ICP-AES法同时测定茶叶中的锌、铁、锰、铜、镍、镁

研究了用硝酸＋硫酸＋高氯酸消解样品，用ICP－AES法同时测定茶叶中锌，铁，锰，铜，镍，镁的新方法，在选定的最佳条件下，测锌，铁，锰，铜，镍，镁的检出限分别为4．2，7.8,0.4,7.3,7.6,4.8ng.mL^-1，回收率为94．7％－104．2％，RSD为0．3％－4．7％，该法准确，快速，简便，适用于茶叶样品的测定，结果令人满意。     

灵武长枣VC含量的高光谱快速检测研究

采用可见-近红外高光谱成像技术结合化学计量学方法检测灵武长枣维生素C(VC)含量，探究一种全新的水果内部成分的快速无损检测方法。采用高效液相色谱法(HPLC)测得长枣的VC含量化学值，可见-近红外高光谱成像系统采集164个灵武长枣400～1 000 nm的高光谱图像，利用ENVI4.8软件提取图像的感兴趣区域(region of interest，ROI)，计算其平均光谱，获得光谱值，将化学值与光谱值通过The UnsecramblerX 10.4软件建立模型。利用蒙特卡洛交叉验证法剔除异常值，采用光谱理化值共生距离法(sample set partitioning based on joint x-y distance，SPXY)进行样本划分以提高模型的预测性能；对光谱采用移动平滑(moving average)、中值滤波(median filter)、归一化(normalize)、基线校准(baseline)、多元散射校正(multiple scattering correction，MSC)、去趋势(detrending)和标准正态变量变换(standard normal variate，SNV)等7种方法进行预处理；为进一步减少数据量，降低维度，提高运算速度，使用竞争性自适应加权算法(competitive adaptive reweighted sampling，CARS)、无信息变量消除算法(uninformative variable elimination ，UVE)和连续投影算法(successive projections algorithm，SPA)提取特征波长，以期实现以少数波段代替全波段；将全波段光谱(full spectrum，FS)以及CARS, UVE和SPA三种方法提取的特征波长分别建立偏最小二乘(partial least squares wavelength regression，PLSR)和支持向量机(support vector machine，SVM)模型，从而确定最优的建模模型。利用蒙特卡洛交叉验证法共剔除7个异常样本，采用SPXY法将剔除异常样本后的157个数据区分为校正集和预测集，校正集中样本个数为117，预测集中样本个数为40。将未经光谱预处理的建模结果与分别经过七种光谱预处理的建模结果相比，选择未经光谱预处理的数据进行后续分析；将未经光谱预处理的光谱值采用CARS，UVE，SPA方法进行提取特征波长，CARS共优选出406，415，487，631，636，655，660，665，670，684，689，694，723，732，747和881 nm下的光谱变量16个，利用CARS提取出的特征波长占总波长的12.8%；UVE共优选出406，415，627，631，636，651，655，660，665，670，675，679，684，689，694，699，703，708，742，747，751，756，761，766，771，775，780，785，790，795，919和924 nm下的32个特征波长，利用UVE提取出的特征波长占总波长的25.6%；SPA共优选出401，665，684 nm三个特征波长，利用SPA提取出的特征波长占总波长的2.4%。将全波段光谱与提取出的特征波长建立PLSR模型和SVM模型，对比模型结果显示UVE-SVM模型最优，其R2_c为0.847 1，R2_p为0.714 9，说明UVE有效地对光谱进行降维，简化了数据处理过程。本研究对高光谱成像技术在水果领域的应用进行了有益探索，探究了一种全新的灵武长枣VC含量的无损检测方法，相应建立的可见-近红外高光谱模型为其他水果成分的快速检测提供了理论基础。     

σ^＊和Ф介子对有限温度中子星物质的影响

考虑到矿，中介子的贡献及重子八重态{n，p，∧，∑^-，∑^0，∑^＋，≡^-，≡^0}，采用相对论平均场方法，在5—25MeV的有限温度范围内，对中子星物质的性质进行了研究．发现当考虑到σ^＊，Ф介子的贡献后，超子出现的临界密度降低了（但对∧超子，影响并不显著），超子的粒子数密度增加了，在能量密度较高时物态方程变软，中子星的最大质量变小而相应的半径增大，中子星的中心粒子数密度、中心能量密度和中心压强都降低了．当温度为较低的T=5MeV，10MeV时，σ^＊，Ф介子的参与使出现∑^0，≡^0，∑^＋超子的临界密度极大地降低了；但当温度为较高的T=15MeV，20MeV，25MeV时，影响则较小．对于∧，∑^-，≡^-超子来说，在上述所有温度下，矿，中介子对超子出现的临界密度的影响都不明显．     

