The change in primary extinction during decomposition of a super saturated solid solution 1. System Al-Ag

On the basis of the correlation of diffraction data (intensity and width) of a precipitate with the intensity of reflection of a matrix solid solution it is shown that the change in primary extinction during the decomposition of a solid solution of Agin Alis caused by the precipitation of the phase Ag₂Aland not by the production of lattice defects (zones, stacking faults).

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I. Al-Ag

( ) , Ag Al Ag₂Al, ( , ).

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Reported in part at the VIth Scientific Technical Conference on the Application of X-rays held in Leningrad in 1958.

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The author thanks M. Mikovský for preparing the single crystals of the alloy Al-Ag having a high primary extinction and J. Laek and Prof. J. Bedná for carefully checking their homogeneity and chemical composition.     

The temperature vibrations of urea molecules

The structural and dynamic parameters of urea at 112°K and 295°K were determined by the least squares method. The characteristic temperature of the torsional optical vibrations of a molecule about a C-O bond was determined and is in good agreement with the value determined by Raman scattering. The fractional X-coordinate of the nitrogen atom corrected for torsional vibrations was determined and it was found that the magnitude of the projection of the C-N bond in the given temperature range changes only within the limits of observational errors. A new method, called temperature difference synthesis, is described and it is shown that it is suitable for rapid qualitative determination of the thermal anisotropy of the vibrations of atoms in a crystal lattice.

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112°K 295°K. C-O , , . X- , C-N . , , , .

     

The quantum efficiency of the internal photo-electric effect in indium antimonide

A method is described for measuring the relative quantum efficiency of the internal photo-electric effect in semi-conductors by simultaneously measuring the photo-magnetoelectric and photo-conductive effect. The results of measurements on indium antimonide are given. The quantum efficiency begins to increase if the energy of the photon exceeds 0·47 eVat room temperature. The quantum efficiency as a function of the energy of the photon is analysed on the basis of the conception of impact ionization and it is shown that a study of the structure of this curve can supply information on the, band structure of a semi-conductor in the region of high energies of electrons and holes.

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. . , 0,47 eV . , .

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The authors thank M. Závtová and M. Vantuchová for efficient help with the measurements, K. mirous and V. Vrchovská for preparing the material, E. Antoník for critical remarks and M. Matyá and A. Müller for determining the constants of the material.     

The distribution of ions and their valencies in manganese ferrites I. MnFe2O4+γ ferrites

A model for the distribution of cations in the spinel lattice of manganese ferrites MnFe₂O₄₊ was elaborated on the basis of the experimental studies of the basic magnetic quantities, electrical conductivity and magnetic relaxation of the given ferrites, taking into consideration their crystallographic properties. The conclusions following from this model are in good agreement with the experimental results obtained by us and by other authors both for stoichiometric manganese ferrite and for a ferrite where 0.

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I. MnFe₂O₄₊

, MnFe₂O₄₊ . , , , , , 0.

     

Ausgestaltung der ursprünglichen Methode für das Studium des Barkhauseneffektes und Beurteilung dessen Wiederhol-Barkeit

Ohne Zusammenfassung

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Three variations in the intensity of cosmic radiation in the first half of 1958

The time courses are given of three variations in the intensity of cosmic radiation, which occurred in the first half of 1958. The measuring apparatus is described and the energies of the particles recorded a reestimated. The paper is the partial result of systematic measurements of the intensity of cosmic radiation carried out in Czechoslovakia in the International Geophysical Year.

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1958

, 1958 . . , .

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The authors heartily thank the Institute of Geomagnetism in Krasnaja Pachra, near Moscow, and especially its director, Prof. M. B. Pukov, and Dr Ju. M. Kopylov for the neutron counters.The authors wish to thank Prof. V. Petrílka, corresponding member of the Czechoslovak Academy of Sciences, and Prof. L. Jurkiewicz, from the Academy of Mining and Heavy Industry in Cracow for help in the work and Academician J. Novák, who made possible the numerical evaluation of the data in the Mathematical Institute of the Czechoslovak Academy of Sciences. Especial thanks go to F. Pilát and B. Slavík for their great help in setting up the apparatus and to all colleagues who took part in the measurements.     

