传统滤波方法应用在相位条纹图中,相图灰度信息丢失10%~40%的问题。     

Use of a joint transform correlator architecture for study of speckle displacements

The optical speckle–displacement correlation technique (OSDCT) is proposed for study of in-plane speckle displacements. The joint transform correlator architecture is used to evaluate the displacements of speckle subimages of strained surfaces. The procedure of the correlation response producing as a result of cross-correlation of strainless and strained surfaces in a conventional joint transform correlator (JTC) is considered. The convenient techniques for a joint power spectrum transformation are selected. The systematic and random errors of a mean speckle pattern displacement of a rigid body motion calculated by using the OSDCT and the digital speckle–displacement measurement technique are compared. The robustness of some JTC versions (a conventional JTC, a JTC with median thresholding, a JTC with subset median thresholding, and a fringe adjusted filter JTC) to input noise of speckle patterns and output noise of a correlation response is studied.