X射线荧光光谱法测定硅酸盐中硫等20个主、次、痕量元素

本文使用新研制的偏硼酸锂和四硼酸锂混合熔剂，在１０００℃熔融制样，以Ｘ射线荧光光谱法测定硅酸盐等样品中的Ｓ，Ｎａ，Ｍｇ，Ａｌ，Ｓｉ，Ｐ，Ｋ，Ｃａ，Ｔｉ，Ｍｎ，Ｆｅ，Ｂａ，Ｃｒ，Ｖ，Ｓｒ，Ｚｒ，Ｒｂ，Ｃｕ，Ｎｉ和Ｎｂ等２０种元素，采用理论α系数和康普顿散射线作内标校正元素间的吸收－增强效应。其分析结果的精密度和准确度可与化学法相比     

非碳纳米管研究的新进展

文章系统地论述了非碳纳米管的制备，较详尽地介绍了多种非碳纳米管制备最新的进展，包括硫化物、氮化物、氧化物等等，特别重点地总结了非碳纳米管前沿材料，例如WS2，Bi2S，，ZnS，GaN，BN，AlN，InP，Eu2O3，，V2O3等．最后对非碳纳米管的研究趋势作了展望．     

元素在探针表面上的原子化机理研究

探针原子人经法是一种新技术，本文系统地总结了用探针原子化法研究Ａｕ（１Ｂ），Ｓｒ（ⅡＡ），Ｃｄ（ⅡＢ），Ａｌ（ⅢＡ），Ｌａ，Ｓｍ，Ｆｕ（ⅢＢ），Ｇｅ，Ｓｎ，Ｐｂ（ⅣＡ），Ｓｂ，Ｂｉ（ⅤＡ），Ｖ（ⅤＢ），Ｃｒ，Ｍｏ（ⅥＢ），Ｍｎ（ⅦＢ），Ｆｅ，Ｃｏ，Ｎｉ，Ｐｔ（Ⅷ）等２０个元素的原子化机理了起源于卤化物分解的元素有Ａｕ与Ｐｔ，起源于氧化物分解的元素有Ｃｄ，Ａｌ，Ｌａ，Ｓｍ，Ｅｕ，Ｇｅ，Ｍｎ与Ｆｅ。     

中药方剂煎煮液中ICP—AES法同时测定16个元素

本文提出了用硝酸－过氧化氢对中药方剂煎煮液进行处理，ＩＣＰ－ＡＥＳ法对煎煮液中Ｌｉ，Ｎａ，Ｂｅ，Ｃａ，Ｓｒ，Ｂａ，Ｍｇ，Ｃｕ，Ｃｏ，Ｎｉ，Ｚｎ，Ｍｎ，Ｃｄ，Ｆｅ，Ｃｒ，Ｖ１６个元素进行同时测定的方法，该方法简单，快速，准确度高，所测元素的加标回收率均在８５～１０３％之间，样品分析结果满意。     

f0（975）和Ф（1020）介子对中子星物质的影响

利用相对论平均场理论，考虑了σ＊，Ф介子及重子八重态{N，P，A，∑^-，∑0,∑＋，Ξ^-，Ξ^0}，研究了中子星的性质．发现当考虑了σ＊，Ф介子的贡献时，超子出现的临界重子数密度降低了，超子数目增加了，超子星的转变密度poH降低了，物态方程变软，最大质量变小而相应的中子星半径增大，中子星的中心重子数密度、中心能量密度和中心压强均降低．     