Entstehung von Elektronen und Löchern bei Chemischen Reaktionen an der Oberfläche des Germaniums

Ohne Zusammenfassung

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qc

     

Change in primary extinction during decomposition of supersaturated solid solution II. Al-Cu 4% alloy-formation of G.P. zones

The change in integrated intensity of the (200) reflections of a solid solution during the formation of G.P. zones was measured and compared with the change in the character of the diffuse streaks corresponding to them. It was found that the. formation of G.P. zones does not lead to a decrease in primary extinction despite the great changes in the distribution of the copper atoms. It was shown that the formation of a precipitate accompanied by the formation of crystallographically incoherent boundaries greatly decreases the primary extinction.

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. II. 1-u 4%: [. . ]

(200) . . , . , . . , . , , , .

     

Steady temperature in a composite rectangle

The present paper solves the steady temperature problem in a rectangle consisting of any number of homogeneous isotropic parts. As usual with such questions, the results are very complicated and cannot be found in the literature.

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, . , - .

     

Vereinfachung der Formeln zur Berechnung der Optischen Konstanten von Absorbierenden Stoffen

Ohne Zusammenfassung

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The influence of the spectral asymmetry of X-ray emission lines on the results of studying defects in crystals by X-rays of different wavelength

Since the asymmetry of X-ray emission lines was found to influence the exact measurements of lattice parameters of powdered samples the author has revised the results she once obtained when carrying out exact measurements of the lattice parameter with radiations of various wavelengths for tungsten crystals containing admixtures of different elements. It is shown that with samples having an inhomogeneous distribution of the admixtures in the crystals the typical graphs of lattice parameter found originally remain when respecting the influence of the spectral asymmetry. On the other hand, with a sintered sample which has been homogeneized by long annealing the introduction of corrections to spectral asymmetry leads to an adjustment of the differences measured originally, for which it was difficult to find a probable explanation.

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, . , , . , , , , , , .

     

Die halbleitende Vebbindung SiTe

Ohne Zusammenfassung

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SiTe

     

Double quantum transitions in paramagnetic resonance

The theory of double quantum transitions of the M=±2 type, with regard to inhomogeneously broadened spin systems is studied in this paper with the approximation ²T₂T₃ 1. We suppose that the inhomogeneous broadening is formed by an inhomogeneous crystal field. The obtained results describe the magnitude of absorption as a function of the h.f. power and also describe the shape of the absorption curve. It is demonstrated that in inhomogeneously broadened spin systems the absorption curve of double quantum transitions has the form of the difference of two different Lorentz's curves and that at the saturation ( ²T₂T₁ 1) the absorption increases with the cube of the h.f. field intensity. The shape of the curves is expressed by means of phenomenological relaxation constants of the system.

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M=±2 ²T₂T₃ 1. , - . . , ( ²T₂T₁ 1) . .

     

Anwendung der Hochfrequenzmessmethode für die Elektronenkonzentration zur Messung in der geschichteten positiven säule der Gleichstromglimmentladung

Zusammenfassung In der vorliegenden Arbeit werden Beziehungen abgeleitet, mit deren Hilfe es möglich ist, die Hochfrequenzresonanzmethode der Diagnostik des Plasmas zur Messung der Änderungen der Elektronenkonzentration in den laufenden Schichten in der positiven Säule der Glimmentladung zu verwenden. Ferner wird die Anwendung dieser Methode diskutiert, und zwar für den Fall, daß die Zusammenstoßfrequenz der Elektronen nicht von der Elektronengeschwindigkeit abhängt, und für den Fall, in dem die Zusammenstoßfrequenz der Elektronen eine Funktion der Elektronengeschwindigkeit ist.

