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P. Paufler 《Crystal Research and Technology》1995,30(7):920-920
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P. Rdolph 《Crystal Research and Technology》1992,27(6):824-824
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Vivek K. Gupta K. N. Goswami D. K. Gupta K. K. Bhutani 《Crystal Research and Technology》1995,30(3):359-366
The crystal structure of R(–)-1-tosyl-2-methylpyrrolidine has been determined by X-ray structure analysis. The compound crystallizes in the monoclinic space group P21 with cell parameters a = 7.858(1), b = 14.929(6), c = 11.128(1) Å, β = 105.42(1)°. The structure has been solved by direct methods and refined to R = 0.046. There are two crystallographically independent molecules A and B in the asymmetric unit. The pyrrolidine ring of molecule A is disordered with atom C4 occupying two possible sites. The S atom has a distorted tetrahedral coordination in both the molecules. Two bifurcated hydrogen bonds are observed. Molecules are held together by hydrogen bonds. 相似文献
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A. Andreeff 《Crystal Research and Technology》1991,26(4):446-446
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V. Gottschalch 《Crystal Research and Technology》1995,30(2):236-236
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