LHCD的径向扩散效应

根据低杂波驱动电流的准线性理论，利用二维Ｆｏｋｋｅｒ－Ｐｌａｎｋ方程模拟程序，求出速度空间扩散的驱动电流，考虑快电子的径向扩散效应对驱动电流的影响，对原有程序加以完善，并ＨＴ－７，ＨＴ－６Ｍ装置进行了大量模拟计算，结果表明，考虑径向扩散后，原有的驱动电流以分变平很宽，并且变得光滑，同时驱动电流明显减小，驱动效率降低，另外，对于不同的径向扩散系数，电流密度的分布也有较大的差异。     

TBP色层分离—ICP／AES法测定锆铀铒合金中十七个微量杂质元…

本法对锆铀铒合金中十七个微量杂质元素和铒的测定进行了较系统的实验研究。取样１００ｍｇ时，Ａｌ，Ｃａ，Ｃｏ，Ｃｒ，Ｃｕ，Ｆｅ，Ｍｇ，Ｍｎ，Ｍｏ，Ｎｉ，Ｐｂ，Ｓｎ，Ｔａ，Ｔｉ，Ｖ，Ｙ和Ｚｎ的测定范围为３０－３２００μｇ／ｇ，Ｅｒ为０．２－３．２％，回收率９４－１０８％，ＲＳＤ为０．２－２．１％。     

Use of optical fiber bundle in digital image plane holography

Use of optical fiber bundles (OFBs) in digital image plane holography systems is limited due to, first, poor quality of transmitted images through the OFB and, second, further image degradation caused by overlappings in the image (also hologram) plane. Existing systems are aimed at near-distant (order of a centimeter) objects and use demanding procedures to achieving acceptable quality of holographic reconstructions. This paper presents an OFB based holographic system capable of achieving fast and good-quality holographic and interferometric reconstructions of far-distant (order of a meter) objects. The proposed system is based on performing subtraction operations through the image acquisition interface buffers directly accessed to process the holograms and instantly display the output. The system is analyzed theoretically and its effectiveness is validated by experimental results.     

Optical corrosion meter

In a previous study, a mathematical model relating surface and bulk behaviours of metals in aqueous solution has been developed. The model was established based on principles of holographic interferometry for measuring microsurface dissolution, i.e. mass loss, and on those of electrochemistry for measuring the bulk electronic current, i.e. corrosion current. In the present work, an optical corrosion meter was built based on the above model. The corrosion meter consists of an electrochemical cell in which the sample is immersed in aqueous solution. Furthermore, the corrosion meter has a holographic camera with a thermoplastic film for in situ processing of holograms in order to obtain real-time holographic interferoms of the sample in the electrochemical cell. Results of the present work indicate that optical holography is a very useful technique for measuring the corrosion current density of different alloys in aqueous solutions. As a result, the corrosion current density of aluminium, stainless steel, and low-carbon steel in 1 M KCl, 1 M NaCl, and 1 M NaOH solutions were obtained. A comparison between the corrosion data of samples showed that the corrosion current density of the stainless steel in 1 M NaCl is nearly three-folds higher than that of the aluminium in 1 M KCl and the low-carbon steel in 1 M NaOH.     

动态全息三维显示研究最新进展

全息三维显示是真三维显示技术, 其原理是利用光学干涉记录和衍射再现将物体或场景的三维信息全部重建出来, 所以观看全息三维图像与观看真实物体或场景的效果一样. 近期全息研究领域有一些突破性的成果被报道, 将推动全息显示的应用不断走向成熟. 本文将重点介绍基于光学材料和空间光调制器为全息图承载载体的动态全息三维显示最新发展状况. 虽然动态全息三维显示研究仍然存在挑战, 但最近研究中已经利用光学材料实现了实时动态全息三维视频显示, 这为未来实现大尺寸、高分辨率、彩色全息真三维视频显示提供了可能.     

Holographic distant display in dichromated gelatin

A transmission holographic optical element (HOE) has been manufactured, which changes the direction and divergence of light from a laser-illuminated transparent object, for example, a meter scale, so creating a virtual image a considerable distance from the viewer. The HOE is made in dichromated gelatin, with Ar laser light of wavelength 488 nm, and is reconstructed at 633 nm with a HeNe laser. Diffraction efficiency, luminance and contrast are measured at various points in the 16 X 16 cm² hologram. The visibility is good and there are modest distortions.     