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. , , , , .

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Abschließend dankt der Verfasser den Herren Prof. V. Kunzl und R. Bakule für ihre wertvollen Hinweise zu dieser Arbeit.     

Stationary states of an electron in the field of a hole in an ionic crystal

An approximate solution is given of the Schrödinger equation for S-states of an electron in the field of a hole, when the potential energy of the electron has the form — e²/r [1+exp (–qr].

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s- , –e²/r [1+exp (–qr].

     

Quantitative method for determination of fibre texture in wires I. Principle of method and analytical expression of absorption factor

An X-ray diffraction method is described for the quantitative determination of the fibre texture in cylindrical specimens (wires), which does not require specimen preparation. The integrated intensity of the diffracted radiation from a certain atomic plane is measured in the direction parallel to the plane determined by the axis of the wire and by the direct beam for different orientations of the axis of the wire. These measurements can be carried out in practice using an X-ray counter diffractometer or Weissenberg goniometer. The pole figure is determined from the dependence of the diffracted intensity on the orientation of the wire after correcting the intensities for the absorption of radiation in the specimen. The geometric arrangement enables the absorption factor to be calculated analytically. Its form was verified experimentally by measuring the dependence of the intensity of the 220 reflection on the orientation of the axis of a cylindrical specimen of Al containing randomly oriented crystals.

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I.

( ), . , , , . . , . . 220 .

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The author wishes to thank Z. iký for help in carrying out the measurements and calculations.     

Energy spectrum of electron pairs in a high energy photon-electron cascade

The energy spectrum of electron pairs generated in a high energy photon-electron cascade up to a depth of 1·5 c. u. was measured and the possible influence of the medium on the shape of the spectrum according to Landau-Pomeranuk-Ter Mikaelyan and Migdal was investigated. Two procedures were used for the analysis; no significant deviation from the Bethe-Heitler spectrum could be observed. Different ways of estimating the primary energy were applied; the resulting value, 2×10¹²eV, was accepted as the primary energy.

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-

, - 1,5 , - . ; - . ; 210¹² eV.

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The authors wish to thank Dr. Lanius for kindly lending them the necessary plate from the Berlin part of the I-stack.     

Die Veränderung einer Metalloberfläche nach der Elektronenemission unter atmosphärischen Bedingungen

Ohne Zusammenfassung

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The influence of compression on the absorption of AgBr single crystals

The influence of compression on the edge of self absorption of AgBr single crystals was studied. The measurements were performed at a temperature of –180°C. The shift of the edge of self absorption was studied both in the field of elastic and plastic deformations. The shift of the absorption edge towards the UV end of the spectrum was determined in the field of elastic deformations and towards the i.r. end in the field of plastic deformations. After the ending of the deformation and after unloading the crystal the return of the absorption edge towards the original position was observed.

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AgBr

AgBr. –180°C. , . , — . .

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The author thanks Prof. Dr. L. Zachoval and K. K. Vacek C. Sc. for their interest in this work and for many comments given during the work.     

Ferromagnetic resonance in thin cobalt films

The paper gives the results of measuring ferromagnetic resonance on thin cobalt films, vacuum deposited on unheated glass slides. The values of the (g-factor, the width of the curve, the effective stress and uniaxial induced anisotropy were determined as a function of the thickness of the film from measurements of the ferromagnetic absorption in a magnetic field normal and parallel to the surface of the film. Measurements were carried out on a frequency of 9200 MHz and on film thicknesses of 180 to 1800 Å. A qualitative explanation of the observed dependences is given.

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, . , , g-, , , . 9200 MHz 180–1800 Å. .

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The author thanks V. Kamberský and Z. Málek, C. Sc., for providing some of the cobalt films and for help in depositing and measuring the thicknesses, S. Kadeková and M. Polcarová for valuable advice in determining the structure of the films, J. Míová for carefully plotting the results of measurements and Z. Málek and O. tirand for carefully reading the paper and for valuable discussions.