Holographic particle image velocimetry (HPIV)

There are several well-known difficulties in forming and analysing holographic particle data in the micrometre and sub-micrometre size range. This paper suggests that these problems can be overcome by using a combination of research techniques. Firstly, it has been found that it is possible to record images of sub-micrometre particles using conventional photographic materials. Essentially, a diffraction limited optical component has been used to provide aberration free particle images. Secondly, the sensitivity of the holographic material has been increased with the use of specialized holographic processing chemicals. Thirdly, it has been found that it is possible to encode holoraphically double, slightly displaced, particle images using a pulse laser. Thus, Young's fringes can be obtained directly from the stored holographic data and the particle velocity can be measured directly from the hologram. Fourthly, the holographic particle data can be automatically analysed using a software programme. Finally, since the data is stored holographically, it is possible to obtain instantaneous three-dimensional particle velocity. This paper demonstrates that it is possible to perform holographic particle image velocimetry automatically, with only a small amount of pre-processing.     

Quantitative analysis of holographic particle data

There are several well known difficulties in forming and analysing holographic particle data in the micrometre and submicrometre size range. This paper suggests that these problems can be overcome by using a combination of research techniques. Firstly, it has been found that it is possible to record images of submicrometre particles by using conventional photographic materials. Essentially, a diffraction limited optical component has been used to provide aberration free particle images. Secondly, the sensitivity of the holographic material has been increased with the use of specialized holographic processing chemicals. Thirdly, it has been found that it is possible to encode holographically double, slightly displaced, particle images by using a pulse laser. Thus, Young's fringes can be obtained directly from the stored holographic data, and the particle velocity can be measured directly from the hologram. Fourthly, the holographic particle data can be automatically analysed, using a software program. Finally since the data is stored holographically, it is possible to obtain instantaneous 3-D particle velocities. This paper demonstrates that it is possible to perform holographic particle image velocimetry automatically, with only a small amount of preprocessing.     

An approach for sensing marine plankton using digital holographic imaging

The goal of this paper is to use digital holographic imaging for sensing marine plankton in recording sampling volume. The process stage of this approach includes: wavefront recording using in-line holographic recording set up and numerical reconstruction using Fresnel approximation and convolution algorithm. So, by capturing hologram of marine plankton and reconstructing hologram, the recorded optical field of marine plankton is retrieved. Digital holographic imaging is an extremely powerful technique for the study of marine plankton fields as it allows instantaneous, noninvasive, high-resolution recording of substantial volumes. Finally, this paper presents that it is possible for digital holographic imaging system to sense marine plankton according to laboratory results.     

Archival storage of color films by rainbow holographic technique

A technique of generating color holographic images with a one-step rainbow holographic process is described. This technique offers the capability of archival storage of color materials on a single black and white photographic film. The process is very simple to implement and it allows the reconstruction of the color image with a white light source. Although some degree of color blur is inherent with the rainbow holographic process, it can be minimized by the proper design of the optical system. A simple experimental result is also presented.     

尾流的全息成像方法研究

鉴于全息三维成像的独特优点,提出了一种新的尾流测量方法---全息成像测量.在对影响水下全息成像各种因素进行详细理论分析的基础上,自行设计了激光在尾流场的衰减实验和尾流全息成像试验.衰减实验表明,在气泡幕数密度一定的情况下,激光衰减率基本保持恒定;尾流全息成像利用双脉冲激光配合使用4F放大系统首次记录下了气泡幕的全息图像.实验表明,气泡幕全息成像效果良好,证明尾流参量的全息测量方法是可行的.     

Holographic dark energy in a cyclic universe

In this paper we study the cosmological evolution of the holographic dark energy in a cyclic universe, generalizing the model of holographic dark energy proposed by Li. The holographic dark energy with c<1 can realize a quintom behavior; namely, it evolves from a quintessence-like component to a phantom-like one. The holographic phantom energy density grows rapidly and dominates the late-time expanding phase, helping to realize a cyclic universe scenario in which the high energy regime is modified by the effects of quantum gravity, causing a turn-around (and a bounce) of the universe. The dynamical evolution of holographic dark energy in the regimes of low energy and high energy is governed by two differential equations, respectively. It is of importance to link the two regimes for this scenario. We propose a link condition giving rise to a complete picture of holographic evolution of a cyclic universe.